专利号:US-2002173644-A1 优先权日:1997-03-07 标题:Methods of making cross-bridged macropolycycles 发明人:HILER GEORGE DOUGLAS; PERKINS CHRISTOPHER MARK 摘要:Improved synthesis of a macropolycycle, more particularly, of a cross-bridged tetraazamacrocycle.
专利号:US-2002184969-A1 优先权日:2001-03-29 标 题 :Combinatorial synthesis of particulate materials 发明人:KODAS TOIVO T; HAMPDEN-SMITH MARK J 摘要:Methods for fabricating and analyzing particulates having a varying material property such that particulates having a selected desirable material property can be identified. The particulates can be analyzed to determine the particulates having the best properties for a particular application. The particulates can be metals, inorganic compounds, organic compounds and composites. The method of the present invention enables the rapid and economical fabrication and screening of a large number of different compositions.
专利号:US-2024425890-A1 优先权日:2022-02-11 标 题:Process for the synthesis of alpha-methylene-gamma-butyrolactone 发明人:TADEN ANDREAS; BECK HORST; MYRTOLLARI KAMELA; KOURIST ROBERT; NIGL ANDREA 权利人:HENKEL AG & CO KGAA 摘要:The present application provides a process for the preparation of α-methylene-γ-butyrolactone, said process comprising the steps of:a) acetylating the C1-hydroxyl group of isoprenol to yield isoprenyl acetate;b) forming 4-acetoxy-2-methylene-butan-1-ol from said isoprenyl acetate by whole cell biotransformation, said step comprising:i) contacting a cell (CB) with a culture medium containing said isoprenyl acetate or with a culture medium contiguous with an organic phase containing said isoprenyl acetate under conditions that enable the cell to form 4-acetoxy-2-methylene-butan-1-ol from isoprenyl acetate; and,ii) optionally isolating the resultant 4-acetoxy-2-methylene-butan-1-ol, wherein said cell (CB) exhibits activity of at least one alkane monooxygenase enzyme which catalyzes the formation of 4-acetoxy-2-methylene-butan-1-ol from isoprenyl acetate;c) oxidizing said 4-acetoxy-2-methylene-butan-1-ol to yield 4-acetoxy-2-methylene butyric acid; and,d) converting said 4-acetoxy-2-methylene butyric acid to α-methylene-γ-butyrolactone by hydroxylysis to γ-hydroxy-α-methylenebutyric acid and subsequent cyclization of said γ-hydroxy-α-methylenebutyric acid.
专利号:US-6444808-B2 优先权日:1997-03-07 标 题 :Methods of making cross-bridged macropolycycles 发明人:HILER II GEORGE DOUGLAS; PERKINS CHRISTOPHER MARK 权利人:PROCTER & GAMBLE 摘要:Improved synthesis of a macropolycycle, more particularly, of a cross-bridged tetraazamacrocycle.
专利号:WO-2024201469-A1 优先权日:2023-03-29 标 题:Process for the preparation of amine intermediates 发明人:YACOVAN AVIHAI; BAR NAHUM ITSIK; KRAKOVICH VLADA; PARNES REGEV; WANG HONGFA; ZHANG QINGLONG; Zi Weiwei 权利人:ADAMA AGAN LTD 摘要:The present disclosure relates a process for the preparation of amines as intermediates for the synthesis of triazines, which are suitable for use as herbicides for controlling weeds.
专利号:US-6689919-B1 优先权日:1999-09-22 标 题 :Catalysts for oxidative polymerization of fluorophenol, method of oxidative polymerization of fluorophenol, and poly(oxyfluorophenylene) derivative 发明人:TSUCHIDA EISHUN; OYAIZU KENICHI; KUMAKI YOSUKE; SAITO KEI 权利人:JAPAN SCIENCE & TECH CORP 摘要:The synthesis of fluoropolyarylene ether with a high degree of polymerization is enabled, by using a copper complex catalyst with an oxidation potential in the range of -1V to 2V, for the oxidative polymerization of fluorophenols that contain at least one hydrogen atom as well as a fluorine atom bonded to the carbon atoms constituting the benzene ring.