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CAS号74-83-9 溴甲烷 | CAS号75-18-3 二甲基硫 | CAS号1618-26-4 二甲硫基甲烷 | CAS号506-68-3 溴化氰 | CAS号106-93-4 1,2-二溴乙烷 | CAS号535-11-5 2-溴丙酸乙酯 | CAS号26805-54-9 3-(bromomethyl)... | CAS号67-68-5 二甲基亚砜 | CAS号105-36-2 溴乙酸乙酯 | CAS号598-72-1 2-溴丙酸 | CAS号2745-17-7 2-(oxiran-2-yl)furan | CAS号75-18-3 二甲基硫 | CAS号74-83-9 溴甲烷 | CAS号34557-54-5 methane | CAS号96-09-3 氧化苯乙烯 | CAS号125116-23-6 叶菌唑 | CAS号6388-72-3 Oxirane,2-(4-me...合成工艺路线路线简述
- 合成目标产物 Trimethylsulfonium Bromide 主要起始原料 Benzyl Bromide And Dimethyl Sulfoxide
- (文献来源)合成步骤主要原料 Benzyl Bromide 和 Dimethyl Sulfoxide
溴甲烷,二甲基硫 以 乙腈 作为反应溶剂,化学反应生成 三甲基溴化锍
参考文献:环氧化物异质固液可行性水合物:自sel结构的自发反应
标题:环氧化物异质固液可行性水合物:自sel结构的自发反应
摘要:描述了在少量水的存在下,在非均相条件下通过硫化合物插入醛中形成的环氧化物.研发了三甲基s和s-甲基硫基溴化铵和碘化物.对于所有的烷基取代基,溴化物比碘化物具有更好的结果,这是根据反应机理来解释的.在最佳条件下,可获得高收率的环氧化物.
DOI:10.1016/s0040-4020(01)81676-8
专利信息
专利号:US-2022356139-A1
优先权日:2019-09-03
标 题:Synthesis of deuterated aldehydes
发明人:WANG WEI
权利人:ARIZONA BOARD OF REGENTS ON BEHALF OF ATHE UNIV OF ARIZONA
摘要:Described are methods for preparing a deuterated aldehyde using N-heterocyclic carbene catalysts in a solvent comprising D 2 O. The methods may be used to convert a wide variety of aldehydes (e.g., aryl, alkyl, or alkenyl aldehydes) to C-1 deuterated aldehydes under mild reaction conditions without functionality manipulation.
专利号:US-8940880-B2
优先权日:2010-09-20
标 题:Process for the preparation of 9-deoxo-9a-homoerythromycin A, modified in the C-4″ of the cladinose ring by an epoxide group
发明人:GARCIA RAFAEL; MARTORELL ORIOL; CODONY ALBERT
权利人:GARCIA RAFAEL; MARTORELL ORIOL; CODONY ALBERT; NOVARTIS AG
摘要:The present invention concerns a process for the preparation of the compound of formula n n n n n n n n n n The compound of formula (1) is the key intermediate in the synthesis of some antibacterial agents of the triamilide class, such as Tulathromycin, useful to treat bacterial and protozoa infections.
专利号:US-5853555-A
优先权日:1997-04-03
标 题:Synthesis of onium hydroxides from onium salts
发明人:SHARIFIAN HOSSEIN; HULME DAVID R
权利人:SACHEM INC
摘要:The present invention provides a process for preparing onium hydroxide from a corresponding onium salt and for purifying onium hydroxide including providing an electrochemical cell containing a cathode, an anode, a divider and a bipolar membrane, the bipolar membrane having an anion selective side facing the anode and a cation selective side facing the cathode, wherein the divider is positioned between the cathode and the bipolar membrane, and the bipolar membrane is positioned between the divider and the anode, thereby defining a feed compartment between the divider and the bipolar membrane, a recovery compartment between the divider and the cathode, and a water compartment between the bipolar membrane and the anode; charging a solution containing at least one of the onium salt and the onium hydroxide to be purified to the feed compartment; charging a liquid electrolyte to the other compartments; passing a current through the electrochemical cell to produce the onium hydroxide in the recovery compartment; and recovering the onium hydroxide from the recovery compartment.
专利号:RU-2163606-C1
优先权日:1999-12-08
标题 :METHOD OF SYNTHESIS OF γ-LACTONE 3 OF (7α-ACETYLTHIO-17β-HYDROXY-3-OXOANDROST-4-ENE-17α-YL)-PROPIONIC ACID
专利号:WO-9844169-A1
优先权日:1997-04-03
标 题:Synthesis of onium hydroxides from onium salts
专利号:EP-1025281-A4
优先权日:1997-04-03
标题:SYNTHESIS OF ONIUM HYDROXIDES FROM ONIUM SALTS