CAS: 15951-41-4; Dichlorobis(Trimethylsilyl)Methane

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5926-35-2

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chloro-trimethyl-silane (dichloromethyl)trimethylsilane tetrachloromethane dichloromethane1,3-bis(4′-tolyl)-1,1,3,3-tetramethyldisiloxane 1-[(Chloro-bis-trimethylsilanyl-methyl)-dimethyl-silanyl]-4-methyl-benzene 1,1,3,3-tetramethyl-1,3-bis(4-chlorophenyl)disiloxane 1-Chloro-4-[(chloro-bis-trimethylsilanyl-methyl)-dimethyl-silanyl]-benzene

合成工艺路线路线简述

    📜三甲基氯硅烷,氯仿置于magnesium体系中,化学反应生成二氯双(三甲基硅基)甲烷
    参考文献:Silylation De Derives Gem-Polychlores
    标题:Silylation De Derives Gem-Polychlores
    摘要:
    Doi:10.1016/s0022-328X(00)95169-6

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    主要参考文献

    参考标题:Fluoride Ion-Catalyzed Generation And Carbonyl Addition Of α-Halo Carbanions Derived From α-Halo Organosilicon Compounds
    作者:Makoto Fujita,Michio Obayashi,Tamejiro Hiyama |发布日期:1988.1
    摘要:The Title Carbanion Species Are Generated From The Corresponding α-Haloorganosilicon Compounds By The Action Of A Catalytic Amount Of Tris(Diethylamino)Sulfonium Difluorotrimethylsilicate And Are Found To Undergo Addition To Aldehyde Carbonyl Efficiently At Ambient Temperature. The Synthetic Potential Of The Reaction Is Demonstrated By Application To The Synthesis Of Some Insecticides.

    合成参考文献


    参考文献:10.1007/978-3-540-45278-2_470
    摘要:Marsmann HC, Uhlig F. Silicon-29 NMR data of C7H18Cl2Si2. 2008. In: Chemical Shifts and Coupling Constants for Silicon-29. : Springer Berlin Heidelberg; 2008.
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