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CAS号1153-85-1 3-溴-N-苯基咔唑 | CAS号121-43-7 硼酸三甲酯 | CAS号5419-55-6 硼酸三异丙酯 | CAS号502161-03-7 3-碘-9-苯基咔唑 | CAS号1150-62-5 N-苯基咔唑 | CAS号591-50-4 碘苯 | CAS号86-74-8 咔唑 | CAS号108-86-1 溴苯 | CAS号7647-01-0 盐酸 | CAS号1028647-93-9 3-(4-溴苯基)-9-苯基咔唑合成工艺路线路线简述
- 合成目标产物 9-Phenyl-9H-Carbazol-3-Ylboronic Acid 主要起始原料 3-Bromo-9-Phenyl-9H-Carbazole And Trimethyl Borate And Water
- 1153-85-1 = 854952-58-2
反应条件:1.1 Reagents: Butyllithium Solvents: Tetrahydrofuran; -78 °C; 1 H,-78 °C1.2 -78 °C; 2 H,-78 °C; -78 °C -> Rt; Overnight,Rt; Rt -> 0 °C1.3 Reagents: Hydrochloric Acid Solvents: Water; 3 H,0 °C; 3 H,Rt
标题:Synthesis And Optoelectronic Properties Of A Novel Phosphorescence Host Material Containing Carbazole Moiety
作者:Peng,Hua-Nan; Et Al
参考文献:Hecheng Huaxue 日期:2013 卷标:21(1) 页码:58-61]
591-50-4 = 854952-58-2
反应条件:1.1 Reagents: 1,10-Phenanthroline,Potassium Carbonate,Cuprous Iodide Solvents: P-Xylene; 100 °C1.2 Reagents: N-Bromosuccinimide Solvents: Dimethylformamide; 0 °C1.3 Reagents: Butyllithium Solvents: Tetrahydrofuran; -78 °C1.4 Reagents: Triisopropyl Borate,Hydrochloric Acid Solvents: Water; Rt
标题:Synthesis Of Novel Star-Shaped Carbazole-Functionalized Triazatruxenes
作者:Feng,Guo-Liang; Et Al
参考文献:Tetrahedron Letters 日期:2006 卷标:47(39) 页码:7089-7092]
1150-62-5 = 854952-58-2
反应条件:1.1 Reagents: N-Bromosuccinimide Solvents: Chloroform2.1 Reagents: Butyllithium,Trimethyl Borate Solvents: Tetrahydrofuran; -78 °C
标题:Water-Soluble Iridium(Iii) Complexes As Multicolor Probes For One-Photon,Two-Photon And Fluorescence Lifetime Imaging
作者:Ma,Yun; Et Al
参考文献:Journal Of Organometallic Chemistry 日期:2023 卷标:992]
591-50-4 = 854952-58-2
反应条件:1.1 Reagents: Potassium Hydroxide Catalysts: 1,10-Phenanthroline,Cuprous Iodide Solvents: Xylene; 130 °C2.1 Reagents: N-Bromosuccinimide Solvents: Chloroform3.1 Reagents: Butyllithium,Trimethyl Borate Solvents: Tetrahydrofuran; -78 °C
标题:Water-Soluble Iridium(Iii) Complexes As Multicolor Probes For One-Photon,Two-Photon And Fluorescence Lifetime Imaging
作者:Ma,Yun; Et Al
参考文献:Journal Of Organometallic Chemistry 日期:2023 卷标:992]
591-50-4 = 854952-58-2
反应条件:1.1 Reagents: Sodium Hydroxide Catalysts: 1,10-Phenanthroline,Cuprous Iodide Solvents: Xylene; 48 H,140 °C2.1 Reagents: N-Bromosuccinimide Solvents: Chloroform; Rt3.1 Reagents: Butyllithium; -78 °C3.2 Reagents: Trimethyl Borate; -78 °C3.3 Reagents: Hydrochloric Acid Solvents: Water
标题:Color-Tunable Thiazole-Based Iridium(Iii) Complexes: Synthesis,Characterization And Their Oled Applications
作者:Chau,Nga-Yuen; Et Al
参考文献:Journal Of Organometallic Chemistry 日期:2017 卷标:829 页码:92-100]
1592-95-6 + 591-50-4 = 854952-58-2
反应条件:1.1 -2.1 Reagents: Butyllithium,Trimethyl Borate2.2 Reagents: Hydrochloric Acid Solvents: Water
标题:Bipolar Host Materials Comprising Carbazole,Pyridine And Triazole Moieties For Efficient And Stable Phosphorescent Oleds
作者:Zhang,Ting; Et Al
参考文献:Dyes And Pigments 日期:2021 卷标:192]
= 854952-58-2
反应条件:1.1 Catalysts: 1,10-Phenanthroline,Potassium Hydroxide,Cuprous Iodide Solvents: Xylene; 140 °C2.1 Reagents: N-Bromosuccinimide Solvents: Dichloromethane3.1 Reagents: Butyllithium Solvents: Tetrahydrofuran3.2 Reagents: Trimethyl Borate3.3 Reagents: Hydrochloric Acid
标题:Synthesis,Characterization,Photophysics And Electrophosphorescent Applications Of Phosphorescent Platinum Cyclometalated Complexes With 9-Arylcarbazole Moieties
作者:Ho,Cheuk-Lam; Et Al
参考文献:Journal Of Organometallic Chemistry 日期:2009 卷标:694(17) 页码:2735-2749]
= 854952-58-2
反应条件:1.1 Reagents: N-Bromosuccinimide Solvents: Dimethylformamide2.1 -3.1 Reagents: Butyllithium,Trimethyl Borate3.2 Reagents: Hydrochloric Acid Solvents: Water
标题:Bipolar Host Materials Comprising Carbazole,Pyridine And Triazole Moieties For Efficient And Stable Phosphorescent Oleds
作者:Zhang,Ting; Et Al
参考文献:Dyes And Pigments 日期:2021 卷标:192
硼酸三甲酯置于正丁基锂,盐酸体系中,用 四氢呋喃,正己烷,水 作为反应溶剂,化学反应 28.0H,以58%的收率获得产物n-苯基-3-咔唑硼酸
参考文献:Wo2007/125934
标题:Wo2007/125934
专利信息
专利号:US-8729310-B2
优先权日:2009-09-22
标题:Halogenated diarylamine compound and synthesis method thereof
