📜1,2,3,5,6,7-Hexaacetoxy-Anthraquinone置于水,Sodium Hydroxide体系中,用 乙醇 作为反应溶剂,化学反应 2.0H,反应生成 六羟基蒽醌
参考文献:Microwave-Assisted Synthesis Of Novel Oligomeric Rod-Disc Hybrids
标题:Microwave-Assisted Synthesis Of Novel Oligomeric Rod-Disc Hybrids
摘要:Microwave-Assisted Syntheses Of Five New Oligomeric Liquid Crystals (Lc) Are Reported For The First Time Consisting Of Rufigallol-Based Core Attached To Which 8-Cyanobiphenyl Units Via Flexible Alkyl Spacers. The Synthesis Of The Target Compounds Was Challenging Since Classical Reactions Failed To Produce These Hybrids. Chemical Structures Of These Hybrids Were Determined By H-1 NMR,C-13 NMR,Ir,Uv Spectroscopy And Elemental Analysis. The Thermotropic Liquid Crystalline Properties Of These New Compounds Were Investigated By Polarizing Optical Microscopy (Pom),Differential Scanning Calorimetry (Dsc) And X-Ray Diffractometry (Xrd). (C) 2012 Elsevier Ltd. All Rights Reserved.
DOI:10.1016/j.Tetlet.2012.09.058