CAS: 481-30-1; Epitestosterone

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CAS号36025-82-8 3-oxoandrost-4-... | CAS号58-22-0 睾酮 | CAS号51067-43-7 16,17-epoxy-4-a... | CAS号83-46-5 β-谷甾醇 | CAS号63-05-8 雄烯二酮 | CAS号897-06-3 1,4-雄烯二酮 | CAS号1425-09-8 3-oxoandrost-4-... | CAS号850848-14-5 testosterone 2-... | CAS号315-37-7 庚酸睾酮 | CAS号63-05-8 雄烯二酮

合成工艺路线路线简述

    📜睾酮置于偶氮二甲酸二异丙酯,三苯基膦,2,3-二氯-5,6-二氰基-1,4-苯醌体系中,用 四氢呋喃,二氯甲烷,水 作为反应溶剂,化学反应 31.0H,反应生成 表睾酮
    参考文献:2-(Prenyloxymethyl)Benzoyl (Pomb) Group: A New Temporary Protecting Group Removable By Intramolecular Cyclization
    标题:2-(Prenyloxymethyl)Benzoyl (Pomb) Group: A New Temporary Protecting Group Removable By Intramolecular Cyclization
    摘要:2-(Prenyloxymethyl)Benzoates Can Be Prepared From Alcohols And Readily Available 2-(Prenyloxymethyl)Benzoic Acid By Standard Acylation Techniques Or By Mitsunobu Reaction With Inversion Of Configuration. The Pomb Group Can Be Cleaved First By Oxidative Removal Of The Prenyl Group With Ddq Followed By Lactonization With Expulsion Of The Alcohol Catalyzed By Yb(Otf)(3). These Reaction Conditions Are Compatible With The Presence Of A Large Number Of Common Protecting Groups. (C) 2007 Elsevier Ltd. All Rights Reserved.
    DOI:10.1016/j.Tet.2007.08.065

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    合成参考文献


    参考文献:10.1016/j.steroids.2011.06.005
    摘要:Mazzarino M, Braganò MC, de la Torre X, Molaioni F, Botrè F. Relevance of the selective oestrogen receptor modulators tamoxifen, toremifene and clomiphene in doping field: endogenous steroids urinary profile after multiple oral doses. Steroids. 2011 Nov;76(12):1400–6. doi: 10.1016/j.steroids.2011.06.005.
    参考文献:10.1002/rcm.5117
    摘要:Lee KM, Kim HJ, Jeong ES, Yoo HH, Kwon OS, Jin C, Kim DH, Lee J. Simple and accurate quantitative analysis of seven prohibited threshold substances in human urine by liquid chromatography/tandem mass spectrometry in doping control. Rapid Commun Mass Spectrom. 2011 Aug 30;25(16):2261–7. doi: 10.1002/rcm.5117.
    参考文献:10.1016/j.cca.2011.06.028
    摘要:McDonald TJ, Perry MH, Jones AG, Donohoe M, Salzmann MB, O'Connor J. A novel case of a raised testosterone and LH in a young man. Clin Chim Acta. 2011 Oct 09;412(21-22):1999–2001. doi: 10.1016/j.cca.2011.06.028.
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