专利号:US-7591897-B2 优先权日:2005-03-22 标 题 :Method for the rapid synthesis of large quantities of metal oxide nanowires at low temperatures 发明人:SUNKARA MAHENDRA KUMAR; VADDIRAJU SREERAM; MOZETIC MIRAN; CVELBAR UROS 权利人:UNIV LOUISVILLE RES FOUND 摘要:A process for the rapid synthesis of metal oxide nanoparticles at low temperatures and methods which facilitate the fabrication of long metal oxide nanowires. The method is based on treatment of metals with oxygen plasma. Using oxygen plasma at low temperatures allows for rapid growth unlike other synthesis methods where nanomaterials take a long time to grow. Density of neutral oxygen atoms in plasma is a controlling factor for the yield of nanowires. The oxygen atom density window differs for different materials. By selecting the optimal oxygen atom density for various materials the yield can be maximized for nanowire synthesis of the metal.
专利号:US-4468523-A 优先权日:1982-06-16 标题 :Synthesis of dialkyl oxalates by the heterogeneously catalyzed oxidative carbonylation of alcohols 发明人:LEONARD JOHN J; SOFRANKO JOHN A 权利人:ATLANTIC RICHFIELD CO 摘要:Synthesis of dialkyl oxalates by the oxidative carbonylation of liquid monohydric saturated alcohols of from 1 to 20 carbon atoms with carbon monoxide and oxygen or an oxygen-containing gas in the presence of a catalytic amount of a catalyst comprising palladium or a salt thereof in combination with vanadium in the oxide (V 2 O 5 , V 2 O 4 , V 2 O 3 ) form and titanium or a non-hydrolyzable salt thereof, said catalyst being present in a heterogeneous phase.
专利号:US-4619822-A 优先权日:1984-04-24 标题:Novel process for the synthesis of vanadium oxide, V6 O13 发明人:HAMMOU ABDELKADER; RIGAUD PHILIPPE; ROUSSEAU CATHERINE 权利人:ELF AQUITAINE 摘要:Process for the synthesis of vanadium V 6 O 13 by reduction of V 2 O 5 in the presence of reducing gas. The reducing gas is a mixture of CO and CO 2 .
专利号:US-4065469-A 优先权日:1974-11-25 标题:Process for the synthesis of dibenzofuran 发明人:MOGGI PIETRO ANTONIO; IORI GIUSEPPE 权利人:ANIC SPA 摘要:The invention relates to a process for the synthesis of dibenzofuran by the dehydrocyclization of 2-cyclo-hexenyl-cyclohexanone at high temperature in the presence of air and a catalyst system selected among the known dehydrogenation catalysts. n By the claimed process very high yields of dibenzofuran are achieved.
专利号:US-6254940-B1 优先权日:1996-07-11 标题:Electrically assisted synthesis of particles and film with precisely controlled characteristic 发明人:PRATSINIS SOTIRIS E; VEMURY SRINIVAS 权利人:UNIV CINCINNATI 摘要:The present invention related to methods of manufacturing oxide, nitride, carbide, and boride powders and other ceramic, organic, metallic, carbon and alloy powders and films and their mixtures having well-controlled size and crystallinity characteristics. This invention relates, more particularly, to a development in the synthesis of the ceramic, metallic, composite, carbon and alloy nanometer-sized particles with precisely controlled specific surface area, or primary particle size, crystallinity and composition. The product made using the process of the present invention and the use of that product are also claimed herein.
专利号:US-5487876-A 优先权日:1993-04-02 标题:Apparatus and method for continuous synthesis of vanadium oxide 发明人:MALLINSON STEVEN M; MCALEAVEY MICHAEL E 摘要:In a method for the continuous synthesis of vanadium oxide from ammonium metavanadate, ammonium metavanadate is fed to the interior of a dryer apparatus through an inlet opening. The interior of the apparatus is maintained at a temperature of approximately 440° C. and an inert carrier gas flows through the interior of the apparatus. The ammonium metavanadate is conveyed through the interior of the dryer apparatus on a conveyer to an outlet opening over a period of approximately two hours, during which period the ammonium metavanadate is continuously agitated so that it is uniformly exposed to heat and to the carrier gas, thereby synthesizing homogeneous vanadium oxide. The vanadium oxide is continuously removed from the apparatus.
参考标题:Liquid-Phase Synthesis Of Ba2V2O7 Phosphor Powders And Films Using Immiscible Biphasic Organic-Aqueous Systems 作者:Mami Takahashi,Manabu Hagiwara,Shinobu Fujihara |发布日期:2016.8.15 摘要:A Liquid-Phase Synthesis Of Inorganic Phosphor Materials At A Moderate Temperature Was Proposed By Using Immiscible Liquid-Liquid Biphasic Systems. A Self-Activated Ba2V2O7 Phosphor Was Actually Synthesized From Vanadium Alkoxide Dissolved In An Organic Solution And Barium Acetate In An Aqueous Solution. A Mild Hydrolysis Reaction Of The Alkoxide Started At The Organic-Inorganic Interface, And An Intermediate
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