📜Sodium Triethylborohydride 以2%的收率获得 参考文献:Koster,Roland;Seidel,Gunter;Boese,Roland;Wraekmeyer,Bernd,Chem. Ber.,121,(1988) N 11,C. 1955-1966 标题:Koster,Roland;Seidel,Gunter;Boese,Roland;Wraekmeyer,Bernd,Chem. Ber.,121,(1988) N 11,C. 1955-1966
专利信息
专利号:US-7615169-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY FIELDING; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-7927516-B2 优先权日:2004-09-20 标题 :Method for synthesis of colloidal nanoparticles 发明人:STROUSE GEOFFREY F; GERBEC JEFFREY A; MAGANA DONNY 权利人:UNIV CALIFORNIA 摘要:A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.
专利号:US-8354524-B2 优先权日:2001-03-22 标 题:Synthesis of selenium-derivatized nucleosides, nucleotides, phosphoramidites, triphosphates and nucleic acids 发明人:HUANG ZHEN 权利人:UNIV GEORGIA STATE RES FOUND; HUANG ZHEN 摘要:The present invention provides selenium derivatives of nucleosides, nucleoside phosphoramidites, nucleotides, nucleotide triphosphates, oligonucleotides, polynucleotides, and larger nucleic acids and methods for their synthesis. Selenium derivatives of both ribonucleic acids and deoxyribonucleic acids, as well as methods for their synthesis, crystallization and uses in structural determinations, particularly by X-ray crystallographic techniques are disclosed. The selenium derivatives of the present invention are also useful as food supplements.
专利号:US-2004171072-A1 优先权日:1998-03-31 标题:Solid support based on selenium useful in solid phase synthesis 发明人:RUHLAND THOMAS; ANDERSEN KIM; PEDERSEN HENRIK 权利人:LUNDBECK & CO AS H 摘要:This invention relates to novel solid support based on selenium and a method for the preparation thereof. The solid support is useful in solid phase synthesis of organic compounds including combinatorial libraries of compounds.
专利号:WO-0104382-A1 优先权日:1999-07-13 标题:Sonoelectrochemical synthesis of inorganic fullerene-like nanoparticles of metal chalcogenides 发明人:HODES GARY; MASTAI YITZHAK; HOMYONFER MOSHE; TENNE RESHEF 权利人:YEDA RES & DEV; HODES GARY; MASTAI YITZHAK; HOMYONFER MOSHE; TENNE RESHEF 摘要:Inorganic fullerene-like (IF) nanoparticles of metal chalcogenides, particularly molybdenum sulphide, including one or more layers of desired sizes and shapes, e.g., spheres, sphere-like, nanotubes and polyhedral shapes, are manufactured by sonoelectrochemical liquid-phase synthesis comprising: (a) dissolving in a suitable solvent: (i) at least one compound of said metal and at least one compound of said chalcogen, or (ii) at least one said chalcogen-containing said metal compound; (b) immersing an electrically conductive ultrasonic probe in the solution obtained in (a); (c) electrically connecting the ultrasonic probe, which operates as an electrode, to one terminal of an electric power supply, and the other terminal of said electric power supply is connected to a counter electrode; (d) applying an ultrasonic signal to said ultrasonic probe electrode and an electric voltage to both the ultrasonic probe electrode and the counter electrode; and (e) recovering the IF-metal chalcogenide structures that precipitated in step (d).
专利号:US-2006240590-A1 优先权日:2004-11-09 标题:Controlled synthesis of nanowires, nanodiscs, and nanostructured materials using liquid crystalline templates 发明人:MOUNTZIARIS TRIANTAFILLOS J; ALEXANDRIDIS PASCHALIS; KARANIKOLOS GEORGIOS N 权利人:UNIV NEW YORK STATE RES FOUND 摘要:A process for synthesizing nanostructures involving providing a first reactant, forming a liquid crystalline template containing the first reactant and contacting the template with a gas phase composed of a second reactant under conditions effective to form nanostructures is disclosed. A method of making a liquid crystalline template by combining and allowing to react a block copolymer, a polar continuous phase material, and a dispersed nonpolar phase material under conditions effective to form the liquid crystalline template is also disclosed.