CAS: 949-99-5; H-Phe(4-No2)-Oh

该化合物是一种该化合物是一种具有硝基和氨基混合物的手性化合物,具有多种化学反应性,该化合物的结构复杂性允许有机合成中的各种应用,包括合成药品和精美化学品,其性能在不对称合成中具有明显的优势,有可能使由此产生的产品具有更高的对等纯度.

结构式图片

相似化合物

207591-86-4 444777-67-7 95753-55-2

物理性质

MSDS等安全信息

欧盟法规

ECHA物质C&L通报REACH预注册

上下游产品

CAS号63-91-2 L-苯丙氨酸 | CAS号33305-77-0 B°C-L-4-硝基苯丙氨酸 | CAS号62561-97-1 Phenylalanine, ... | CAS号56-40-6 甘氨酸 | CAS号100-11-8 4-硝基溴化苄 | CAS号38335-24-9 (对硝基苯基)丙酮酸 | CAS号1991-83-9 4-nitrophenylalanine | CAS号17363-92-7 (S)-2-乙酰胺基-4-硝基苯丙氨酸 | CAS号101468-97-7 N-benzoyl-(4'-n... | CAS号943-80-6 4-氨基-L-苯丙氨酸 | CAS号33305-77-0 B°C-L-4-硝基苯丙氨酸 | CAS号55533-24-9 B°C-4-氨基-L-苯丙氨酸 | CAS号55533-25-0 N-alpha-t-丁基氧基羰... | CAS号34276-53-4 3-(4-硝基苯基)-L-丙氨酸 | CAS号58816-66-3 3-(4-硝基苯基)-L-丙氨酸盐酸盐 | CAS号49607-21-8 (S)-2-氨基-3-(2,4... | CAS号943-80-6 4-氨基-L-苯丙氨酸 | CAS号79815-20-6 (S)-(-)-吲哚啉-2-羧酸 | CAS号95753-55-2 Fm°C-对硝基-L-苯丙氨酸 | CAS号95753-56-3 FM°C-4-氨基-L-苯丙氨酸

