CAS: 615-72-5; 3,4-Diaminophenol

该化合物是一种高纯度芳香二胺化合物,主要用作有机合成和工业应用的中间体,其主要优点包括它因其活性氨基和氢氧基功能组,在染料,药品和摄影开发者生产过程中发挥先质作用.该化合物在极地溶剂中表现出良好的溶解性,便于其在各种化学工艺中使用.纯度超过80%,它确保合成反应的性能一致,特别是在热循环和聚合化学中.由于它具有在长期接触光或空气情况下对氧化的敏感性和潜在的不稳定性,需要妥善处理.

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上下游产品

CAS号610-81-1 3-硝基-4-氨基苯酚 | CAS号577-71-9 3,4-二硝基苯酚 | CAS号861623-47-4 (4-ethoxy-2-ami... | CAS号768-10-5 苯并[c][1,2,5]噻二唑-5-醇 | CAS号156-43-4 对氨基苯乙醚 | CAS号2623-33-8 双醋氨酯 | CAS号2243-69-8 Acetamide,N-[4-... | CAS号554-84-7 3-硝基苯酚 | CAS号7647-01-0 盐酸 | CAS号7467-91-6 6-羟基喹喔啉 | CAS号91144-67-1 1H-2,1,3-benzos...

合成工艺路线路线简述

    📜N-(4-乙氧基苯基)氨基甲酸乙酯置于盐酸,Tin,硝酸体系中,化学反应生成 3,4-二氨基苯酚
    参考文献:Koehler,Journal Fur Praktische Chemie (Leipzig 1954),1884,Vol. <2>29,P. 261,263,270
    标题:Koehler,Journal Fur Praktische Chemie (Leipzig 1954),1884,Vol. <2>29,P. 261,263,270

    海关参考信息

    专利信息


    专利号:US-6251689-B1
    优先权日:1998-05-14
    标 题:Methods for the solid phase synthesis of combinatorial libraries of benzimidazoles benzoxazoles benzothiazoles and derivatives thereof
    发明人:LABORDE EDGARDO; MATSUMOTO YUKIHARU
    权利人:TELIK INC
    摘要:The present invention provides an efficient and versatile method for the synthesis and screening of combinatorial libraries of benzimidazoles, benzoxazoles, benzothiazoles, and derivatives thereof. In order to expedite the synthesis of large arrays of compounds possessing these core structures, a general methodology for solid phase synthesis of these derivatives is provided. Arrays of benzimidazoles, benzoxazoles, benzothiazoles, and derivatives thereof useful as peptidomimetics and for the identification of agents having antifungal, antiviral, antimicrobial, anticoagulant, and antiulcer activity, or use in the treatment of inflammation, hypertension, cancer, and other conditions can be prepared by this method.

    专利号:US-6051704-A
    优先权日:1996-07-22
    标题:Synthesis of macrocyclic tetraamido-N ligands
    发明人:GORDON-WYLIE SCOTT W; COLLINS TERRENCE J
    权利人:UNIV CARNEGIE MELLON
    摘要:New synthetic methods for the preparation of macrocyclic amido-N donor ligands are provided. The primary method of the present invention involves in general only two synthetic steps. In the first step, an α or β amino carboxylic acid is allowed to react with an optimal (approximately stoichiometric) amount of an activated malonate or oxalate derivative with mild heating. Upon completion of the double coupling reaction, hydrolysis of the reaction mixture yields a diamide containing intermediate (a macro linker). In the second step, stoichiometric amounts of a diamine, preferably an orthophenylene diamine, are added to the macro linker intermediate in the presence of a coupling agent and heat. This second double coupling reaction, is allowed to proceed for a period of time sufficient to produce a macrocyclic tetraamido compound. The substituent groups on the α or β amino carboxylic acid, the malonate, and the aryl diamine may all be selectively varied so that the resulting tetraamido macrocycle can be tailored to specific desired end uses. The macrocyclic tetraamide ligand may then be complexed with a metal, such as a transition metal, and preferably the middle and later transition metals, to form a robust chelate complex suitable for catalyzing oxidation reactions.

    专利号:US-10982047-B2
    优先权日:2016-09-28
    标 题 :Solvent systems for synthesis of poly(amic acid) and polyimide polymers
    发明人:KIM EUNGKYU; HARRIS WILLIAM J; JIANG QI; JIANG XIN; OHBA KAORU
    权利人:DOW GLOBAL TECHNOLOGIES LLC
    摘要:The process for synthesizing a poly(amic acid) polymer or a polyimide polymer is improved by using a solvent system consisting essentially of: (A) a first component consisting essentially of at least one of a sulfoxide, e.g., DMSO, and an alkyl phosphate, e.g., triethyl phosphate, and (B) optionally, a second component consisting essentially of at least one aprotic glycol ether, e.g., dipropylene glycol dimethyl ether.

    专利号:US-2019218344-A1
    优先权日:2016-09-28
    标题:Solvent Systems for Synthesis of Poly(Amic Acid) and Polyimide Polymers

    专利号:US-2019202989-A1
    优先权日:2016-09-28
    标 题 :DMPA-Based Solvent Systems for the Synthesis of Poly (Amic Acid) and Polyimide Polymers

    专利号:WO-2004076425-A1
    优先权日:2003-02-21
    标题:Improved synthesis of macrocyclic tetraamido compounds and new metal insertion process

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    ✅ COA系统入驻 | 共享模式

    合成参考文献


    参考文献:10.1107/s1600536809015797
    摘要:Gu Z, Cheng W. 4-Acetamido-3-nitro-phenyl acetate. Acta Crystallogr Sect E Struct Rep Online. 2009 May 07;65(Pt 6):o1194.
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