发明人:OSAKA HARUE; INOUE HIROTO
权利人:OSAKA HARUE; INOUE HIROTO; SEMICONDUCTOR ENERGY LAB
摘要:An object is to provide a new halogenated diarylamine compound serving as a source material for synthesis of a variety of diarylamine compounds and triarylamine compounds and a synthesis method of the new halogenated diarylamine compound. A halogenated diarylamine compound represented by the following general formula (G1) and a synthesis method thereof are provided. Note that a variety of diarylamine compounds and triarylamine compounds can be synthesized using the halogenated diarylamine compound represented by the following general formula (G1).
专利号:US-8283855-B2
优先权日:2010-01-11
标 题 :Method for synthesis of anthracene derivative
发明人:OSAKA HARUE
权利人:OSAKA HARUE; SEMICONDUCTOR ENERGY LAB
摘要:A method for synthesizing an anthracene derivative represented by a general formula (G1) is provided, in which a 9-arylanthracene derivative having an active site at a 10-position is subjected to coupling with a carbazole-3-yl-aryl derivative having an active site in an aryl group with the use of a metal or a metal compound, wherein A represents a substituted or unsubstituted phenyl group, wherein D represents any of an alkyl group having 1 to 4 carbon atoms and a substituted or unsubstituted phenyl group, wherein α represents any of a substituted or unsubstituted phenylene group and a substituted or unsubstituted biphenyl-4,4′-diyl group, and wherein R1 to R9 independently represent any of hydrogen, an alkyl group having 1 to 4 carbon atoms, and a substituted or unsubstituted phenyl group.
专利号:US-11767302-B2
优先权日:2020-10-01
标题 :Reagents and methods for tetrazine synthesis
发明人:FOX JOSEPH M; LAMBERT WILLIAM; FANG YINZHI; AM ENDE CHRISTOPHER WILLIAM; MAHAPATRA SUBHAM; XIE YIXIN; WANG CHUANQI
权利人:UNIV DELAWARE
摘要:Disclosed herein are mono- and di-substituted tetrazines and methods of their preparation and converting an oxetanyl ester to a thio-substituted tetrazine, which is then converted to a mono-substituted tetrazine, a di-substituted tetrazine, or a vinylether disubstituted tetrazine.
专利号:US-2011172441-A1
优先权日:2010-01-11
标题 :Method for synthesis of anthracene derivative
专利号:US-9718764-B2
优先权日:2013-03-22
标题:Synthetic building blocks for the production of materials for organic electroluminescence devices
发明人:STOESSEL PHILIPP; PARHAM AMIR HOSSAIN; JATSCH ANJA
权利人:MERCK PATENT GMBH
摘要:The present invention relates to compounds which are suitable as synthesis precursors for the production of electronically active materials for use in organic electroluminescence devices.
专利号:US-2025042877-A1
优先权日:2021-11-30
标题:Organic compound, organic device, light-emitting apparatus, and electronic appliance
发明人:HAYASHI YUKI; KAWAKAMI SACHIKO; HASHIMOTO NAOAKI
权利人:SEMICONDUCTOR ENERGY LAB
摘要:A novel compound, a synthesis method thereof, and an organic device including the novel compound are provided. A compound represented by General Formula (G1) is provided. In General Formula (G1), each of R1, R2, and R5 to R7 independently represents any of hydrogen (including deuterium), an alkyl group having 1 to 10 carbon atoms, a substituted or unsubstituted aryl group having 1 to 60 carbon atoms, and a substituted or unsubstituted heteroaryl group having 1 to 60 carbon atoms. R3 represents a condensed ring composed of 4 to 10 rings containing nitrogen as an element forming the ring, and R4 represents any of a substituted or unsubstituted condensed ring having 1 to 60 carbon atoms, a substituted or unsubstituted aryl group with a molecular weight of 78 or more, and a substituted or unsubstituted heteroaryl group with a molecular weight of 80 or more. At least one of A1 to A3 represents nitrogen, and each of the others represents substituted carbon. Each of substituents of A1 to A3 independently represents any of hydrogen (including deuterium), an alkyl group having 1 to 10 carbon atoms, a substituted or unsubstituted aryl group having 1 to 60 carbon atoms, and a substituted or unsubstituted heteroaryl group having 1 to 60 carbon atoms.