合成工艺路线路线简述

  • 63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 60 S,0 °C
    标题:Green Preparation Of Zolmitriptan Intermediate
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid; 35 Min,0 - 5 °C; 1 H,0 - 5 °C1.2 Reagents: Ammonium Hydroxide Solvents: Water; Neutralized,Cooled
    标题:Chiral Gap Catalysts Of Phosphonylated Imidazolidinones And Their Applications In Asymmetric Diels-Alder And Friedel-Crafts Reactions
    作者:Qiao,Shuo; Mo,Junming; Wilcox,Cody B.; Jiang,Bo; Li,Guigen
    参考文献:Organic & Biomolecular Chemistry 日期:2017 卷标:15(7) 页码:1718-1724]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 0 °C; 1 H,0 °C1.2 Solvents: Water; 15 Min,Cooled; Heated1.3 Reagents: Ammonium Hydroxide Solvents: Water; Neutralized
    标题:Design And Synthesis Of Calcium Responsive Magnetic Resonance Imaging Agent: Its Relaxation And Luminescence Studies
    作者:Tanwar,Jyoti; Datta,Anupama; Chauhan,Kanchan; Kumaran,S. Senthil; Tiwari,Anjani K.; Et Al
    参考文献:European Journal Of Medicinal Chemistry 日期:2014 卷标:82 页码:225-232]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid; 3 H,0 °C
    标题:Transformation Of L-Phenylalanine To (S)-Indoline-2-Carboxylic Acid Without Group-Protection
    作者:Liu,Jin-Qiang; Chen,Xin-Zhi; Ji,Baoming; Zhao,Bang-Tun
    参考文献:Research On Chemical Intermediates 日期:2013 卷标:39(3) 页码:1143-1152]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 50 °C1.2 Reagents: Ammonium Hydroxide Solvents: Water; 1 H,Neutralized,0 °C
    标题:Study On The Synthesis Of L-4-Nitrophenylalanine
    作者:Liu,Jin-Qiang; Qian,Chao; Zhang,Tao; Chen,Xin-Zhi
    参考文献:Gaoxiao Huaxue Gongcheng Xuebao 日期:2009 卷标:23(6) 页码:1007-1012]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; < 20 °C; < 20 °C; 12 H; 0 °C1.2 Reagents: Sodium Hydroxide Solvents: Water; Ph 7 - 8,< 25 °C
    标题:Preparation Of (αs)-α-Methoxy-4-[[3-[4-[(Methylsulfonyl)Oxy]Phenyl]Propyl]Amino]-Benzenepropanoic Acid As Antidiabetic Agent
    参考文献:India]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; Rt -> -20 °C; < 5 °C; 5 °C -> 25 °C; 3 H,25 °C1.2 Reagents: Ammonium Hydroxide Solvents: Water; Ph 7
    标题:Process For Preparation Of (-)-(S)-6-Nitroindoline-2-Carboxylic Acid From L-Phenylalanine
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; Rt; 5 H,Rt1.2 Reagents: Sodium Hydroxide Solvents: Water; Ph 2 - 3
    标题:Synthesis And Anti-Hepatitis B Virus Activities Of Matijing-Su Derivatives
    作者:Xu,Bixue; Huang,Zhengming; Liu,Changxiao; Cai,Zegui; Pan,Weidong; Et Al
    参考文献:Bioorganic & Medicinal Chemistry 日期:2009 卷标:17(8) 页码:3118-3125]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; Rt; 5 H,Rt1.2 Reagents: Sodium Hydroxide Solvents: Water; Ph 2 - 3
    标题:Preparation Of N-(N-Benzoylphenylalanyl)Phenylalanine Dipeptide Derivatives As Antiviral Agents
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; Rt -> 10 °C; 10 °C; 2.5 H,10 °C1.2 Reagents: Ammonia Solvents: Water; Ph 5 - 6
    标题:Synthesis And Biological Evaluation Of Matijing-Su Derivatives As Potent Anti-Hbv Agents
    作者:Qiu,Jingying; Xu,Bixue; Huang,Zhengming; Pan,Weidong; Cao,Peixue; Et Al
    参考文献:Bioorganic & Medicinal Chemistry 日期:2011 卷标:19(18) 页码:5352-5360]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 10 °C; 3 H,8 - 10 °C1.2 Reagents: Sodium Hydroxide Solvents: Water; Ph 6
    标题:Synthesis Of New Tetrazolyl Derivatives Of L- And D-Phenylalanine
    作者:Tolstyakov,V. V.; Tolstobrova,E. S.; Zarubina,O. S.; Popova,E. A.; Protas,A. V.; Et Al
    参考文献:Russian Journal Of Organic Chemistry 日期:2016 卷标:52(11) 页码:1681-1685]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; -10 °C; < 0 °C; < 0 °C -> -10 °C1.2 -10 °C; < 5 °C; 1 H,0 °C; 1 H,0 °C -> Rt1.3 Reagents: Ammonia Solvents: Water; Ph 8 - 9
    标题:Preparation Of Melphalan As Nitrogen Mustards Chemotherapy Drug
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 10 °C; 2.5 H,10 °C1.2 Reagents: Ammonium Hydroxide Solvents: Water; Ph 5
    标题:Distinct Metabolites For Photoreactive L-Phenylalanine Derivatives In Klebsiella Sp. Ck6 Isolated From Rhizosphere Of A Wild Dipterocarp Sapling
    作者:Wang,Lei; Hisano,Wataru; Murai,Yuta; Sakurai,Munenori; Muto,Yasuyuki; Et Al
    参考文献:Molecules 日期:2013 卷标:18 页码:8393-8401]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 0 °C; 60 Min,0 °C; 1 H,Rt1.2 Reagents: Water; 15 Min,Cooled1.3 Reagents: Ammonium Hydroxide Solvents: Water; Ph 6 - 8,Cooled
    标题:Process For The Preparation Of L-P-Nitrophenylalanine
    作者:Kong,Ling-Qiang; Su,Xiao-Yan; Wang,Lin-Fa; Du,Pei-Yan; Yang,Da-Cheng
    参考文献:Xinan Daxue Xuebao 日期:2009 卷标:31(9) 页码:102-105]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 3 H,0 - 20 °C
    标题:A Facile Chiral Pool Synthesis Of (S)-6-Nitroindoline-2-Carboxylic Acid From L-Phenylalanine
    作者:Liu,Jin-Qiang; Qian,Chao; Chen,Xin-Zhi
    参考文献:Synthesis 日期:2010 卷标:(3) 页码:403-406]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 5 Min,50 °C1.2 Reagents: Ammonium Hydroxide Solvents: Water; Ph 7 - 8,Cooled
    标题:Method For Synthesis Of L-4-Nitrophenylalanine
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; < 2 °C; < 20 °C; 30 Min,20 °C -> Rt1.2 Reagents: Ammonia Solvents: Water; Ph 9.5 - 10.5,< 5 °C
    标题:Process For Preparation Of Zolmitriptan Via Cyclization,Reductive Hydrogenation And Diazotization
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; 0 - 5 °C; 2 H,0 - 5 °C; 2 H,20 - 30 °C; 2 H,40 - 50 °C; 50 °C -> Rt1.2 Reagents: Sodium Hydroxide Solvents: Water; Ph 6 - 7,0 °C
    标题:Process For Synthesis Of L-4-Nitrophenylalanine
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; Rt -> 0 °C; 0 °C -> Rt; 60 Min,Rt1.2 Reagents: Water; 0 °C1.3 Reagents: Ammonium Hydroxide Solvents: Water; Ph 6
    标题:Process For Preparation Of L-P-Nitrophenylalanine Dipeptide Derivative And Its Application To Prepare The Medical Preparations For Treating Diabetes Mellitus
    参考文献:China]

