CAS: 6342-60-5; 2-Chloro-5-Methylbenzoic Acid

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CAS号73129-52-9 2'-chloro-5-met... | CAS号106-43-4 对氯甲苯 | CAS号2941-78-8 2-氨基-5-甲基苯甲酸 | CAS号79-37-8 草酰氯 | CAS号63549-34-8 3-chloro-1-(2-c... | CAS号7697-37-2 硝酸 | CAS号89-56-5 5-甲基水杨酸 | CAS号16220-95-4 2-氯-5-甲基苯甲酸甲酯 | CAS号945262-03-3 ethyl 2-chloro-...

合成工艺路线路线简述

    2-氨基-5-甲基苯甲酸 反应生成 2-氯-5-甲基苯甲酸
    参考文献:Ultraviolet Spectra Of Substituted Acetophenones And Benzoic Acids
    标题:Ultraviolet Spectra Of Substituted Acetophenones And Benzoic Acids
    摘要:
    DOI:10.1021/jo01076A039

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    专利信息


    专利号:US-6525061-B1
    优先权日:1999-11-16
    标题 :Methods for the solid phase synthesis of 2-amino-4(H)-quinazolinone derivatives
    发明人:GOPALSAMY ARIAMALA; YANG HUI Y
    权利人:WYETH CORP
    摘要:The present invention relates to solid phase synthesis of substituted 2-amino-4(H)-quinazolinone compounds of formula (I):having pharmacological activity, to processes for their preparation, to a combinatorial library and solid phase methods for preparing libraries of the compounds, to utilizing libraries of the compounds for drug discovery, and to pharmaceutical compositions thereof.

    专利号:US-7943723-B2
    优先权日:2006-12-21
    标 题:Process for the synthesis of ethers of aromatic acids
    发明人:RITTER JOACHIM C
    权利人:DU PONT
    摘要:The inventions disclosed herein include processes for the preparation of an ether of an aromatic acid, processes for the preparation of products into which such an ether can be converted, the use of such processes, and the products obtained and obtainable by such processes. A key feature of the processes described is the use of a solvent comprising an alcohol ROH and an alcoholate RO − M + .

    专利号:US-8207374-B2
    优先权日:2006-12-21
    标 题:Process for the synthesis of ethers of aromatic acids
    发明人:RITTER JOACHIM C
    权利人:RITTER JOACHIM C; DU PONT
    摘要:Ethers of aromatic acids are produced from halogenated aromatic acids in a reaction mixture containing a copper (I) or copper (II) source and a diketone ligand that coordinates to copper.

    专利号:US-2011060118-A1
    优先权日:2009-09-02
    标 题:Process for the synthesis of fluorinated ethers of aromatic acids
    发明人:RITTER JOACHIM C; MOLOY KENNETH GENE; POLLINO JOEL M; MAHAJAN DU SURBHI
    权利人:DU PONT
    摘要:Fluorinated ethers of aromatic acids are produced from halogenated aromatic acids in a reaction mixture containing a copper (I) or copper (II) source and a Schiff base ligand that coordinates to copper. The fluorinated ethers of aromatic acids made using the process described herein can be applied to, e.g., fibers, yarns, carpets, garments, films, molded parts, paper and cardboard, stone, and tile to impart soil, water and oil resistance. By incorporating the fluorinated ethers of aromatic acids, or diesters thereof, into polymer backbones, more lasting soil, water and oil resistance, as well as improved flame retardance, can be achieved.

    专利号:US-7985825-B2
    优先权日:2006-12-21
    标 题 :Process for the synthesis of ethers of aromatic acids
    发明人:RITTER JOACHIM C
    权利人:DU PONT
    摘要:Ethers of aromatic acids are produced from halogenated aromatic acids in a reaction mixture containing a halogenated aromatic acid such as is described by the structure of Formula II n nwherein each X is independently Cl, Br or I; the reaction mixture further comprising;n (i) a polar protic solvent, a polar aprotic solvent or an alcoholic solvent containing the alcoholate RO-M+ (wherein M is Na or K), wherein the polar protic solvent, polar aprotic solvent or alcoholic solvent is either ROH or is a solvent that is less acidic than ROH; (ii) a copper (I) or copper (II) source; and (iii) an amino acid ligand that coordinates to copper, wherein the ligand comprises an amino acid in which the amine nitrogen and the carboxyl carbon are separated by no more than two carbon atoms.

    专利号:US-2011060117-A1
    优先权日:2009-09-02
    标题:Process for the synthesis of fluorinated ethers of aromatic acids
    发明人:RITTER JOACHIM C; MOLOY KENNETH GENE; POLLINO JOEL M; MAHAJAN DU SURBHI
    权利人:DU PONT
    摘要:Fluorinated ethers of aromatic acids are produced from halogenated aromatic acids in a reaction mixture containing a copper (I) or copper (II) source and a diamine ligand that coordinates to copper. The fluorinated ethers of aromatic acids made using the process described herein can be applied to, e.g., fibers, yarns, carpets, garments, films, molded parts, paper and cardboard, stone, and tile to impart soil, water and oil resistance. By incorporating the fluorinated ethers of aromatic acids, or diesters thereof, into polymer backbones, more lasting soil, water and oil resistance, as well as improved flame retardance, can be achieved.
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    合成参考文献


    参考文献:10.1107/s1600536810017393
    摘要:Samas B, Préville C, Thuma BA, Mascitti V. 2-[4-Chloro-3-(4-ethoxy-benz-yl)phen-yl]-1,3-dithiane. Acta Crystallogr Sect E Struct Rep Online. 2010 May 19;66(Pt 6):o1386.
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