CAS: 92260-82-7; 7-(Hydroxyimino)-8,9-Dihydro-2,9A-Diazabenzo[cd]Azulene-1,6(2H,7H)-Dione
相似化合物
92260-81-6 1021910-71-3 75655-10-6物理性质
合成工艺路线路线简述
- 合成目标产物 4,5-Dihydro-6-Oxime-Imidazo[4,5,1-Jk][1]Benzazepine-2,6,7(1H)-Trione 主要起始原料 5,6-Dihydroimidazo[4,5,1-Jk][1]Benzazepine-2,7(1H,4H)-Dione
- 92260-81-6 = 92260-82-7
反应条件:1.1 Reagents: Tert-Butyl Nitrite Solvents: Dimethylformamide; 20 °C -> 40 °C1.2 Reagents: Hydrochloric Acid Solvents: Water; 2 - 3 H,40 °C1.3 Reagents: Water; Cooled
标题:Methods For Synthesizing Zilpaterol And Salts Thereof
参考文献:India]
92260-81-6 = 92260-82-7
反应条件:1.1 Reagents: Tert-Butyl Nitrite,Hydrochloric Acid Solvents: Acetic Acid,1,4-Dioxane; 3 H,Rt
标题:Preparation Of Imidazobenzazepinones As β2 Adrenoceptor Agonists For Use As Livestock Feed Additives And As Drugs.
参考文献:United States]
92260-81-6 = 92260-82-7 [标题:Reaction Conditions
标题:Derivatives Of 6-Amino-7-Hydroxy-4,5,6,7-Tetrahydroimidazo[4,5,1-Jk][1]Benzazepin-2(1H)-One.
参考文献:France]
92260-81-6 = 92260-82-7
反应条件:1.1 Solvents: Dimethylformamide; 20 °C; 45 °C; 45 °C -> 20 °C1.2 Reagents: Sodium Nitrite Solvents: Dimethylformamide; 20 °C -> 45 °C; 45 °C -> 48 °C1.3 Reagents: Hydrochloric Acid Solvents: Water; 1 H,48 °C -> 65 °C; 60 - 65 °C; 30 Min,60 °C
标题:Process For Making A Crystalline Zilpaterol Salt
参考文献:World Intellectual Property Organization]
92260-81-6 = 92260-82-7
反应条件:1.1 Reagents: Sodium Nitrite,Hydrochloric Acid Solvents: Isopropanol,Dimethylformamide,Water; Rt -> 50 °C; 30 Min,50 °C -> 70 °C; 30 Min,60 °C; 2 H,60 °C -> 35 °C
标题:Processes For Preparation Of Zilpaterol Via Chlorination Of 4-(2-Oxo-2,3-Dihydrobenzimidazol-1-Yl)Butyric Acid Or Nitrosation Of 8,9-Dihydro-2H,7H-2,9A-Diazabenzo[cd]Azulene-1,6-Dione.
参考文献:World Intellectual Property Organization]
92260-81-6 = 92260-82-7
反应条件:1.1 Reagents: Tert-Butyl Nitrite,Hydrochloric Acid Solvents: Acetic Acid,1,4-Dioxane; 3 H,Rt
标题:Preparation Of Imidazobenzazepin-2(1H)-Ones As β2 Adrenoceptor Agonists.
参考文献:United States]
92260-81-6 = 92260-82-7
反应条件:1.1 Reagents: Tert-Butyl Nitrite,Hydrochloric Acid Solvents: Acetic Acid,1,4-Dioxane; 3 H,Rt
标题:Preparation Of Imidazo[4,5,1-Jk][1]Benzazepin-2(1H)-One Derivatives As Anabolic Agents
参考文献:World Intellectual Property Organization
📜5,6-Dihydroimidazo[4,5,1-Jk][1]Benzazepin-2,7-[1H,4H]-Dione置于盐酸,Sodium Nitrite体系中,用 水,N,N-二甲基甲酰胺 作为反应溶剂,化学反应生成 4,5-二氢-6-肟-咪唑并[4,5,1-Jk][1]苯并氮杂卓-2,6,7(1H)-三酮
参考文献: Process For Making A Crystalline Zilpaterol Salt[fr] Procédé Pour La Fabrication D'Un Sel De Zilpaterol Cristallin
标题: Process For Making A Crystalline Zilpaterol Salt[fr] Procédé Pour La Fabrication D'Un Sel De Zilpaterol Cristallin
摘要:这项发明通常涉及制备晶体硫酸盐,特别是晶体盐酸盐.该发明还涉及使用根据本发明制备的晶体硫酸盐进行治疗的方法,以增加家畜,家禽和鱼类的体重增长速度,改善饲料效率,和/或增加胴体瘦肉率.
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