CAS: 362049-56-7; Carbaryl-D7

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1-naphthol-d7 methyl is°Cyanate α-naphthol

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    📜萘酚置于platinum On Activated Charcoal 氢气,重水体系中,化学反应 34.0H,反应生成甲萘威-D7
    参考文献:Aromatic Ring Favorable And Efficient H-d Exchange Reaction Catalyzed By Pt/c
    标题:Aromatic Ring Favorable And Efficient H-d Exchange Reaction Catalyzed By Pt/c
    摘要:An Effective And Applicable Pt/c-Catalyzed Deuteration Method Of Aromatic Rings Using D2O As A Deuterium Source Under Hydrogen Atmosphere Was Developed. Five Percent Pt/c Would Lead To Quite Effective H-D Exchange Results On The Aromatic Ring Systems. The Reaction Is General For A Variety Of Aromatic Compounds Including Biologically Active Compounds. (C) 2005 Elsevier Ltd. All Rights Reserved.
    Doi:10.1016/j.Tetlet.2005.08.067

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    主要参考文献

    参考标题:Efficient And Selective Pt/c-Catalyzed H-D Exchange Reaction Of Aromatic Rings
    作者:Nobuhiro Ito,Hiroyoshi Esaki,Tsuneaki Maesawa,Eikoh Imamiya,Tomohiro Maegawa,Hironao Sajiki |发布日期:2008.2.15
    摘要:An Effective And Applicable Deuteration Method For Aromatic Rings Using Pt/c-D2O-H2 System Was Established. Especially, Phenol Was Fully Deuterated Even At Room Temperature, And Other Electron-Rich Aromatic Nuclei Were Efficiently Deuterated Under Mild Conditions. The Scope And Limitations Of The Presence Method And Its Application To The Synthesis Of Deuterium-Labeled Biologically Active Compounds And Deuterium-Labeled Building Blocks For Practical Multi-Gram Scale Syntheses Are Reported.

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    合成方法参考DOI号:10.1016/j.tetlet.2005.08.067
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