CAS: 7378-99-6; N,N-Dimethyloctan-1-Amine

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N,N-二甲基辛酰胺置于三乙基硼,苯硅烷,Sodium Hydroxide体系中,用 四氢呋喃,甲基叔丁基醚 作为反应溶剂,化学反应 48.0H,以94%的收率获得产物n,N-二甲基正辛胺
参考文献:用于硅烷还原酰胺的bet 3基催化剂
标题:用于硅烷还原酰胺的bet 3基催化剂
摘要:本文报道了一种简单但实用的催化体系的开发,该体系用于用氢硅烷或氢硅氧烷选择性还原酰胺.发现低成本且易于获得的三乙基硼烷(在thf中为1.0 M)与催化量的碱金属碱结合,可催化所有三种酰胺类别(叔,仲和伯酰胺)的还原反应,从而在室温下形成胺.温和的条件.另外,还可以通过使用bet 3和碱的适当组合来实现将仲酰胺选择性转化为醛亚胺和将伯酰胺选择性转化为腈.这些赌注3的范围碱催化的酰胺氢化硅烷化反应已被深入研究.机理研究的初步结果表明,经过改进的piers硅烷si-h...b活化方式,其中bet 3提取氢化物的过程是通过烷氧基或氢氧根阴离子与si中心的配位来促进的.
DOI:10.1021/acs.Joc.9B00277

专利信息

专利号:US-6540970-B1
优先权日:1999-11-18
标题:Method for the synthesis of molecular sieves
发明人：STROHMAIER KARL G; VAUGHAN DAVID E W
权利人:EXXON MOBIL CHEM PATENTS INC
摘要:The present invention provides a method for the synthesis of MeAPO molecular sieves which includes the following steps: providing a source of alumina, a source of phosphorus, water, and a template suitable for forming a MeAPO molecular sieve; providing a source of metal (Me) including metal particles, the metal particles measuring, in their largest dimension, equal to or less than five nanometers; providing a water soluble organic solvent capable of solubilizing the source of metal; forming a synthesis mixture from the source of alumina, the source of phosphorus, the water, the template, the source of metal, and the solvent; and forming a MeAPO molecular sieve from the synthesis mixture.

专利号:EP-0443532-B1
优先权日:1990-02-20
标题:Temporary minimal protection synthesis of LH-RH analogs
发明人：NESTOR JOHN J JR; MCCLURE NATALIE L
权利人:SYNTEX INC
摘要:A solid phase synthesis of LH-RH analogs in which the amino acids serine and histidine, if present, are side chain protected during the synthesis with groups labile to selected alpha -amino or deprotecting agents.

专利号:US-2024383940-A1
优先权日:2021-03-31
标题 :Synthesis of trinucleotide and tetranucleotide caps for mrna production
发明人：ENDO ATSUSHI
权利人:MODERNA TX INC
摘要:Provided herein are methods of making trinucleotides and tetranucleotides for use as 5′ mRNA caps. The methods utilize a novel “top-downâ€? strategy and provide for synthesis of oligonucleotides with higher yields and increased efficiency compared to traditional methods. A key step of the methods disclosed, herein can also be adapted to utilize a “one-potâ€? approach, resulting in an increase in the yield of the final oligonucleotide product.

专利号:US-5212288-A
优先权日:1990-02-20
标 题:Temporary minimal protection synthesis of serine-containing polypeptides
发明人：NESTOR JR JOHN J; MCCLURE NATALIE L; ARZENO HUMBERTO
权利人:SYNTEX INC
摘要:In a process for the solid phase synthesis of a polypeptide containing at least one serine residue, the improvement comprising temporarily protecting the side chain of the serine residue with a protecting group which is removed immediately following the addition of the serine to the peptide chain.

专利号:US-5859237-A
优先权日:1995-04-28
标 题:Process for the production of phthalocyanine pigment
发明人：NOGUCHI HIDETO; HAYASHI MIKIO; MOMOSE MASATOSHI
权利人:TOYO INK MFG CO
摘要:A process for the production of a phthalocyanine pigment having a clear color tone, a high tinting strength and a finely milled structure by an efficient and economical process, in which the pigmentation from a phthalocyanine crude can be carried out without removing an aromatic hydrocarbon solvent used in the synthesis of the phthalocyanine crude, the process comprising thes steps of n (a) reacting phthalic anhydride or its derivative, urea or its derivative and a catalyst in an organic solvent to synthesize a phthalocyanine crude, n (b) wet-milling a slurry of the synthesized phthalocyanine crude in the presence of a milling medium without removing the aromatic hydrocarbon solvent, and n (c) removing the organic solvent from the slurry of the milled product, purifying the milled product and drying the milled product with a spray type dryer.

专利号:US-6175009-B1
优先权日:1999-11-18
标题:Process for the preparation of quinazolinones
发明人：CONFALONE PASQUALE NICHOLAS; MAGNUS NICHOLAS ANDREW; STORACE LOUIS
权利人:DU PONT PHARM CO
摘要:The present invention relates generally to an asymmetric synthesis of 4,4-disubstituted-3,4-dihydro-2(1H)-quinazolinones, and intermediates thereof. The target compounds are useful for the treatment of human immunodeficiency virus (HIV) as an inhibitor of reverse transcriptase.