📜2,4-二硝基酚,草酰氯 以 二氯甲烷 用作溶剂,化学反应 0.67H,反应生成双(2,4-二硝基苯基)草酸酯 参考文献:An Optimised Procedure For Ptfe Phase Vanishing Reactions: An Improved Reaction Design And The Use Of Reagents Adsorbed On Silica 标题:An Optimised Procedure For Ptfe Phase Vanishing Reactions: An Improved Reaction Design And The Use Of Reagents Adsorbed On Silica 摘要:虽然相消 (Pv)-聚四氟乙烯反应设计在多种基质和反应条件下都能很好地进行,但偶尔也会出现问题.本文讨论了这些问题及其重要性,包括它们对反应结果的影响以及解决这些问题的方法.此外,还介绍了一种改进设计的细节,即以前报道过的 Pv-Ptfe 和无溶剂 Pv-Ptfe 混合设计,以及二氧化硅支撑试剂的使用. Doi:10.3184/174751915X14416158938073
专利号:US-7384739-B2 优先权日:2001-11-14 标题 :Compositions for enhancing DNA synthesis, DNA polymerase-related factors and utilization thereof 发明人:KITABAYASHI MASAO; KUROITA TOSHIHIRO; ISHIDA YOSHIKAZU; KOMATSUBARA HIDEYUKI; NISHIYA YOSHIAKI; OKA MASANORI; KAWAMURA YOSHIHISA; IMANAKA TADAYUKI 权利人:TOYO BOSEKI 摘要:The invention provides methods, kits, and compositions for enhancing synthesis of DNA involving a carboxylate ion-supplying substance that is effective in promoting DNA synthesis in enzymatic DNA synthesis reactions. The invention further provides a thermostable DNA polymerase-related factor derived from Thermococcus species, which has an activity to promote the DNA synthesis activity of DNA polymerase or which binds to DNA polymerase.
专利号:WO-9102040-A1 优先权日:1989-08-04 标 题:Cyclodextrin labels for nucleic acid and biochemical analysis 发明人:KOSAK KENNETH M 权利人:KOSAK KENNETH M 摘要:This invention provides a method of qualitative and quantitative nucleic acid sequence analysis using luminescent cyclodextrin (CD), labels for dideoxy-nucleotide chain terminators and oligonucleotide primers. The CD labels are nonradioactive and detected in a ''black'' background, avoiding problems of fluorescence and allowing more sensitivity. Through formation of inclusion complexes with various fluorophores, the CD labels provide the versatility of different colored labels, with potentially higher signal efficiency in aqueous solutions. The CD labels have similar structures and thereby provide simplicity of synthesis and use, with more uniform chemical/physical properties, even with different colored labels. The invention is intended for high volume nucleic sequencing employing photomultipliers or charge-coupled device cameras for detection. Through the combination of these features, this invention provides advantages of speed, sensitivity, simplicity and versatility previously unknown or suggested in the art of nucleic acid sequence analysis.
专利号:US-2010089271-A1 优先权日:2007-02-19 标题:Novel explosives 发明人:COLCLOUGH MARTIN E; HASKINS PETER J; MILLAR ROSS W; SAGE IAN C 权利人:COLCLOUGH MARTIN E; HASKINS PETER J; MILLAR ROSS W; SAGE IAN C 摘要:This invention relates to the field of novel explosives, compositions and munitions comprising the same, as well as methods of synthesis and their use. The invention particularly relates to the field of explosives which are switchable between two different liquid crystalline states, and which possesses a general formula below. n n n n n n n n n n wherein M is a mesogenic core, R 1 and R 2 are independently selected terminal end groups attached to the mesogenic core, and wherein the mesogenic core contains sufficient (NO 2 ) x to provide an explosive output. The explosive compound may form part of an explosive composition, which may be used as a high explosive fill for any part of a munition. The explosive composition may contain other components such as non-explosive LC compounds, or binders, or further known explosive compounds. The explosive composition has one or more liquid crystalline states, which may possess differing sensitivities
参考文献:10.1007/978-3-642-72544-9_12 摘要:Eberson L. Applications of Outer-sphere Electron Transfer. 1987. In: Reactivity and Structure Concepts in Organic Chemistry. 参考文献:10.1007/978-3-658-41568-6_8 参考文献:10.1007/s40242-024-4166-6 摘要:Chen Y, Budianta R, Ning Y. Near-infrared Emissive 1,2-Dioxetane-based Chemiluminescent Probes. Chem. Res. Chin. Univ. 2024 Sep 12;40(5):806–23. doi: 10.1007/s40242-024-4166-6.