    63-91-2 = 949-99-5
    反应条件:1.1 Reagents: Sulfuric Acid,Nitric Acid Solvents: Water; < 30 °C; 30 °C -> 0 °C; 5 °C; 2 H,5 °C; 2 H,20 - 30 °C; 2 H,40 - 50 °C; 50 °C -> Rt1.2 Reagents: Water; < 20 °C1.3 Reagents: Ammonium Hydroxide Solvents: Water; 20 °C -> 0 °C; 1 H,Ph 6.3,0 °C
    标题:Method For Preparing Zolmitriptan
    参考文献:China
对硝基肉桂酸置于ammonium Hydroxide,硼烷铵络合物体系中,用 Aq. Buffer 作为反应溶剂,以57%的收率获得产物4-硝基-L-苯丙氨酸
参考文献:苯丙氨酸氨裂解酶合成 D-和 L-苯丙氨酸衍生物:多酶级联过程
标题:苯丙氨酸氨裂解酶合成 D-和 L-苯丙氨酸衍生物:多酶级联过程
摘要:通过将苯丙氨酸解氨酶 (Pal) 胺化与化学酶脱外消旋(基于立体选择性氧化和非选择性还原).还开发了一种简单的高通量固相筛选方法来鉴定具有较高非天然d-苯丙氨酸形成率的 Pal.在化学酶级联中利用了最佳变体,从而提高了d配置产品的产量和 Ee 值.此外,该系统还扩展到制备低浓度的l-苯丙氨酸.ee 值使用pal胺化.
DOI:10.1002/anie.201410670

海关参考信息

专利信息


专利号:US-5545568-A
优先权日:1992-09-14
标题:Solid phase and combinatorial synthesis of compounds on a solid support
发明人：ELLMAN JONATHAN A
权利人:UNIV CALIFORNIA
摘要:Methods, compositions, and devices for synthesizing combinatorial libraries of various useful compounds, such as benzodiazepines, prostaglandins, β-turn mimetics and glycerol-derived drugs is described. In order to expediently synthesize such combinatorial libraries of derivatives based upon these core structures, a general methodology for the solid phase synthesis of these derivatives is also provided. This disclosure thus also describes an important extension of solid phase synthesis methods to nonpolymeric organic compounds.

专利号:US-9938509-B2
优先权日:2010-12-08
标 题 :Biocatalysts and methods for the synthesis of armodafinil
发明人：ANG EE LUI; ALVIZO OSCAR; BEHROUZIAN BEHNAZ; CLAY MICHAEL D; COLLIER STEVEN J; EBERHARD ELLEN D; FAN FU; SONG SHIWEI; SMITH DEREK J; WIDEGREN MAGNUS; WILSON ROBERT; XU JUNYE; ZHU JUN
权利人:CODEXIS INC
摘要:The present invention relates to non-naturally occurring polypeptides useful for preparing armodafinil, polynucleotides encoding the polypeptides, and methods of using the polypeptides. The non-naturally occurring polypeptides of the present invention are effective in carrying out biocatalytic conversion of the (i) 2-(benzhydrylsulfinyl)acetamide to (−)-2-[(R)-(diphenylmethyl)sulfinyl]acetamide (armodafinil), or (ii) benzhydryl-thioacetic acid to (R)-2-(benzhydrylsulfinyl)acetic acid, which is a pivotal intermediate in the synthesis of armodafinil, in enantiomeric excess.

