CAS: 161489-05-0; 4-Iodo-6-Methoxypyrimidine

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CAS号67-56-1 甲醇 | CAS号19646-06-1 4,6-二碘嘧啶

📜甲醇,4,6-二碘嘧啶置于sodium Methylate体系中,化学反应 2.0H,以85%的收率获得4-碘-6-甲氧基嘧啶
参考文献:Use Of Hydrogen Bonds To Control Molecular Aggregation. Behavior Of Dipyridones And Pyridone-Pyrimidones Designed To Form Cyclic Triplexes
标题:Use Of Hydrogen Bonds To Control Molecular Aggregation. Behavior Of Dipyridones And Pyridone-Pyrimidones Designed To Form Cyclic Triplexes
摘要:The Tendency Of 2-Pyridones And Related Heterocycles To Form Cyclic Hydrogen-Bonded Dimers Allows Them To Be Used As Sticky Sites That Induce Molecules In Which They Are Incorporated To Associate In Particular Ways. Compound 7,Which Is Constructed From Pyridone And Pyrimidone Subunits Linked To A Rigid Linear Acetylenic Spacer,Incorporates An Array Of Hydrogen-Bonding Sites Designed To Favor The Formation Of A Cyclic Tripler. Pyridone-Pyrimidone 7 Was Synthesized And The Structure Of Its Dmso Solvate Was Determined By X-Ray Crystallography. Aggregation Does Not Produce A Cyclic Tripler But Rather Gives Chains In Which Adjacent Molecules Of Compound 7 Are Linked By Single Hydrogen Bonds.
Doi:10.1021/jo00110A050