CAS: 12011-67-5; Iron Carbide(Fe3C)

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合成工艺路线路线简述

    📜二茂铁置于双氧水体系中,用 丙酮 用作溶剂,化学反应 49.0H,反应生成碳化铁
    参考文献:Effect Of Annealing Temperature On The Structure Of Carbon Encapsulated Fe3O4 Nanospheres
    标题:Effect Of Annealing Temperature On The Structure Of Carbon Encapsulated Fe3O4 Nanospheres
    摘要:在600oc下获得了核壳结构的fe3O4@c.阐述了核壳向核壳结构fe3O4@c的可能演化机制.
    Doi:10.1039/c5Ra19326E

    专利信息


    专利号:US-2023159337-A1
    优先权日:2021-11-19
    标题:Synthesis of uniform diamond nanoparticles
    发明人:YAN HAO; LYU TENGTENG
    权利人:UNIV NORTH TEXAS
    摘要:The synthesis of sub-five-nanometer nanodiamonds with high uniformity and purity. Inspired by the formation of natural diamond, iron carbide nanoparticles embedded in iron oxide matrices as the carbon source were used. High-pressure-high-temperature treatment of the precursor yields nanodiamonds with tunable diameters down to 2.13 nm and 0.22-nm standard deviation. The disclosed synthesis procedures also include a method for forming fluorescent nanodiamonds.

    专利号:US-11760636-B2
    优先权日:2018-10-26
    标 题 :Vacuum-free, hydrogen-free catalytic synthesis of graphene from solid hydrocarbons
    发明人:RAMSURN HEMA; KUNDU RAHUL
    权利人:THE UNIV OF TULSA
    摘要:Disclosed is a process for producing graphene from solid hydrocarbons including biomass and coal. The disclosed method does not require the presence of hydrogen and does not operate under a vacuum. The method begins by converting biomass to a graphene precursor while coal is used as is. Subsequently, the method grinds the graphene precursor to provide a desired particle size. The particles of graphene precursor (biocoal or coal) are converted to graphene by catalytic conversion on metallic foil under atmospheric conditions and in the absence of hydrogen.

    专利号:US-7273509-B1
    优先权日:2001-12-10
    标 题 :Synthesis of metal nanoparticle compositions from metallic and ethynyl compounds
    发明人:KELLER TEDDY M; QADRI SYED B
    权利人:US OF AMERICA AS OF OF AMERICA
    摘要:A process of making metal nanoparticles comprising the steps of: providing a precursor composition comprising at least one metallic compound and at least one organic compound; wherein the organic compound is selected from the group consisting of an ethynyl compound, a metal-ethynyl complex, and combinations thereof; wherein the precursor composition is a liquid or a solid at room temperature; and heating the precursor composition under conditions effective to produce metal nanoparticles. A metal nanoparticle composition comprising metal nanoparticles dispersed homogenously in a matrix selected from the group consisting of ethynyl polymer, crosslinked ethynyl polymer, amorphous carbon, carbon nanotubes, carbon nanoparticles, graphite, and combinations thereof.

    专利号:WO-2025133656-A1
    优先权日:2023-12-21
    标题 :Synthesis and use of tuned precatalyst for carbon-monoxide and carbon-dioxide based fischer-tropsch catalyst for controlled product distribution
    发明人:SÃ?PI ANDRÃ?S; NAJARI SARA; KÓNYA ZOLTÃ?N; KUKOVECZ Ã?KOS; SAEIDE SAMRAND
    权利人:UNIV SZEGEDI
    摘要:The present invention belongs to the technical field of design and synthesis of carbon-monoxide and carbon-dioxide-based Fischer-Tropsch synthesis catalysts, and discloses a novel iron-based Fischer-Tropsch synthesis catalyst containing both iron and carbon and a synthesis method and use thereof. The present invention specifically relates to a catalyst mixture for use in hydrogenation of CO and/or CO2, which catalyst mixture comprises i) iron oxide promoted by alkali metal, alkaline earth metal or transition metal, and ii) iron carbide. The invention further relates to a method for production of iron carbide composite comprising different iron carbides, and the use of said carbide composite in combination with alkali metal, alkaline earth metal or transition metal promoted iron oxide for use in hydrogenation of CO and/or CO2.

    专利号:US-2024097109-A1
    优先权日:2021-02-11
    标 题:Bottom-Up, Scalable Synthesis Of Oxide-Based Sub-Nano And Nanofilaments And Nanofilament-Based Two-Dimensional Flakes And Mesoporous Powders
    发明人:BARSOUM MICHEL W; BADR HUSSEIN OSAMA
    权利人:UNIV DREXEL
    摘要:Provided are methods to convert—through a bottom-up approach—binary and ternary titanium carbides, nitrides, borides, phosphides, aluminides, and silicides into lepidocrocitic nanofilaments that in some cases self-assemble into 2D flakes by immersing them in a quaternary ammonium solution at moderate temperatures. The resulting flakes can comprise nanofilaments in cross-section, some of which nanofilaments can be few microns long in some instances.

    专利号:WO-2022174264-A1
    优先权日:2021-02-11
    标题:Bottom-up, scalable synthesis of oxide-based sub-nano and nanofilaments and nanofilament-based two-dimensional flakes and mesoporous powders
    发明人:BADR HUSSEIN O; BARSOUM MICHEL W
    权利人:UNIV DREXEL
    摘要:Provided are methods to convert - through a bottom-up approach – binary and ternary titanium carbides, nitrides, borides, phosphides, aluminides, and silicides into nanofilaments that in some cases self-assemble into 2D flakes by immersing them in a quaternary ammonium solution at moderate temperatures. The resulting flakes can be C-containing anatase-based layers that are in turn comprised of nanofilaments in cross-section, some of which nanofilaments can be few microns long in some instances. Electrodes made from these materials performed well in energy systems. The materials also reduce the viability of some cancer cells. Also provided are mesoporous materials, devices, and related methods.

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