CAS: 304-06-3; 2-Hydroxy-[1,1'-Biphenyl]-3-Carboxylic Acid

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CAS号124-38-9 二氧化碳 | CAS号132-27-4 邻苯基苯酚钠 | CAS号90-43-7 2-苯基苯酚 | CAS号14562-10-8 2-羟基-[1,1'-联苯]-3-甲醛 | CAS号108-90-7 氯苯 | CAS号16094-36-3 3-Cyclohexylsal... | CAS号17755-10-1 3-甲基联苯-2-醇 | CAS号99514-99-5 5-Bromo-2-hydro... | CAS号478942-85-7 1-ethenyl-3-phe... | CAS号60821-26-3 2-acetyloxy-3-p... | CAS号63992-45-0 N,N-Diethyl-2-h... | CAS号63992-48-3 2-Hydroxy-N-(2-... | CAS号63906-82-1 2-(β-Hydroxyeth...

📜邻苯基苯酚置于咪唑,Boc-L-亮氨酸,2,2,2-三氟乙醇,四丁基氟化铵,水,Silver(I) Acetate,Palladium Diacetate,碳酸氢钠体系中,用 四氢呋喃,乙醚,1,2-二氯乙烷,N,N-二甲基甲酰胺 作为反应溶剂,化学反应 19.58H,反应生成 3-苯基水杨酸
参考文献:钯催化硅烷醇引导的 CH 羧化反应从酚类合成水杨酸的通用方法
标题:钯催化硅烷醇引导的 CH 羧化反应从酚类合成水杨酸的通用方法
摘要:已经开发出一种硅烷醇引导,钯催化的苯酚 C-> H 羧化反应,反应生成水杨酸.该方法具有高效,选择性高,官能团耐受性好的特点.该方法的通用性通过雌酮的羧化和通过两个连续的c-H官能化过程合成不对称o,O'-二取代酚类化合物得到证明.
DOI:10.1002/anie.201410375

专利信息

专利号:US-10919904-B2
优先权日:2016-08-17
标 题 :Northern-southern route to synthesis of bacteriochlorins
发明人：LIU YIZHOU; LINDSEY JONATHAN S; ALLU SRINIVASA RAO; FUJITA HIKARU
权利人:UNIV NORTH CAROLINA STATE
摘要:Described herein are chlorins, bacteriochlorins, methods and intermediates for the synthesis of bacteriochlorins, and methods of using such bacteriochlorins for, among other things, diagnostic and therapeutic purposes such as luminescent compounds in flow cytometry, and as active agents in photodynamic therapy (PDT).

专利号:US-2010137421-A1
优先权日:2006-11-08
标题 :Small molecule therapeutics, synthesis of analogues and derivatives and methods of use
发明人：THEODORAKIS EMMANUEL; BATOVA AYSE
权利人:THEODORAKIS EMMANUEL; BATOVA AYSE
摘要:Provided herein are compounds that are inducers of apoptosis activators of caspases and pharmaceutically acceptable derivatives thereof. Also provided are methods of synthesis of the compounds and methods for treatment of diseases in which there is uncontrolled cell growth and spread of abnormal cells, such as cancers, by administering the compounds.

专利号:US-6362009-B1
优先权日:1997-11-21
标 题 :Solid phase synthesis of heterocycles
发明人：MUNOZ BENITO; CHEN CHIXU
权利人:MERCK & CO INC
摘要:Methods for solid phase and combinatorial synthesis using a resin activation/capture approach are provided. In particular, methods for the production of dihydropyridones, N-acyidihydropyridones, tetrahydropyridones, pyridines, aminopyridines, N-acyltetrahydropyridines and tetrahydropyridines compounds and libraries containing such compounds are provided. Methods for screening the libraries and compounds and pharmaceutical compositions containing compounds prepared by the methods are provided.

专利号:US-9822123-B2
优先权日:2005-02-18
标 题 :De novo synthesis of bacteriochlorins
发明人：KIM HAN-JE; LINDSEY JONATHAN S
权利人:UNIV NORTH CAROLINA STATE
摘要:A method of making a bacteriochlorin is carried out by condensing a pair of compounds of Formula II n nto produce the bacteriochlorin, wherein R is an acetal or aldehyde group. The condensing may be carried out in an organic solvent, preferably in the presence of an acid. The bacteriochlorins are useful for a variety of purposes such as active agents in photodynamic therapy, luminescent compounds in flow cytometry, solar cells, light harvesting arrays, and molecular memory devices.

专利号:US-2004110228-A1
优先权日:2002-04-01
标 题:Combinatorial organic synthesis of unique biologically active compounds
发明人：MCALPINE SHELLI R; TAYLOR RACHEL E; BOLLA MEGAN L; SEGALL ANCA M
摘要:The invention provides a method for making a combinatorial library of cyclic compounds, such as Holliday junction-trapping compounds, comprising the steps of (a) obtaining a plurality of trimers according to the generic structure X 1- X 2- X 3 , wherein X 1 , X 2 and X 3 can be independently any naturally or nonnaturally occurring amino acids or peptidomimetics thereof; (b) optionally coupling a spacer S to the trimer at either end; (c) cyclizing two trimers or trimer-spacer conjugates in a head-to-tail orientation; thereby obtaining a combinatorial library of compounds, wherein the library does not include an unmodifed or naturally occurring Holliday Junction-trapping compounds. The invention additionally provides methods macrocyclic compounds that are synergimycin derivatives.

专利号:US-8207329-B2
优先权日:2005-11-30
标题:Synthesis of chlorins and phorbines with enhanced red spectral features
发明人：LINDSEY JONATHAN S; LAHA JOYDEV K; CHINNASAMY MUTHIAH; BORBAS K ESZTER
权利人:LINDSEY JONATHAN S; LAHA JOYDEV K; CHINNASAMY MUTHIAH; BORBAS K ESZTER; UNIV NORTH CAROLINA STATE
摘要:The present invention provides compounds of the general Formula DI: along with methods of making such compounds, formulations containing the same, and methods of using the same (e.g., in photodynamic therapy, for the production of solar cells, etc.).