CAS: 5468-75-7; 2,2'-((3,3'-Dichloro-[1,1'-Biphenyl]-4,4'-Diyl)Bis(Diazene-2,1-Diyl))Bis(3-Oxo-N-(O-Tolyl)Butanamide)

上下游产品

联苯胺黄 Pigment Yellow 13 5102-83-0

2'-甲基乙酰乙酰苯胺,3,3'-Dichloro-Biphenyl-4,4'-Bisdiazonium; Chloride置于sodium Hydroxide,溶剂黄146体系中,用 水 作为反应溶剂,化学反应 0.23H,反应生成 C.I.颜料黄14
参考文献:Production Process And System For Insoluble Azo Pigments
标题:Production Process And System For Insoluble Azo Pigments
摘要:通过将二氧化溶液和接地溶液连续喷射到喷射器中,使得在喷射器内,二氧化溶液和接地溶液相互混合并进行偶联反应,从而产生一种不溶性偶氮颜料.不溶性偶氮颜料的生产系统包括以下单元(1)至(4):(1)第一个供液罐(2),用于第一个流体,可选择为二氧化溶液或接地溶液,第一个流通路径(a),用于将第一个流体送入喷射器(1)的喷嘴,并且通过第一个流通路径供给第一个流体的泵(d);(2)喷射器(1),具有喷嘴,吸气室,扩散器和温度控制装置(g);(3)第二个供液罐(3),用于第二个流体,第二个流通路径(b),用于将第二个流体引导到吸气室,并且通过第二个流通路径(b)的流量控制装置(e)用于控制第二个流体的流速;(4)热处理罐(5),用于对由第一个流体和第二个流体反应形成的不溶性偶氮颜料的悬浮液进行热处理,以及从扩散器引导悬浮液到热处理罐的第三个流通路径(a').

专利信息

专利号:WO-2024097977-A1
优先权日:2022-11-04
标题:Silk nanoparticle synthesis: tuning size, dispersity, and surface chemistry for drug delivery
发明人：SHAIDANI SAWNAZ; FALCUCCI THOMAS; FOSTER OLIVIA; SAHOO JUGAL KISHORE; HASTURK ONUR; KAPLAN DAVID L; JACOBUS CHARLOTTE S
权利人:TUFTS COLLEGE
摘要:Methods disclosed herein relate to generating silk nanoparticles with a low polydispersity index (PDI). Methods include adding a silk solution dropwise into a volatile solvent that is miscible with water, thereby forming a precipitate-bearing solution and applying shear forces to the precipitate-bearing solution for a length of time sufficient to achieve evaporation of at least 95% of the volatile solvent, thereby producing a population of silk fibroin nanoparticles in water having a polydispersity index (PDI) of 0.35 or less, including but not limited to, a PDI of 0.330 or less, 0.325 or less, 0.315 or less, 0.310 or less, 0.30 or less, 0.275 or less, 0.250 or less, 0.225 or less, or 0.200 or less. Parameters related to silk fibroin molecular weight, silk fibroin concentration, shear force application, and temperature may all be modified to achieve silk nanoparticles of a particular size exhibiting particular PDIs.

专利号:CN-111921465-B
优先权日:2019-05-13
标题:A kind of azo pigment continuous synthesis micro-mixer and continuous preparation method thereof