专利号:US-11649213-B2 优先权日:2018-09-26 标题 :Synthetic method for the preparation of a 3-[5-amino-4-(3-cyanobenzoyl)-pyrazol compound 发明人:MEISENBACH MARK; MARTIN BENJAMIN; RONDE NIEK JOHANNES; RUIZ CARMEN 权利人:MEREO BIOPHARMA 1 LTD 摘要:Provided is a process for preparing a compound, comprising the steps of a) Reacting a compound of Formula A (Formula A) with the compound 3 (3) to provide the compound 5 (5) or a salt or solvate thereof, wherein R is a linear or branched C1-C5 alkyl. Further provided is the compound 5 or a salt or solvate thereof. (5) The use of these compounds in the synthesis of 3-[5-Amino-4-(3-Cyanobenzoyl)-Pyrazol-1-yl]-N-Cyclopropyl-4-Methylbenzamide is also provided.
专利号:US-11400438-B2 优先权日:2018-12-05 标 题 :Synthesis and immobilization of a ferrous sulfite catalyst and method of degrading fluorinated organic chemicals in aqueous media 发明人:DIONYSIOU DIONYSIOS D; ABDELRAHEEM WAEL H M; NADAGOUDA MALLIKARJUNA N 权利人:UNIV CINCINNATI; THE US ADMINISTRATOR OF THE U S ENVIRONMENTAL PROTECTION AGENCY 摘要:A composition includes an aqueous solution including at least one fluorinated organic compound; and a reaction product of a source of iron(II) and a source of sulfite in the presence of water and molecular hydrogen. A method of making a catalyst includes reacting a source of iron(II) and a source of sulfite in the presence of water and molecular hydrogen. The water may include less than or equal to 1 weight percent dissolved molecular oxygen. The catalyst may be used for degrading fluorinated organic chemicals in aqueous media.
专利号:WO-2011138356-A1 优先权日:2010-05-07 标 题 :Process for preparing synthesis gas and at least one organic, liquid or liquefiable value product 发明人:PROCHAZKA ROMAN; BITTERLICH STEFAN; MACHHAMMER OTTO; DEUERLEIN STEPHAN; KLINGLER DIRK; PANTOUFLAS EMMANOUIL; KINDLER ALOIS; ZOELS BERND 权利人:BASF SE; PROCHAZKA ROMAN; BITTERLICH STEFAN; MACHHAMMER OTTO; DEUERLEIN STEPHAN; KLINGLER DIRK; PANTOUFLAS EMMANOUIL; KINDLER ALOIS; ZOELS BERND 摘要:The present invention relates to a process for preparing synthesis gas and at least one organic, liquid or liquefiable value product, by a) providing a biomass starting material, b) subjecting the biomass starting material to digestion, c) optionally, from the digested material obtained in step b), isolating at least one fraction C1) with a heightened aromatics content and at least one fraction C2) with a lowered aromatics content, d) feeding the digestion product from step b) or the high-aromatics fraction C1) from step c) into a dealkylating zone and reacting it in the presence of hydrogen and/or steam, e) taking a discharge from the dealkylating zone and subjecting it to separation, to produce at least one organic, liquid or liquefiable value product and at least one stream with a heightened content of volatile components lighter than the organic value product, and f) using the stream obtained in step e), with a heightened content of volatile components lighter than the organic value product, at least partially for preparing synthesis gas.
专利号:US-2011275869-A1 优先权日:2010-05-07 标题:Process for producing synthesis gas and at least one organic liquid or liquefiable material of value 发明人:PROCHAZKA ROMAN; BITTERLICH STEFAN; MACHHAMMER OTTO; DEUERLEIN STEPHAN; KLINGLER DIRK; PANTOUFLAS EMMANOUIL; KINDLER ALOIS; ZOELS BERND 权利人:BASF SE 摘要:The present invention relates to a process for producing synthesis gas and at least one organic liquid or liquefiable material of value, whereinn a) a biomass starting material is provided, b) the biomass starting material is subjected to a decomposition, c) at least one aromatics-enriched fraction C1) and at least one aromatics-depleted fraction C2) are optionally isolated from the decomposed material obtained in step b), d) the decomposition product from step b) or the aromatics-enriched fraction C1) from step c) is fed into a dealkylation zone and reacted in the presence of hydrogen and/or water vapor, e) a discharge is taken from the dealkylation zone and subjected to a separation to give at least one organic liquid or liquefiable material of value and at least one stream enriched in components which are more volatile than the organic material of value, f) the stream enriched in components which are more volatile than the organic material of value which is obtained in step e) is at least partly used for producing synthesis gas.
专利号:US-5288882-A 优先权日:1992-12-21 标题:Process for recovering an optically active epoxy alcohol 发明人:SHIH T THOMAS; SHUM WILFRED P-S 权利人:ARCO CHEM TECH 摘要:A method of recovering optically active epoxy alcohols from asymmetric epoxidation reaction mixture is provided whereby the epoxy alcohol may be obtained in high yield with minimal degradation of optical purity. The process is also suitable for the synthesis of useful organic sulfonate derivatives of chiral epoxy alcohols.
专利号:US-2016052903-A1 优先权日:2013-04-29 标题:5-(hydroxymethyl) furan-2-carbaldehyde (hmf) sulfonates and process for synthesis thereof 发明人:STENSRUD KENNETH 权利人:ARCHER DANIELS MIDLAND CO 摘要:5-(hydroxymethyl)furan-2-carbaldehyde (HMF)-sulfonates and a method of preparing the same are described. The method involves reacting a mixture of 5-(hydroxymethyl)furfural (HMF), with at least one of a) a trifluoromethanesulfonate anhydride (triflate), b) a p-toluene-sulfonyl halide (tosylate), and c) methane-sulfonyl halide (mesylate), and a reagent of either 1) a nucleophilic base or 2) a combination of a non-nucleophilic base and a nucleophile. The HMF-sulfonates (e.g., triflate, tosylate, mesylate, etc. analogs of HMF) can serve as precursor materials from which various derivative compounds can be synthesized.
摘要:Merck Index - O'Neil MJ, Heckelman PE, Dobbelaar PH, Roman KJ (eds). The Merck Index, An Encyclopedia of Chemicals, Drugs, and Biologicals, 15th Ed. Cambridge, UK: The Royal Society of Chemistry, 2013.