参考标题:Pentafluoronitrosulfane, Sf5No2 作者:Norman Lu,Joseph S. Thrasher,Stefan Von Ahsen,Helge Willner,Drahomir Hnyk,Heinz Oberhammer |发布日期:2006.2.1 摘要:The Synthesis Of Pentafluoronitrosulfane, Sf5No2, Is Accomplished Either By Reacting N(Sf5)3 With No2 Or By The Photolysis Of A Sf5Br/no2 Mixture Using Diazo Lamps. The Product Is Purified By Treatment With Csf And Repeated Trap-To-Trap Condensation. The Solid Compound Melts At -78 Degrees C, And The Extrapolated Boiling Point Is 9 Degrees C. Sf5No2 Is Characterized By 19F, 15N Nmr, Ir, Raman, And
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