CAS: 107-71-1; Tert-Butyl Ethaneperoxoate

上下游产品

tert.-butylhydroperoxide Ketene acetic anhydride acetyl chloride3-acetoxy-1-hexene °Ct-1-en-3-yl acetate rac-3-acetoxycyclohexene 2-acetoxy-4-benzoyl-1-oxa-4-azacyclohexane

📜叔丁基过氧化氢,Trifluoroacetic Anhydride置于吡啶体系中,用 甲苯 用作溶剂,化学反应 0.75H,反应生成过氧化乙酸叔丁酯
参考文献:New Synthesis Of Tert-Butyl Peroxycarboxylates
标题:New Synthesis Of Tert-Butyl Peroxycarboxylates
摘要:Tert-Butyl Peroxyacetate,Tert-Butyl Peroxybutyrate,Tert-Butyl Phenylperoxyacetate,And Tert-Butyl Peroxyundecanoate Were Obtained In Nearly Quantitative Yields By The Esterification Of The Corresponding Carboxylic Acids With Tert-Butyl Hydroperoxide In The Presence Of Trifluoroacetic Anhydride And Pyridine In Nonaqueous Medium At 0-5 Degrees C. No Terl-Butyl Peroxytrifluoroacetate Was Formed As A By-Product During The Process. A Possible Reaction Mechanism Is Discussed.
Doi:10.1134/s1070428006040026

专利信息

专利号:WO-2023102600-A1
优先权日:2021-12-06
标题:Synthesis of amphiphilic block copolymers and polymeric nanofibers produced therefrom
发明人：ZETTERLUND PER B; ISHIZUKA FUMI; KIM HYUN JIN; CHATANI SHUNSUKE; NIINO HIROSHI
权利人:NEWSOUTH INNOVATIONS PTY LTD
摘要:The present disclosure relates to the field of synthesis of block copolymers, and polymeric nanofibers having a core-shell morphology produced therefrom. The present disclosure relates to the field of synthesis of block copolymers where one block is more hydrophobic than the other block and is a different composition. The disclosure also relates to uses of these polymeric nanofibers in various applications, such as reinforcing a polymeric matrix and for coatings applications.

专利号:US-6512081-B1
优先权日:1997-07-21
标题:Synthesis of dithioester chain transfer agents and use of bis(thioacyl) disulfides or dithioesters as chain transfer agents
发明人：RIZZARDO ENZIO; THANG SAN HOA; MOAD GRAEME
权利人:E I DUPONT NEMOURS AND COMPANY; COMMW SCIENT IND RES ORG
摘要:This invention relates to the synthesis of dithiocarboxylic acid esters by reaction of bis(thioacyl) disulphides, thioacetals or vinylidane bis(thioether) with free-radicals (optionally in the presence of monomers). The invention also relates to processes for the synthesis of polymers utilising these dithioesters as polymerisation regulators (chain transfer agents) or to the use of bis(thioacyl) disulphides to generate dithioester chain transfer agents in situ.

专利号:US-8871975-B2
优先权日:2011-01-05
标题 :Process for the synthesis of agomelatine
发明人：ZARD SAMIR; SIRE BÉATRICE; BOUMEDIENE MEHDI
权利人:ZARD SAMIR; SIRE BÉATRICE; BOUMEDIENE MEHDI; SERVIER LAB
摘要:Process for the industrial synthesis of the compound of formula (I)

专利号:US-5788950-A
优先权日:1994-08-03
标 题 :Method for the synthesis of mixed metal oxide powders
发明人：IMAMURA KUNIO; DIGREGORIO JOHN F; SMITH DOUGLAS M; IZAWA HIROZUMI; YAMAGUCHI TETSUHIKO
权利人:SHOWA DENKO KK
摘要:A technique to synthesize complex oxide ceramic powders which offers advantages of both the coprecipitation and sol-gel routes while doing away with the disadvantages is disclosed. Namely, the ability to achieve chemical homogeneity and crystallite size on the namometer length scale at a nonprohibitive cost is provided by the disclosed method. In one embodiment of the invention, a method for the synthesis of a mixed metal oxide powder is provided including (a) combining a liquid absorbent resin with at least one solution selected from the group consisting of solutions containing at least one organo-metallic compound and solutions containing at least one metallic salt compound, such that at least two metals are present in the liquid absorbent resin after the combining is completed; (b) after the combining, allowing the liquid absorbent resin to swell and gel and thereby form a swollen gel; (c) preparing a precursor material by changing at least one of the pH and temperature of the swollen gel; (d) pyrolyzing the precursor material to form a pyrolyzed precursor material; and (e) calcining the pyrolyzed precursor material to form a mixed metal oxide powder.

专利号:US-3888936-A
优先权日:1972-03-09
标题:Removal of free radical inhibitors to promote synthesis of alpha, omega-dichloroalkane telomers from ethylene and sulfuryl chloride
发明人：HUDSON JR JOSEPH A
权利人:CONTINENTAL OIL CO
摘要:In the synthesis of alpha,omega-dichloroalkanes such as 1,2dichlorobutane and 1,6-dichlorohexane from ethylene and sulfuryl chloride, yield is improved when the reaction environment is scrupulously rendered and maintained free from Lewis acids and other free radical inhibiting materials.

专利号:US-RE46218-E
优先权日:2011-01-05
标 题 :Process for the synthesis of agomelatine
发明人：ZARD SAMIR; SIRE BÉATRICE; BOUMEDIENE MEHDI
权利人:SERVIER LAB
摘要:Process for the industrial synthesis of the compound of formula (I)