CAS: 527-89-9; Dithiosalicylic Acid

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CAS号89-95-2 邻甲基苄醇 | CAS号90-02-8 水杨醛 | CAS号74976-14-0 1-anilino-ethan... | CAS号64-17-5 乙醇 | CAS号7732-18-5 水 | CAS号82799-44-8 2,4-二乙基硫杂蒽酮

📜邻甲基苄醇置于ammonium Polysulfide体系中,用 乙醇 作为反应溶剂,化学反应 1.0H,反应生成 二硫代水杨酸
参考文献:N-水杨酰基-N'-羟基硫代苯甲酰肼的mn(II),Fe(iii),Co(II),Ni(II),Cu(II)和zn(II)配合物的合成,表征和抗肿瘤研究.
标题:N-水杨酰基-N'-羟基硫代苯甲酰肼的mn(II),Fe(iii),Co(II),Ni(II),Cu(II)和zn(II)配合物的合成,表征和抗肿瘤研究.
摘要:一种新的配体n-水杨酰-N'-邻-羟基硫代苯并肼(h2Sotbh)形成复合物[mn(hsotbh)2],[fe(sotbh-H)(h2O)2],[m(sotbh)] [m = Co(Ii),Cu(II)和zn(II)]和[ni(sotbh)(h(2)o)2],通过各种物理化学技术进行了表征.[fe(sotbh-H)(h2O)2]的穆斯堡尔光谱揭示了5/2和3/2自旋态的量子混合物.观测到mn(II),Cu(II)和ni(II)配合物在体外抑制肿瘤的生长,而fe(iii),Co(II),Zn(II)配合物则不能.体内施用mn(II),Cu(II)和ni(II)可延长荷瘤小鼠的生存期.给予mn(II),Cu(II)和ni(II)配合物的荷瘤小鼠显示出与淋巴细胞凋亡诱导相关的肿瘤生长逆转.
DOI:10.1016/s0968-0896(01)00373-X

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