CAS: 5470-49-5; 4-(Methylsulfonyl)Aniline

上下游产品

CAS号2976-30-9 1-(甲磺酰)-4-硝基苯 | CAS号104-96-1 4-氨基茴香硫醚 | CAS号98-57-7 4-氯苯基甲基砜 | CAS号22821-80-3 4'-甲基磺酰乙酰苯胺 | CAS号20277-69-4 甲烷亚磺酸钠 | CAS号106-40-1 对溴苯胺 | CAS号540-37-4 对碘苯胺 | CAS号701-57-5 4-硝基茴香硫醚 | CAS号3466-32-8 4-溴苯甲砜 | CAS号710-24-7 对乙酰氨基苯亚磺酸 | CAS号4052-30-6 4-甲砜基苯甲酸 | CAS号4393-16-2 4-甲砜基苄胺 | CAS号189500-91-2 2-(4-fluorophen... | CAS号29209-05-0 2-Methyl-N-[4-(... | CAS号82964-91-8 4-甲基磺酰苯磺酰氯 | CAS号80866-96-2 2,6-二氯-4-(甲基磺酰基)苯胺 | CAS号722-27-0 4,4'-二硫代二苯胺 | CAS号5345-30-2 (2E)-3-[4-(甲基磺酰... | CAS号5398-77-6 对甲砜基苯甲醛 | CAS号15863-56-6 1-isothi°Cyanat...

4-硝基苯硫醇置于palladium 10% On Activated Carbon 氢气,间氯过氧苯甲酸体系中,用 甲醇,二氯甲烷 作为反应溶剂,化学反应 2.0H,反应生成 4-甲磺酰基苯胺
参考文献:Wo2006/123145
标题:Wo2006/123145

专利信息

专利号:US-6590119-B2
优先权日:1999-06-11
标题 :Methods for the synthesis of dioxoalkanoic acid compounds
发明人：FERRO MICHAEL P; MCCOY KATHLEEN A
权利人:ORTHO MCNEIL PHARM INC
摘要:The invention relates to improved methods of producing aryl dioxoalkanoic acid compounds and derivatives useful as intermediates for diarylpyrrole therapeutic agents by the alcoholysis of benzoylcyclohexanone ketal compounds.

专利号:WO-2023035571-A1
优先权日:2021-09-10
标 题:Synthesis method for esaxerenone and intermediate thereof
发明人：RUAN JING; ZHANG XINXIN; YAN GONGCHAO; RUAN XIAONA; ZHANG WEI
权利人:SHANGHAI DINGYA PHARMACEUTICAL CHEMICALS CO LTD
摘要:Provided is a new synthesis method for an intermediate of esaxerenone. The method comprises: (1) reacting 2-(trifluoromethyl)phenylacetic acid as a raw material with ethyl chloroformate or isobutyl chloroformate in an inert solvent in the presence of an alkali to produce a mixed anhydride, then reacting same with ammonia to obtain a corresponding amide compound of formula II; (2) subjecting the amide compound of formula II obtained in step (1) to a dehydration reaction in the presence of a dehydrating agent and an acid-binding agent to obtain an isocyanide compound of formula III; and (3) subjecting the isocyanide compound of formula III obtained in step (2) to a cyclization reaction with ethyl 2-butynonate in the presence of an alkali and a metal catalyst to form a pyrrole ring compound of formula IV; and the reaction equation is shown below: Compared to the prior art, the technical solution of the present invention has the advantages of a high yield, a simple post-treatment, low costs and easy industrialization, etc.

专利号:US-4719053-A
优先权日:1980-08-01
标题 :Beta-chloroethylsulfonylmethyl-benzoic halides as intermediates
发明人：SCHLAEFER LUDWIG; HAEHNLE REINHARD
权利人:HOECHST AG
摘要:New beta -chloroethylsuflonylmethyl-benzoic acid halides which can serve as fibre-reactive anchors for thesynthesis of novel organic, water-soluble compounds, preferably dyestuffs, having fibre-reactive and fibre-finishing properties, such as preferably dyestuff properties, and containing, as a fibre-reactive group, one or two beta -chloroethylsufonylmethylbenzoic acid amide groups. For the synthesis of these novel fibre-finishing compounds, said new beta -chloroethylsulfonylmethyl-benzoic acid halide compounds are reacted with an organic, water-soluble compound having fibre-finishing properties and continuing one or two amino groups. Also precursors of the fibre-finishing, fibre-reactive compounds, containing said beta -chloroethylsulfonylmethyl-benzxoic acid amid grouping, can be employed for their synthesis. The novel fibre-finishing compounds can be applied onto suitable fibre materials, such as especially cellulose fibre material and natural or synthetic polyamide fibre materials, and fixed on these fibre materials in a manner similar to application and fixation methods usual in the technique for fibre-reactive compounds. The fibre-finished material, such as dyed material, shows very good wet fastnesses.

专利号:US-2007060558-A1
优先权日:2004-07-30
标 题 :Hybrid molecules QA where Q is an aminoquinoline and A is an antibiotic residue, the synthesis and uses thereof as antibacterial agents
发明人：SANCHEZ MURIEL; MEUNIER BERNARD
权利人:CENTRE NAT RECH SCIENT
摘要:The invention concerns an aminoquinoline-antibiotic hybrid compound of general formula (I): Q—(Y 1 ) p —(U) p —(Y 2 ) p -A: wherein Q represents an aminoquinoline, (Y 1 ) p (U) p —(Y 2 ) p″ is an optional spacer and A is an antibiotic residue. The invention enables the antibiotic residue activity to be unexpectedly enhanced.

专利号:US-4257942-A
优先权日:1977-10-06
标题:New water-insoluble azo dyes
发明人：DEFEO FRANCESCO; CIPOLLI ROBERTO
权利人:ACNA
摘要:The present invention relates to the synthesis of new dyes having the following general formula: wherein: D is the residue of a diazotizable component of the carbocyclic or heterocyclic series X is an ethylene group, optionally substituted by halogen-methyl, alkyl C1-C4, aryl, aralkyl or CH2OCO(HN)nR (wherein R and n have the meanings hereinafter defined); R is alkyl C1-C8 optionally substituted by halogen, CN,COOH; aryl optionally substituted by one or more atoms of halogen, alkyl C1-C4, alkoxyl C1-C4; alkoxyl C1-C4; alkoxyl C1-C8; Aryloxy; aralkoxy; cycloalkoxy; aralkyl; naphthyl optionally substituted by halogen; alkenyl C2-C8, optionally substituted by halogen, CN, COOH; R1 and R2, either like or unlike each other, may be alkyl C1-C4 optionally substituted by halogen or CN groups; aralkyl; R3 is H; halogen, alkyl C1-C4; alkoxyl C1-C4, optionally substituted. n is 0 or 1.

专利号:US-4740604-A
优先权日:1986-05-26
标题:Benzanthrone lactones
发明人：WEIS CLAUS D; SUTTER PETER
权利人:CIBA GEIGY CORP
摘要:There are disclosed benzanthrone lactones of formula ##STR1## wherein R 1 , R 2 and R 3 are as defined in claim 1. The benzanthrone lactones of formula (1) are important intermediates for the synthesis of novel dyes which are obtained by coupling suitable diazo components to said compounds of formula (1).