CAS: 473-06-3; 2-Pinen-7-One

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      专利号:US-5900227-A
      优先权日:1996-06-17
      标题 :Multicyclic nitrone spin trapping compositions
      发明人：JANZEN EDWARD G; SANKURATRI NAGARAJU
      权利人:OKLAHOMA MED RES FOUND
      摘要:Multicyclic nitrone spin trapping compounds capable of forming stable free radical spin adducts are provided as well as methods for their synthesis. The multicyclic nitrone spin trapping compounds can be reacted with a free radical, such as a hydroxy or hydroperoxy radical, in solution to form a spin adduct which is stable and readily detectable by electron paramagnetic resonance (EPR) spectroscopy. The multicyclic nitrone spin traps can be used to detect free radicals in a sample such as a biological system. In one embodiment, the spin trapping compound, 1,3,3-trimethyl-6-azabicyclo-[3.2.1]oct-6-ene-N-oxide ('TRAZON') is provided, as well as methods for the synthesis of TRAZON and of modified forms of TRAZON. TRAZON can react with a wide range of different free radicals in solution to form free radical spin adducts which are readily detectable by EPR.

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      参考文献:10.1016/0031-9422(88)83114-5
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      参考文献:10.1080/10412905.1995.9698577
      摘要:Küsmenoglu S, Baser KHC, Özek T, Harmandar M, Gökalp Z. Constituents of the Essential Oil ofAchillea biebersteiniiAfan. Journal of Essential Oil Research. 1995 Sep;7(5):527–8. doi: 10.1080/10412905.1995.9698577.
      参考文献:10.1016/s0031-9422(00)83196-9
      摘要:Metwally MA, Jakupovic J, Youns MI, Bohlmann F. Eudesmanolides from Artemisia judaica. Phytochemistry. 1985 Jan;24(5):1103–4. doi: 10.1016/s0031-9422(00)83196-9.
      参考文献:10.1016/0031-9422(94)85021-6
      摘要:Ahmad A, Misra LN. Terpenoids from Artemisia annua and constituents of its essential oil. Phytochemistry. 1994 Jan;37(1):183–6. doi: 10.1016/0031-9422(94)85021-6.
      参考文献:10.1016/s0031-9422(00)82268-2
      摘要:Flynn TM, Southwell IA. Essential oil constituents of the genus Zieria. Phytochemistry. 1987 Jan;26(6):1673–86. doi: 10.1016/s0031-9422(00)82268-2.
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