专利号:US-2006211083-A1
优先权日:2005-01-21
标题:Products and processes for in vitro synthesis of biomolecules
发明人：KATZEN FEDERICO; KUDLICKI WIESLAW; FLETCHER JULIA
权利人:KATZEN FEDERICO; KUDLICKI WIESLAW; FLETCHER JULIA
摘要:Provided herein are products and processes for efficiently synthesizing biomolecules in vitro using cell-free extracts derived from mammalian cells and insect cells. In an embodiment, provided is a process for preparing a cell-free extract from insect cells and mammalian cells that efficiently synthesizes post-translationally modified target proteins (e.g., glycosylated target proteins). In some embodiments, a ribonucleic acid is synthesized in vitro that comprises a cap, a 5′ untranslated region comprising an 18S rRNA binding ribonucleotide sequence, and a target ribonucleotide sequence. It has been determined that such ribonucleic acids result in efficient in vitro synthesis of a target protein using cell-free extracts derived from non-rabbit mammalian cells and insect cells.

专利号:US-10087221-B2
优先权日:2013-03-21
标题 :Synthesis of hydantoin containing peptide products
发明人：HENKEL BERND
权利人:SANOFI AVENTIS DEUTSCHLAND
摘要:The present invention relates to a method of synthesizing a peptide product comprising at least one hydantoin group. The peptide product may be used as a reference material for the quality control of pharmaceutical peptides, particularly for the quality control of exendin peptides. Further, the invention relates to hydantoin building blocks, a method for manufacturing such building blocks and their use for the synthesis of peptide products.

专利号:WO-2017100796-A1
优先权日:2015-12-11
标 题 :Modulation of globoseries glycosphingolipid synthesis and cancer biomarkers
发明人：WONG CHI-HUEY; HSU TSUI-LING; WU CHUNG-YI; CHEUNG SARAH K C; CHUANG PO-KAI
权利人:SINACA ACAD; WONG CHI-HUEY; HSU TSUI-LING
摘要:The present disclosure relates to methods and compositions which can modulate the globoseries glycosphingolipid synthesis. Particularly, the present disclosure is directed to glycoenzyme inhibitor compound and compositions and methods of use thereof that can modulate the synthesis of globoseries glycosphingolipid SSEA-3/SSEA-4/GloboH in the biosynthetic pathway; particularly, the glycoenzyme inhibitors target the alpha-4GalT; beta- 4GalNAcT-I; or beta-3GalT-V enzymes in the globoseries synthetic pathway. Additionally, the present disclosure is also directed to vaccines, antibodies, and/or immunogenic conjugate compositions targeting the SSEA-3/SSEA-4/GLOBO H associated epitopes (natural and modified) which elicit antibodies and/or binding fragment production useful for modulating the globoseries glycosphingolipid synthesis. Moreover, the present disclosure is also directed to the method of using the compositions described herein for the treatment or detection of hyperproliferative diseases and/or conditions. Furthermore, the instant disclosure also relates to cancer stem cell biomarkers for disgnostic and therapeutic uses.

专利号:US-2023212788-A1
优先权日:2020-03-26
标 题:New method for automated on-demand biomolecular array synthesis
发明人：ZHANG YIXIN; LIN WEILIN
权利人:UNIV DRESDEN TECH
摘要:The invention provides an amphiphilic coating for the direct and rapid synthesis of an array of peptides and small molecular compounds on a planar surface of a solid support, comprising a hydrophilic chemical structure and a lipophilic group, wherein said peptides and small molecular compounds differ from spot to spot from each other in the chemical structure, characterized in that said amphiphilic coating possesses low wettability to polar aprotic solvents used in the array synthesis; said amphiphilic coating possessing low wettability is designed that it can be converted to a coating possessing high wettability by hydrolysis of the lipophilic group; and said amphiphilic coating comprises an amino group for the reaction with an electrophilic reagent. The invention further provides a solid support comprising said amphiphilic coating and a method for method for the direct and rapid synthesis of an array of peptides and small molecular compounds on a planar surface of a solid support, wherein said planar surface of a solid support comprises said amphiphilic coating. Said method includes the enhancing of the wettability of a glass surface to organic solvents to realize automated on-demand biomolecular array synthesis comprising both, peptides and small molecular compounds. The amphiphilic surface can be switched to a hydrophilic surface, resulting in high density arrays suitable for protein- and cell-based screening.

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合成参考文献


摘要:Bartsch, S.; Vogel, A., Science of Synthesis: Biocatalysis in Organic Synthesis, (2015) 2, 302.
摘要:Parmeggiani, F.; Galman, J. L.; Montgomery, S. L.; Turner, N. J., Science of Synthesis, (2019) , 408.
参考文献:10.1186/1756-3305-1-7
摘要:Sojka D, Franta Z, Horn M, Hajdusek O, Caffrey CR, Mares M, Kopácek P. Profiling of proteolytic enzymes in the gut of the tick Ixodes ricinus reveals an evolutionarily conserved network of aspartic and cysteine peptidases. Parasit Vectors. 2008 Mar 18;1(1):7.
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