CAS: 7789-21-1; Sulfurofluoridic Acid

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欧盟法规

统一分类与标签REACH注册ECHA物质工作场所安全标识要求ECHA物质C&L通报REACH预注册废弃物危险特性清单

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CAS号7664-39-3 氟化氢 | CAS号697-18-7 四氟乙烷-beta-磺内酯 | CAS号773-15-9 1,2,2-三氟-2-羟基-1... | CAS号7783-05-3 disulphuric acid | CAS号13709-32-5 bis(fluorosulfu... | CAS号2925-25-9 2,2,2-trifluoro... | CAS号7446-11-9 三氧化硫 | CAS号14483-63-7 fluorosulfonic acid | CAS号7790-94-5 氯磺酸 | CAS号14996-02-2 Hydrogen Sulfate | CAS号430-71-7 丙醯氟 | CAS号455-16-3 对甲苯磺酰气氟 | CAS号13036-75-4 DISULFURYL FLUO... | CAS号381-72-6 二氟乙酰氯 | CAS号13478-20-1 Phosphoryl fluoride | CAS号15099-42-0 tetrabromophosp... | CAS号7726-95-6 溴素 | CAS号14483-63-7 fluorosulfonic acid | CAS号14984-73-7 imido-bis(sulfu... | CAS号7647-01-0 盐酸

合成工艺路线路线简述

    氢氟酸置于硫酸体系中,用 水 作为反应溶剂,化学反应生成 氟磺酸
    参考文献:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: F: Svol.1,54,Page 207-209
    标题:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: F: Svol.1,54,Page 207-209

    专利信息


    专利号:US-10711138-B2
    优先权日:2016-04-08
    标题:Intermediates and procedures for the synthesis of functional materials
    发明人:KIRSCH PEER; GUNST SUSANN
    权利人:MERCK PATENT GMBH
    摘要:The present invention relates to heteroaromatic compounds which have two different reactive groups, their use in the synthesis of asymmetrically substituted compounds, and synthesis processes in which the compounds according to the invention are reacted sequentially with two different compounds, whereby an asymmetrically substituted compound is formed.

    专利号:WO-2025119975-A1
    优先权日:2023-12-04
    标 题:A method for synthesis of harmine
    发明人:HETT ROBERT; GRAB HANUSCH; LAGOUTTE ROMAN
    权利人:RECONNECT LABS AG
    摘要:The invention relates to a method of synthesis of a compound of formula (I), harmine, according to the method comprising a step of transforming the compound of formula (II), into the compound of formula (I). The invention further relates to a compound of formula (II), which is an intermediate in synthesis of harmine according to the present invention.

    专利号:US-2025129495-A1
    优先权日:2021-09-24
    标 题:Method for the electrochemical synthesis of ammonia and apparatus for carrying out the method
    发明人:FINKELSHTAIN GENNADI; BORCHTCHOUKOVA NINO; SHIROKOV ALEXANDER V; ENGLANDER JOSEPH ALEXANDER; SHARABI RONIT; ZABILSKIY MAXIM; TSAI TSEPIN
    权利人:GENCELL LTD
    摘要:A method for the electrochemical synthesis of ammonia (NH 3 ) comprises contacting a nitrogen-containing gas with the cathode of an electrochemical cell comprising a cathode, an anode, an alkaline aqueous electrolyte, and preferably an anion exchange membrane. The cathode is a porous gas diffusion electrode which comprises an active layer comprising a material which is capable of catalyzing the electrochemical reduction of nitrogen and is in contact with the electrolyte, a layer of electroconductive material supporting the active layer, and a porous polymer film on the side of the active layer which does not come into contact with the electrolyte and comes into direct contact with the nitrogen-containing gas. A potential over the electrochemical cell is applied to effect the electrochemical synthesis of ammonia from nitrogen and water. The method can be used to synthesize ammonia without using molecular hydrogen.

    专利号:US-2025188046-A1
    优先权日:2023-12-08
    标题:Ultrafast flow synthesis of functionalized sulfonyl fluorides and subsequent sufex connections via lithiated chemistry
    发明人:KIM DONG-PYO; KANG JI-HO
    权利人:POSTECH RES & BUSINESS DEV FOUND
    摘要:Disclosed are ultrafast flow synthesis of functionalized sulfonyl fluorides and subsequent SuFEx connections via lithiated chemistry. In detail, a method of synthesizing an ortho-functionalized benzenesulfonyl fluoride derivative, the method comprises (a) reacting a benzenesulfonyl fluoride derivative represented by structural formula 1 with an organolithium represented by structural formula 2, thus synthesizing an intermediate represented by structural formula 3 in reaction scheme 1 and (b) reacting the intermediate with an electrophile, thus synthesizing a compound represented by structural formula 4 or a compound represented by structural formula 4′. The present disclosure enables the synthesis of several functionalized sulfonyl fluorides within a few seconds under mild temperature conditions in addition to the chemistry of Sulfonyl Fluoride Exchange (SuFEx), which is a next-generation click chemistry, so that sulfonyl fluoride, the main reactant of the SuFEx reaction, can be efficiently secured.

    专利号:WO-2022269384-A1
    优先权日:2021-06-24
    标 题 :A process for the direct synthesis of fedratinib intermediate
    发明人:DESAI ASIM HEMANTBHAI; PATIL SANJAY NIMBAJI; RADADIYA VAIBHAV GOVINDBHAI; DESAI JIGNASU THAKORBHAI; DUBEY RAJEEV RAMCHANDRA; CHOUBEY Ajit Kumar
    权利人:AMI ORGANICS LTD
    摘要:The present disclosure relates to a process for the direct synthesis of Fedratinib intermediate. Particularly, the present disclosure relates to a process for the direct synthesis of 3-amino-N- (tert-butyl)benzene sulfonamide. The process of the present disclosure has various advantages such as convenient operation conditions, time-saving process, easy purification, low operation costs, good yield and efficiency hence the process is industrially feasible. The use of non-toxic, inexpensive and easily available reagents, in the process of the present disclosure, makes the process cost-efficient economic and environmental friendly.

    专利号:US-8426630-B2
    优先权日:2009-08-31
    标题:Method and apparatus for continuous flow synthesis of ibuprofen
    发明人:MCQUADE D TYLER; BOGDAN ANDREW; POE SARAH LIHOA
    权利人:MCQUADE D TYLER; BOGDAN ANDREW; POE SARAH LIHOA; UNIV FLORIDA STATE RES FOUND
    摘要:A multi-step method for the continuous synthesis of ibuprofen or a synthetic precursor of ibuprofen is provided that does not require any intermediate purification or isolation steps and uses reagents compatible with downstream reactions. According to some embodiments, a method is provided wherein isobutylbenzene and a propionyl compound may be converted into a first product in a first Friedel Crafts acylation reaction. The first product may then be converted into a second product in a 1,2-aryl migration reaction. Finally, the second product may be converted into ibuprofen in a hydrolysis reaction. The present invention also provides a method wherein only the first and second reaction steps or only the second and third reaction steps are performed. An apparatus is also provided having two or more microreactors and two or more junctions in particular arrangements for the synthesis of ibuprofen or a synthetic precursor of ibuprofen.
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    合成参考文献


    摘要:Sax, N.I. Dangerous Properties of Industrial Materials. 5th ed. New York: Van Nostrand Rheinhold, 1979., p. 693
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