CAS: 2562-37-0; 1-Nitro-1-Cyclohexene

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📜环己烯置于碘,Sodium Nitrite体系中,用 乙二醇 用作溶剂,化学反应 72.0H,反应生成1-硝基-1-环己烷
参考文献:非平面铜电化学(ii在非水性介质)tetrabutano-和tetrabenzotetraarylporphyrins
标题:非平面铜电化学(ii在非水性介质)tetrabutano-和tetrabenzotetraarylporphyrins
摘要:合成了两个含有β,β'-稠合的四丁酸或四苯并基的四芳基卟啉铜,并在非水介质中对其电化学和光谱电化学进行了表征.所检查的化合物表示为丁酸-(t P Ypp)cu Ii和苯并-(t P Ypp)cu Ii,其中t P Ypp是卟啉二阴离子,Y是对位上的ch 3,H或cl取代基该化合物的四个内消旋-苯环中的一个.两个系列中的每个中性卟啉均具有esr活性,并在冷冻的ch 2 Cl 2中显示出典型的d 9 Cu(II)信号.解决方案.在含有0.1 M四正丁基高氯酸铵的dmf或ch 2 Cl 2中,每种cu(II)卟啉还经历了两个可逆的一电子还原和两个可逆的一电子氧化,还原后生成π阴离子基团和二价阴离子. π-阳离子具有自由基和氧化作用.还观测到phcn中丁酸-(t P Ypp)cu(y = Ch 3和h)和苯并-(tpp)cu的第三单电子氧化,该过程被分配为cu Ii / Cu Iii过渡.与e相比
Doi:10.1039/c5Ra15593B

专利信息

专利号:US-8071782-B2
优先权日:2007-10-02
标 题 :Synthesis of 1,3,4-trisubstituted and 1,3,4,5-tetrasubstituted pyrazoles
发明人：DENG XIAOHU; MANI NEELAKANDHA S
权利人:DENG XIAOHU; MANI NEELAKANDHA S; JANSSEN PHARMACEUTICA NV
摘要:This invention concerns the synthesis of highly substituted pyrazoles, which are structural components of pharmacological compounds, through reaction of hydrazones with nitroolefins.

专利号:US-2009093637-A1
优先权日:2007-10-02
标题:Synthesis of 1,3,4-Trisubstituted and 1,3,4,5-Tetrasubstituted Pyrazoles

专利号:RU-2083580-C1
优先权日:1991-08-23
标题 :1,7-anular derivatives of 3-(piperazinoalkyl)-indole, method of their synthesis (variants), pharmaceutical composition containing thereof and an intermediate compound for their synthesis