CAS: 101947-16-4; 1H,1H,2H,2H-Perfluorodecyltriethoxysilane

上下游产品

Triethoxysilane 1H,1H,2H-perfluorodecene

三乙氧基硅烷,1H,1H,2H-全氟-1-癸烯置于chloroplatinic Acid体系中,用 异丙醇 用作溶剂,化学反应 0.12H,以97.3%的收率获得1H,1H,2H,2H-全氟癸基三乙氧基硅烷
参考文献:连续性流微反应器合成氟硅化合物的方法
标题:连续性流微反应器合成氟硅化合物的方法
摘要:本发明属于含氟材料技术领域,具体涉及一种连续性流微反应器合成氟硅化合物的方法.所述的合成方法,以连续性流微反应器为反应装置,包括以下步骤:1)将氟代烯烃通过物料通道a,烷氧基硅烷通过物料通道b,溶于有机溶剂的催化剂通过物料通道c分别经计量泵p1,P2和p3流入预设温度为t的混合反应模块m内进行混合反应;2)待混合反应结束后,反应液从出口d流出,对流出的反应液进行后处理,得到氟硅化合物.本发明提供的合成方法,科学合理,简单易行,能够克服现有的氯硅烷硅氢加成中存在的放热剧烈,操作控制难,设备要求苛刻,收率低,反应时间长等问题.

专利信息

专利号:US-7803959-B2
优先权日:2006-04-05
标 题 :Synthesis of aromatic silicon-containing compounds
发明人：COGGAN JENNIFER A; BENDER TIMOTHY P; TOTH ALAN EDWARD JOHN
权利人:XEROX CORP
摘要:Methods are provided for preparing aromatic silicon-containing compounds. The methods include providing an aromatic starting material; reacting the aromatic starting material with a base to form an aromatic salt; and reacting the aromatic salt with a halo-alkylene-silane to form an aromatic silicon-containing compound. Compositions prepared by these methods, protective layers that include hydrolysis and condensation products of such compositions, electrophotographic photoreceptors that include such protective layers, and image forming apparatuses that include such electrophotographic photoreceptors are also provided. In addition, method for preparing electrophotographic photoreceptors that include protective layers including hydrolysis and condensation products of aromatic silicon-containing compounds prepared by the methods for preparing aromatic silicon-containing compounds are provided.

专利号:US-7432031-B2
优先权日:2005-03-22
标 题:Toner for electrostatic charge developing, production method thereof, developer for electrostatic charge developing using the same, and image forming method
发明人：MIZUTANI NORIYUKI; MAEHATA HIDEO; HAMANO HIROKAZU; TANAKA HIROYUKI; KITAGAWA SOICHIRO; IGUCHI MOEGI
权利人:FUJI XEROX CO LTD
摘要:A toner for electrostatic charge developing prepared by a production method including aggregating one or more kind of particles in a raw material dispersion including the particles to form aggregated particles, and coalescing the aggregated particles by heating. At least one kind of the particles is resin particles including an amorphous polyester resin synthesized by copolymerizing one or more polyvalent carboxylic acids and two or more polyhydric alcohols; at least one of the polyvalent carboxylic acids is polyvalent carboxylic acid having a sulfonic acid group; two of the polyhydric alcohols are an ethylene oxide adduct of bisphenol A and a propylene oxide adduct of bisphenol A; and the following equation is satisfied:n n10/90≦ BPA ( EO )/ BPA ( PO )≦90/10.n n In the equation, BPA(EO) represents a total mole amount of the ethylene oxide adduct of bisphenol A used in synthesis of the amorphous polyester resin, and BPA(PO) represents a total mole amount of the propylene oxide adduct of bisphenol A used in synthesis of the amorphous polyester resin.

专利号:US-6177534-B1
优先权日:1997-12-23
标题 :Silylated resins and the synthesis thereof
发明人：ANTONUCCI JOSEPH M; STANSBURY JEFFREY W; FOWLER BRUCE O
权利人:US COMMERCE
摘要:A silylated resin suitable for use as an adhesive binder for composites and in sealant and adhesive dental applications is represented by the general formula (I): n in which: n R 1 is an aliphatic, cycloaliphatic, aryl, hydrocarbon, or fluorocarbon group; n R 2 is the same as R 1 or a different aliphatic, cycloaliphatic, aryl, hydrocarbon, or fluorocarbon group; n M 2 is the same as M 1 or a different functional or nonfunctional group selected from the group consisting of: n n is 1-3; n x is 1-20; and n y is 1-20; n which comprises the reaction product of the exchange reaction of a hydroxylated, aminated, or carboxylated acrylic resin represented by the general formula (II): n in which: n R 4 is an aliphatic, cycloaliphatic, aryl, hydrocarbon, or fluorocarbon group with one or more protic functional groups selected from the group consisting of: n n n OH, N—H, and CO 2 H n n n R 5 is H or CH 3 ; and n R 6 is H or CH 3 ; n with a trialkoxyorganosilane or triacyloxyorganosilane represented by the general formula (III): n in which: n R 7 , R 8 , and R 9 each is: n R 10 is an aliphatic, or aryl group which can optionally be substituted with a group from the group of an acrylic group, a methacrylic group, an epoxy group, and a substituted amino, hydroxyl, or carboxylic acid group such as an ester or an amide.

专利号:US-7576240-B2
优先权日:2006-04-26
标 题 :Arylamine processes
发明人：MURPHY LEANNE DAWN
权利人:XEROX CORP
摘要:Processes for selectively hydrogenating double and/or triple bonds in organic molecules include providing at least one organic molecule containing a double and/or triple bond, providing at least one hydrogen donor molecule, and hydrogenating the double and/or triple bond in the presence of at least one catalyst. Processes for preparing arylamine molecules include selectively hydrogenating double bonds in arylamine compounds by providing at least one organic molecule containing a multiple bond, providing at least one hydrogen donor molecule, and hydrogenating the multiple bond in the presence of at least one catalyst. The processes provide efficient, cost-effective and safe methods for conducting selective hydrogenation reactions in the synthesis of organic molecules, such as charge-transport molecules.

专利号:US-2004035690-A1
优先权日:1998-02-11
标题 :Method and apparatus for chemical and biochemical reactions using photo-generated reagents
发明人：GULARI ERDOGAN
权利人:UNIV MICHIGAN
摘要:This invention provides method and apparatus for performing chemical and biochemical reactions in solution using in situ generated photo-products as reagent or co-reagent. Specifically, the method and apparatus of the present invention have applications in parallel synthesis of molecular sequence arrays on solid surfaces.

专利号:WO-2019218027-A1
优先权日:2018-05-18
标题:Core-shell particles
发明人：MEANEY SHANE; TABOR RICHARD; FOLLINK BART
权利人:UNIV MONASH
摘要:The application relates to a core-shell particle having a) a cross-linked polyelectrolyte core, and b) a silica-based shell having covalently bound thereto one or more groups of formula –R–F, wherein R is an organic group and F is a functional moiety. The application also relates to a method of synthesis of a core-shell particle, the method comprising the steps of: a) providing a cross-linked polyelectrolyte core template, b) coating the core template with a silica-based shell, and c) introducing one or more groups of formula –R–F covalently bound to the silica-based shell, wherein R is an organic group and F is a functional moiety.