CAS: 169051-76-7; 1,2-Dimethyl-3-Propyl-1H-Imidazol-3-Ium Bis((Trifluoromethyl)Sulfonyl)Amide

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CAS号107937-17-7 1-丙基-2,3-二甲基咪唑溴盐 | CAS号90076-65-6 双三氟甲基磺酰亚胺锂 | CAS号1739-84-0 1,2-二甲基咪唑

📜1,2-二甲基咪唑 以 水,乙腈 用作溶剂,化学反应 19.0H,反应生成1,2-二甲基-3-丙基咪唑双(三氟甲基磺酰)亚胺
参考文献:具有三和四取代的咪唑鎓阳离子的离子液体的实验密度和计算的分数自由体积
标题:具有三和四取代的咪唑鎓阳离子的离子液体的实验密度和计算的分数自由体积
摘要:尽管据估计,至少有100万种离子液体(il)可以使用市售的起始原料来获得,但围绕各种应用进行了实验合成,表征和研究的大部分ils仍在使用中相对简单的1-N-烷基-3-甲基咪唑鎓([c Nmim])阳离子基序.然而,对于为什么三或四官能化的咪唑鎓阳离子受到较少关注没有根本的限制或原因.仅有很少的基于三官能化咪唑鎓的il的物理性质数据存在,实际上没有关于四官能化il的数据.因此,Il的"图"上存在广阔的实验空间,而这些空间在很大程度上尚待探索.我们试图对这些"未知水域"进行初步考察,并合成了基于咪唑鎓的il,在其c(2),C(4)和/或c(5)位置带有一个或多个官能团.咪唑环(以及n(1)和n(3)).该手稿报告了这些三功能和四功能化il的合成和实验密度,以及根据cosmotherm计算得出的密度和自由体积分数.
Doi:10.1021/acs.Jced.7B01033

专利信息

专利号:US-9267213-B1
优先权日:2005-03-25
标题:Electrochemical deblocking solution for electrochemical oligomer synthesis on an electrode array
发明人：MAURER KARL; COOPER JOHN J
权利人:CUSTOMARRAY INC
摘要:There is disclosed an electrochemical deblocking solution for use on an electrode microarray. There is further disclosed a method for electrochemical synthesis on an electrode array using the electrochemical deblocking solution. The solution and method are for removing acid-labile protecting groups for synthesis of oligonucleotides, peptides, small molecules, or polymers on a microarray of electrodes while substantially improving isolation of deblocking to active electrodes. The method comprises applying a voltage or a current to at least one electrode of an array of electrodes. The array of electrodes is covered by the electrochemical deblocking solution.

专利号:US-10407676-B2
优先权日:2014-12-09
标题 :High efficiency, small volume nucleic acid synthesis
发明人：POEHMERER THOMAS; KUHN PHILLIP; NOTKA FRANK; ZEIDLER ANDREAS; HEIL KORBINIAN; TREFZER AXEL; FONNUM GEIR; KATZEN FEDERICO; ANDERSSON KRISTIAN
权利人:LIFE TECHNOLOGIES CORP; THERMO FISHER SCIENT GENEART GMBH; LIFE TECH AS
摘要:The disclosure generally relates to compositions and methods for the production of nucleic acid molecules. In some aspects, the invention allows for the microscale generation of nucleic acid molecules, optionally followed by assembly of these nucleic acid molecules into larger molecules. In some aspects, the invention allows for efficient production of nucleic acid molecules (e.g., large nucleic acid molecules such as genomes).

专利号:MX-2007011815-A
优先权日:2005-03-25
标题 :ELECTROCHEMICAL UNLOCK SOLUTION FOR ELECTROCHEMICAL SYNTHESIS OF OLIGOMEROS IN AN ARRANGEMENT OF ELECTRODES.