Magnesium Chloride置于alum Earth Iron Phosphates体系中,用 Neat (No Solvent) 作为反应溶剂,化学反应生成 三氯化铁 参考文献:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: Fe: Mvol.B1,100,Page 225-227 标题:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: Fe: Mvol.B1,100,Page 225-227
专利信息
专利号:WO-2024084510-A1 优先权日:2022-10-20 标题 :Glutamic acid independent process for synthesis of poly gamma glutamic acid 发明人:DHARNE MAHESH SHANTAPPA; NAIR PRANAV GIRIJAVALLABHAN 权利人:COUNCIL OF SCIENT AND INDUSTRIAL RESEARCH AN INDIAN REGISTERED BODY INCORPORATED UNDER THE REGN OF S 摘要:The present invention relates to a cost-effective process for the synthesis of hyper-production of poly gamma glutamic acid using L-glutamic acid independent approach. Specifically, the present invention relates to the synthesis of poly gamma glutamic acid (γ-PGA) from jaggery, blackstrap molasses, and floral waste. More particularly, the present invention relates to a process for the synthesis of poly gamma glutamic acid in high yield and in the presence of Bacillus paralicheniformis NCIM 5769.
专利号:WO-2024185734-A1 优先权日:2023-03-03 标 题:Polyphosphorylated nucleoside, phosphate-activated nucleotide used for synthesis of polyphosphorylated nucleoside and method for synthesis of same, and method for synthesis of polyphosphorylated nucleoside using phosphate-activated nucleotide 发明人:KATAOKA MASANORI; FUKUI CHIHARU; TSUJI YOHEI; FUJIMURA Kazuma 权利人:NATIAS INC 摘要:The present invention provides: a polyphosphorylated nucleoside which has a structure represented by formula (I) and can be efficiently produced by a short process and a simple operation with use of a less expensive material; a phosphate-activated nucleotide which is used for the synthesis of the polyphosphorylated nucleoside and a method for the synthesis of this phosphate-activated nucleotide; and a method for the synthesis of a polyphosphorylated nucleoside using a phosphate-activated nucleotide. In the formula, B represents a protected or unprotected, natural or artificial nucleoside base; R 1 , R 2 , R 4 and R 5 each represent H or an alkyl group or the like, and R 1 , R 2 , R 4 and R 5 may be the same as or different from each other; X and Y each represents H, OH, OCH 3 or the like; h represents an integer of 1 to 3; p, n, m and q each represent 0 or an integer, and p, n, m and q are in no particular order; and (p + n + m + q) is an integer of 0 to 5,000.
专利号:US-4078331-A 优先权日:1976-04-28 标题:Process and culture composition for growth of alga and synthesis of biopolymer 发明人:SAVINS JOSEPH GEORGE; PAUL JAMES M 权利人:MOBIL OIL CORP 摘要:This specification discloses a process and a culture composition for growth of an alga and synthesis of biopolymer by the alga. The process involves growth of the alga and concomitant synthesis of the biopolymer in an aqueous culture containing as a source of phosphate for said alga dibasic sodium or dibasic potassium phosphate. The nitrogen source can be sodium nitrate or urea. Control of the pH of the culture is effected by injecting a mixture of carbon dioxide and air into the culture during growth of the alga and synthesis of the biopolymer. The carbon dioxide also serves as a source of carbon for growth of the alga and synthesis of the biopolymer and provides agitation/mixing within the culture chamber. Preferably, the mixture of carbon dioxide and air is injected continuously into the culture during the entire growth period of the alga.
专利号:US-2025002654-A1 优先权日:2023-06-22 标 题:Methods and applications for synthesis of carbazole phosphazene based polymer and recovery of valuable metal elements from electronic waste materials 发明人:SADAK ALI ENIS; CUCU EVREN; ARI ENGIN BETUL; TUNC MURAT; ALTUNDAS RAMAZAN 权利人:TURKIYE BILIMSEL VE TEKNOLOJIK ARASTIRMA KURUMU 摘要:A synthesis method for carbazole phosphazene based polymer and a method for the recovery of precious metal elements from electronic waste materials are provided. The developed method allows for the efficient and cost-effective synthesis of carbazole phosphazene based polymer in a single step, with high yield and easy purification. In the method for the recovery of precious metal elements from electronic waste materials, a two-step metal leaching process is employed using solutions with different acidity levels, resulting in the high-efficiency recovery of precious metal elements. The carbazole phosphazene based polymer represented by Formula 2 exhibits high selectivity in the adsorption of precious metal elements, particularly gold. Therefore, it can be applied in the recovery of gold and other precious metals from electronic waste materials in the method for the recovery of precious metal elements.
