CAS: 77001-50-4; 16-Nitro-2,3,5,6,8,9,11,12-Octahydrobenzo[b][1,4,7,10,13]Pentaoxacyclopentadecin-15-Amine
- 英文名称16-Nitro-2,3,5,6,8,9,11,12-Octahydrobenzo[b][1,4,7,10,13]Pentaoxacyclopentadecin-15-Amine
- 中文名称4-氨基-5-硝基苯并-15-冠-5
- IUPAC名称16-nitro-2,3,5,6,8,9,11,12-octahydrobenzo[b][1,4,7,10,13]pentaoxacyclopentadecin-15-amine
- 其它别名4'-Amino-5'-Nitrobenzo-15-Crown-5 ; 1,4,7,10,13-Benzopentaoxacyclopentadecin-15-Amine, 2,3,5,6,8,9,11,12-Octahydro-16-Nitro-; 17-Nitro-2,5,8,11,14-Pentaoxabicyclo[13.4.0]Nonadeca-1(15),16,18-Trien-18-Amine; 4,-Amino-5'-Nitrobenzo-15-Crown-5; 4'-Amino-5'-Nitrobenzo-15-Crown-5; 16-Nitro-2,3,5,6,8,9,11,12-Octahydrobenzo[b][1,4,7,10,13]Pentaoxacyclopentadecin-15-Amine; 4,-Amino-5'-Nitrobenzo-15-Crown-5
- CAS编号77001-50-4
- MFCD编号:MFCD00188437
- EINECS号:636-021-2
- 分子式:C14H20N2O7分子量:328.32
- 产品CID: 1762546
- 产品分类化学试剂 → 有机试剂 → 冠醚
物理性质
MSDS等安全信息
欧盟法规
ECHA物质C&L通报上下游产品
CAS号60835-69-0 4'-硝基苯-15-冠醚-5 | CAS号14098-44-3 苯并-15-冠醚-5 | CAS号77001-49-1 15-(Acetylamino... | CAS号77001-48-0 N-(2,3,5,6,8,9,... | CAS号60835-71-4 4'-氨基苯并-15-冠5-醚 | CAS号83935-64-2 15-Is°Cyanato-1... | CAS号83935-77-7 Carbamicacid,(2...合成工艺路线路线简述
- 合成目标产物 4'-Amino-5'-Nitrobenzo-15-Crown-5 主要起始原料 N-(16-Nitro-2,3,5,6,8,9,11,12-Octahydro-1,4,7,10,13-Benzopentaoxacyclopentadecin-15-yl)Acetamide
- (文献来源)合成步骤主要原料 N-(16-Nitro-2,3,5,6,8,9,11,12-Octahydro-1,4,7,10,13-Benzopentaoxacyclopentadecin-15-yl)Acetamide
📜苯并-15-冠醚-5置于palladium On Activated Charcoal 盐酸,氢气,硝酸体系中,用 氯仿,溶剂黄146 作为反应溶剂,20.0~25.0 °C,5.0 Mpa 条件下,反应 48.33H,反应生成 4-氨基-5-硝基苯并-15-冠-5
参考文献:Kruse,Rolf; Breitmaier,Eberhard,Chemische Berichte,1981,Vol. 114,# 2,P. 832-836
标题:Kruse,Rolf; Breitmaier,Eberhard,Chemische Berichte,1981,Vol. 114,# 2,P. 832-836
海关参考信息
- 2905310000-1,2-乙二醇
2907210001-间苯二酚
2909110000-乙醚
2908991010-4-硝基苯酚 - 💡 提示：海关信息按照顺序优先匹配，如需确认的海关信息，请参考相关资料。
- 详情请参考：📖 海关编码查询和海关进出口税则
专利信息
专利号:CN-104470547-B
优先权日:2012-05-24
标题 :Utilize the method for tubular article synthesis of radiopharmaceuticals
专利号:US-9550704-B2
优先权日:2012-05-24
标 题 :Method for synthesizing radiopharmaceuticals using a cartridge
发明人：CHI DAE YOON; LEE BYOUNG SE; LEE JAE HAK; CHU SO YOUNG; JUNG WOON JUNG
权利人:FUTURECHEM CO LTD
摘要:The present invention relates to a method for synthesizing a radiopharmaceutical using a cartridge, which makes it possible to carry out several steps of reaction required for synthesizing a radiopharmaceutical in the cartridge filled with a polymer. A method for synthesizing a radiopharmaceutical according to the present invention enables each step's reaction to be carried out with the solution confined in the cartridge so as not to flow out, thus being simplified compared to the conventional methods for synthesizing radiopharmaceuticals, and expediting the synthesis thereof.
