CAS: 256652-04-7; 4,4,5,5-Tetramethyl-2-(Naphthalen-2-yl)-1,3,2-Dioxaborolane
- 英文名称4,4,5,5-Tetramethyl-2-(Naphthalen-2-yl)-1,3,2-Dioxaborolane
- 中文名称2-萘硼酸频哪醇酯
- IUPAC名称4,4,5,5-tetramethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborolane
- 其它别名2-萘硼酸频哪醇酯; 4,4,5,5-四甲基-2-(2-萘基)-1,3,2-二氧环戊硼烷; Naphthalene-2-Boronic Acid Pinacol Ester
- CAS编号256652-04-7
- MFCD编号:MFCD05663868
- EINECS号:805-570-1
- 分子式:C16H19BO2
- 分子量:254.14
- 产品CID: 1219724
- 产品分类有机原料→分子砌块→芳环类化合物→萘类化合物
相似化合物
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MSDS等安全信息
欧盟法规
ECHA物质C&L通报上下游产品
CAS号612-55-5 2-碘萘 | CAS号25015-63-8 频那醇硼烷 | CAS号580-13-2 2-溴萘 | CAS号61676-62-8 2-异丙氧基-4,4,5,5-... | CAS号3857-83-8 三氟甲烷磺酸2-萘酯 | CAS号91-58-7 β-氯萘 | CAS号73183-34-3 双戊酰二硼 | CAS号25240-59-9 4,4,5,5-四甲基-1,3... | CAS号613-46-7 2-萘甲腈 | CAS号76-09-5 频哪醇 | CAS号580-13-2 2-溴萘 | CAS号2459-25-8 2-萘甲酸甲酯 | CAS号612-78-2 2,2'-联萘酚 | CAS号613-46-7 2-萘甲腈 | CAS号1006714-36-8 2-(2-butenyl)na... | CAS号2489-89-6 4-(2-NAPHTHYL)-...合成工艺路线路线简述
- 76-09-5 = 256652-04-7 + 849543-98-2 + 853377-10-3
反应条件:1.1 Reagents: Boron Triiodide Solvents: 1,2,4-Trichlorobenzene; Rt; 16 H,240 °C; 240 °C -> Rt1.2 Reagents: Triethylamine; 0.5 H,Rt
标题:Multiple Electrophilic C-H Borylation Of Arenes Using Boron Triiodide
作者:Oda,Susumu; Et Al
参考文献:Organic Letters 日期:2020 卷标:22(2) 页码:700-704]
73183-34-3 = 256652-04-7 + 849543-98-2 + 853377-10-3
反应条件:1.1 Catalysts: Bis[(1,2,5,6-η)-1,5-Cyclooctadiene]Di-μ-Methoxydiiridium,4,4′-Bis(1,1-Dimethylethyl)-2,2′-Bipyridine Solvents: Cyclohexane; 16 H,80 °C
标题:Selective Ir-Catalysed Borylation Of Polycyclic Aromatic Hydrocarbons: Structures Of Naphthalene-2,6-Bis(Boronate),Pyrene-2,7-Bis(Boronate) And Perylene-2,5,8,11-Tetra(Boronate) Esters
作者:Coventry,David N.; Et Al
参考文献:Chemical Communications (Cambridge 日期:2005 卷标:(16) 页码:2172-2174
2-萘甲酸置于4-二甲氨基吡啶,氯化亚砜,三丁基膦,Ni(Cod)2,Lithium Carbonate,三乙胺体系中,用 1,4-二氧六环,二氯甲烷,甲苯 用作溶剂,化学反应 38.0H,反应生成2-萘硼酸频哪醇酯
参考文献:Nickel-Catalyzed Decarbonylative Silylation,Borylation,And Amination Of Arylamides Via A Deamidative Reaction Pathway
标题:Nickel-Catalyzed Decarbonylative Silylation,Borylation,And Amination Of Arylamides Via A Deamidative Reaction Pathway
摘要:已开发出一种镍催化的酰胺脱羰基硅化,硼化和胺化反应.这种新方法允许直接将酰胺转化为芳基硅烷,芳基硼酸酯和芳基胺,并以简单和温和的方式实现碳-杂原子键的形成.
Doi:10.1055/s-0036-1591495
海关参考信息
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2902902000-精萘
2905122000-异丙醇
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专利信息
专利号:US-9074050-B2
优先权日:2011-05-30
标 题 :Process for the production of polymers by using coupling reactions
发明人：KLEINER MATTHIAS; ELBS MARTIN; KASTLER MARCEL
权利人:KLEINER MATTHIAS; ELBS MARTIN; KASTLER MARCEL; BASF SE
摘要:The present invention relates to a continuous process for the production of polymeric coupling products by using a reactor assembly which is equipped with two or more reaction cells. The educt fluid is pumped through the reaction cells and thoroughly mixed therein by means of agitators. Preferably the process according to the invention is used for the preparation of coupling products which show at least partially precipitation and/or gelation effects during the performance of the synthesis. The precipitation and/or gelation effects are associated with and increase of the viscosity of the reaction system under reaction conditions. The products which are obtained by the process according to the invention have increased molecular weight and low polydispersity over similar products which were obtained in batch experiments.
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合成参考文献
摘要:Xu, L., Science of Synthesis: Advances in Organoboron Chemistry towards Organic Synthesis, (2019) 1, 295.
摘要:Xu, L., Science of Synthesis: Advances in Organoboron Chemistry towards Organic Synthesis, (2019) 1, 273.
摘要:Xu, L., Science of Synthesis: Advances in Organoboron Chemistry towards Organic Synthesis, (2019) 1, 298.
摘要:Chowdhury, S., Science of Synthesis: Knowledge Updates, (2024) 1, 252.
摘要:Zeng, X., Science of Synthesis: Base-Metal Catalysis, (2023) 2, 752.
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