CAS: 474-70-4; (10R)-3C-Hydroxy-10R.13C-Dimethyl-17C-((1R:4R)-1.4.5-Trimethyl-Hexen-(2T)-yl)-(9Ch.14Th)-δ5.7-Dodecahydro-1H-Cyclopenta[a]Phenanthren

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    维生素d2 Calciferol 50-14-6
    Vitamin D2 50-14-6

    合成工艺路线路线简述

      📜(10R)-3C-Hydroxy-10R.13C-Dimethyl-17C-((1R:4R)-1.4.5-Trimethyl-Hexen-(2T)-yl)-(9Ch.14Th)-δ6-Dodecahydro-4H-5T.8T-Cyclo-Cyclopenta[a]Phenanthren 反应生成 (3Beta,9Beta,22E)-麦角甾-5,7,22-三烯-3-醇
      参考文献:Dimroth,Chemische Berichte,1937,Vol. 70,P. 1631,1635
      标题:Dimroth,Chemische Berichte,1937,Vol. 70,P. 1631,1635

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      参考文献:10.3891/acta.chem.scand.16-0541
      摘要:Alertsen AR, Brunn T, Hemmer E, Sim GA, Theander O, Flood H. The Occurrence of Ergosterol in the Lichen Cornicularia normoerica (Gunnerus) Lynge. Acta Chem. Scand. 1962;16():541–2. doi: 10.3891/acta.chem.scand.16-0541.
      参考文献:10.1007/bf02153672
      摘要:Owades JL. Mechanism of the photocondensation of steroids. Cellular and Molecular Life Sciences. 1950 Jul;6(7):258–61. doi: 10.1007/bf02153672.
      参考文献:10.1007/s10973-023-12017-3
      摘要:Jelić D, Đermanović M, Marković A, Manić N, Veličković S, Veljković F, Janković B. Novel insight in thermo-oxidative kinetics of vitamin D-based supplement formulation using TG–DTG–DTA, ATR-FTIR and MALDI-MS techniques. J Therm Anal Calorim. 2023 Mar 06;148(10):4281–305. doi: 10.1007/s10973-023-12017-3.
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