专利号:US-7326805-B2 优先权日:2003-05-07 标题 :Method for the synthesis of 4-hydroxyisoleucine and the derivatives thereof 发明人:MIOSKOWSKI CHARLES; CATALA CEDRIC; WAGNER ALAIN 权利人:MIOSKOWSKI CHARLES; CATALA CEDRIC; WAGNER ALAIN 摘要:The invention relates to a method for the synthesis of two isomers, at function OH, alone or in mixtures, of amino acids α or the derivatives thereof, having general formula (B), wherein: linkage C—O of the 4-position carbon (represented by symbol) denotes one or other of isomers III or IV, or mixtures thereof. Moreover, R 1 and R 2 represent: a hydrogen atom; or either R 1 or R 2 represents a hydrogen atom and the other substituent is a radical R a , an acyl group —COR a , such as acetyl, or a functional group —COOR a , —SO 2 R a , —N (R a , R b ), R a and R b , which are identical or different, representing a C1-C12 linear or branched alkyl radical, optionally substituted, an aryl group with one or more aromatic rings and heterocycles, comprising between 5 and 8C, optionally substituted, or aralkyl, the alkyl substituent and the aryl group being as defined above; or R 1 and R 2 both represent a substituent as defined above. R 3 represents a hydrogen atom or R a and R 4 has the significance of R a . The invention is characterised in that it comprises: the isomerisation of a compound having formula (I), wherein R 1 , R 2 , R a , R 3 and R 4 are as defined above, such as to produce a compound having formula (II); and the reduction of the carbonyl function thereof which, depending on the catalytic system employed and the formula (I) compound used, produces one of the isomers having general formula (III) or (IV) or a mixture thereof having formula (B). The invention can be used for the synthesis of (2S, 3R, 4S)-4-hydroxyisoleucine.
专利号:US-7692016-B2 优先权日:2005-11-25 标 题 :Process for the synthesis of quinoline derivatives 发明人:MADUGULA SREE RAMA MURTY; THALLAPELLY SWAMY; BANDARUPALLY JYOTHIRMAI; YADAV JHILLU SINGH 权利人:COUNCIL SCIENT IND RES 摘要:The present invention provides an improved process for the synthesis of quinoline derivatives. More particularly the present invention provides an improved and economical process for the synthesis of quinoline derivatives by the reaction of aniline/substituted anilines using two different catalysts, ferric chloride and zinc chloride in a one-pot set up reaction.
参考文献:10.1007/s11064-011-0542-y 摘要:Tang XQ, Fang HR, Li YJ, Zhou CF, Ren YK, Chen RQ, Wang CY, Hu B. Endogenous hydrogen sulfide is involved in asymmetric dimethylarginine-induced protection against neurotoxicity of 1-methyl-4-phenyl-pyridinium ion. Neurochem Res. 2011 Nov;36(11):2176–85. doi: 10.1007/s11064-011-0542-y. 参考文献:10.1007/s12010-011-9310-3 摘要:Papizadeh M, Ardakani MR, Motamedi H, Rasouli I, Zarei M. C–S Targeted Biodegradation of Dibenzothiophene by Stenotrophomonas sp. NISOC-04. Applied Biochemistry and Biotechnology. 2011 Jul 13;165(3-4):938–48. doi: 10.1007/s12010-011-9310-3. 参考文献:10.1007/s10529-011-0690-9 摘要:Juang DF, Yang PC, Chou HY, Chiu LJ. Effects of microbial species, organic loading and substrate degradation rate on the power generation capability of microbial fuel cells. Biotechnol Lett. 2011 Nov;33(11):2147–60. doi: 10.1007/s10529-011-0690-9. 参考文献:10.1007/s10529-011-0684-7 摘要:Upadhyaya CP, Venkatesh J, Gururani MA, Asnin L, Sharma K, Ajappala H, Park SW. Transgenic potato overproducing L-ascorbic acid resisted an increase in methylglyoxal under salinity stress via maintaining higher reduced glutathione level and glyoxalase enzyme activity. Biotechnol Lett. 2011 Nov;33(11):2297–307. doi: 10.1007/s10529-011-0684-7. 参考文献:10.1007/s11033-011-1158-7 摘要:Sun J, Peng RH, Xiong AS, Tian Y, Zhao W, Xu H, Liu DT, Chen JM, Yao QH. Secretory expression and characterization of a soluble laccase from the Ganoderma lucidum strain 7071-9 in Pichia pastoris. Mol Biol Rep. 2012 Apr;39(4):3807–14. doi: 10.1007/s11033-011-1158-7.