CAS: 16355-92-3; 1,10-Diiododecane

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24772-63-2 629-09-4 628-77-3

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CAS号112-47-0 1,10-癸二醇 | CAS号2162-98-3 1,10-二氯癸烷 | CAS号111-20-6 癸二酸 | CAS号4101-68-2 1,10-二溴癸烷 | CAS号61575-02-8 10-phenoxydecox... | CAS号110-40-7 癸二酸二乙酯 | CAS号10471-28-0 十二烷二酸二乙酯 | CAS号53463-68-6 10-溴-1-癸醇 | CAS号10034-85-2 氢碘酸 | CAS号4543-66-2 癸二腈 | CAS号30391-54-9 1H-Isoindole-1,... | CAS号124-18-5 正癸烷 | CAS号112-95-8 二十烷 | CAS号693-23-2 十二烷二酸 | CAS号102119-87-9 methyl 11-(2-pe... | CAS号1871-96-1 癸二腈 | CAS号1191-67-9 1,10-癸二硫醇 | CAS号32113-15-8 1-(10-pyridin-1... | CAS号1420-40-2 碘化十烃季胺

1,10-癸二醇置于咪唑,碘,三苯基膦体系中,用 四氢呋喃 用作溶剂,化学反应 6.0H,以90%的收率获得1,10-二碘癸烷
参考文献:促乙酸素的γ-甲基丁烯内酯单元的sharpless Ad策略:具有蚊幼虫活性的丁烯内酯i和ii的对映选择性合成
标题:促乙酸素的γ-甲基丁烯内酯单元的sharpless Ad策略:具有蚊幼虫活性的丁烯内酯i和ii的对映选择性合成
摘要:基于sharpless不对称二羟基化技术,以高收率和非常好的对映体纯度为基础,建立了一种针对γ-甲基丁烯内酯的新型合成策略.该途径可扩展为合成天然存在的非丙酮产乙酸原素的α,γ-二取代丁烯内酯单元.利用这种策略,对映体选择性合成了三种具有丁烯内酯链段的简单天然产物.
Doi:10.1016/s0040-4020(02)01063-3

专利信息

专利号:US-7557099-B2
优先权日:2004-03-01
标题 :Pyrrolobenzodiazepines as key intermediates in the synthesis of dimeric cytotoxic pyrrolobenzodiazepines
发明人：HOWARD PHILIP WILSON; KANG GYOUNG-DONG
权利人:SPIROGEN LTD
摘要:Compounds and a method of synthesis of compounds of formula (Ia) or (Ib): and salts, solvates, and chemically protected forms thereof, wherein the dotted lines indicate the optional presence of a double bond between C1 and C2 or C2 and C3; R 2 and R 3 are independently selected from —H, â•?O, â•?CH 2 , —CN, —R, OR, halo, â•?CH—R, O—SO 2 —R, CO 2 R and COR; R 10 is a carbamate-based nitrogen protecting group; and R 11 is an oxygen protecting group.

专利号:US-9512250-B2
优先权日:2012-02-23
标 题 :Manganese catalyzed photopolymerization of fluorinated monomers
发明人：ASANDEI ALEXANDRU D
权利人:UNIV CONNECTICUT
摘要:The disclosure discloses initiating systems for the radical polymerization of alkenes, and especially fluorine substituted alkenes. The polymerization is catalyzed by a metal carbonyl, preferably manganese carbonyl. The polymerization is initiated directly from alkyl halides at room temperature under visible white light. The polymers also allow the synthesis of block copolymers. The process comprises polymerizing at least one alkene monomer in the presence of a halide radical initiator, carbonyl catalyst and a solvent, under reaction conditions and for a time sufficient to polymerize the at least one alkene monomer to form a polymer. The present disclosure provides a method for living polymerization of alkene monomers which provides a high level of macromolecular control over the polymerization process and which leads to uniform and controllable polymeric products. This disclosure also provides a method for activating any halide (Cl, Br, I) chain ends of such polymers for the synthesis of block copolymerizations.

专利号:US-6110906-A
优先权日:1989-03-10
标题:Androgen derivatives for use in the inhibition of sex steroid activity
发明人：LABRIE FERNAND; MERAND YVES
权利人:ENDORECHERCHE INC
摘要:Methods for treating sex steroid-dependent diseases by inhibiting sex steroid activity include administration of novel compounds which include an androgenic nucleus substituted at a ring carbon with at least one substituent specified herein. Such compounds may function by inhibiting sex steroid synthesis (both estrogen and androgen synthesis) and/or by antagonistically blocking androgen receptors.

专利号:US-2007191309-A1
优先权日:2004-03-01
标题 :Pyrrolobenzodiazepines as key intermediates in the synthesis of dimeric cytotoxic pyrrolobenzodiazepines

专利号:US-4348377-A
优先权日:1979-08-09
标题:New derivatives of 2,4,6-triiodo-isophthalic acid, proceses for their synthesis and X-ray contrasting materials containing these
发明人：FELDER ERNST; PITRE DAVIDE
权利人:BRACCO IND CHIMICA SPA
摘要:Novel, radio-opaque compounds comprising water-soluble bis-[N-{3,5-bis-(hydroxyalkylaminocarbonyl)-2,4,6-triiodo-phenyl}-N-( alpha -hydroxyacyl)-amino]-alkanes are disclosed for use as X-ray contrast agents. These compounds are relatively simple to synthesize, possess low toxicity and have good stability as well as resistance to hydrolysis. Methods for preparation and use of the compounds are also disclosed.

专利号:WO-2005085259-A2
优先权日:2004-03-01
标 题 :Pyrrolobenzodiazepines as key intermediates in the synthesis of dimeric cytotoxic pyrrolobenzodiazepines