CAS: 6068-72-0; 4-Cyanobenzoyl Chloride

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CAS号619-65-8 对氰基苯甲酸 | CAS号75-44-5 光气 | CAS号1877-72-1 3-氰基苯甲酸 | CAS号34241-39-9 2-(2-cyanopropa... | CAS号105-07-7 对氰基苯甲醛 | CAS号79-37-8 草酰氯 | CAS号874-89-5 羟甲基 | CAS号874-86-2 4-氰基苄氯 | CAS号107676-58-4 N-(4-CYANOPHENY... | CAS号49744-93-6 3-氧代-3-对氰基苯基丙酸乙酯 | CAS号143330-23-8 4-[(4-氰基苯甲酰基)氨基]苯甲酸 | CAS号452929-54-3 4-溴-4'-氰基二苯甲酮 | CAS号17930-02-8 2-(4-氰基苯基)苯并噻唑 | CAS号2246-51-7 (4-cyanobenzoyl... | CAS号18693-97-5 4-cyano-benzoic... | CAS号623-03-0 对氯苯腈 | CAS号873-74-5 对氨基苯腈 | CAS号24167-50-8 4-氰基-N,N-二甲基苯甲酰胺

对氰基苯甲酸置于氯化亚砜体系中,用 苯 作为反应溶剂,化学反应 1.5H,反应生成 对氰基苯甲酰氯
参考文献:(E)-2,3-Dihydro-2-(R-Phenylacylidene)-1,3,3-Trimethyl-1H-Indole (R = 4-Cn,4-Cl) 的晶体结构
标题:(E)-2,3-Dihydro-2-(R-Phenylacylidene)-1,3,3-Trimethyl-1H-Indole (R = 4-Cn,4-Cl) 的晶体结构
摘要:两种新的 1,3,3-Trimethyl-2-Methylene-2,3-Dyhidro-1H-Indole 衍生物,(E)-2,3-Dihydro-2-(4-Cyanophenylacylidene)-1,3,3-Trimethyl-1H-吲哚,(I) 和 (E)-2,3-二氢-2-(4-氯苯亚基)-1,3,3-三甲基-1H-吲哚,(II),已经合成,并且它们的晶体结构由单晶 X 射线衍射确定.(I),C20H18N2O,在单斜空间群 P21/c 中结晶,晶胞参数 A = 9.882 (3),B = 15.614(4),C = 11.181(3) å,β = 106.691(4)°,Z = 4. (II),C19H18Cl No,在单斜空间群中结晶,P21/n,晶胞参数 A = 14.6722(19),B = 7.2597(9),C = 16.304(2) å
DOI:10.1007/s10870-010-9954-9

专利信息

专利号:US-6608196-B2
优先权日:2001-05-03
标题 :Process for solid supported synthesis of pyruvate-derived compounds
发明人：WANG BING; JANAGANI SATYANARAYANA; CALLAWAY WYETH B; SESSLER JONATHAN L
权利人:GALILEO PHARMACEUTICALS INC
摘要:Provided are processes for synthesizing structurally diverse pyruvate-derived compounds using a parallel approach on a solid phase support. Examples of such a solid phase support include resins which have also been used in solid phase peptide synthesis.

专利号:US-7361773-B2
优先权日:2002-03-12
标题 :Preparation of N1-(2'-pyridyl)-1,2-propanediamine sulfamic acid and its use in the synthesis of biologically active piperazines
发明人：CHAN ANITA WAI-YIN; FEIGELSON GREGG BRIAN; ZELDIS JOSEPH; JIRKOVSKY IVO LADISLAV
权利人:WYETH CORP
摘要:A process for making a compound of the formula comprising dialkylating a benzodioxane aniline

专利号:US-6784294-B2
优先权日:2002-03-12
标题 :Preparation of N1-(2′-pyridyl)-1,2-propanediamine sulfamic acid and its use in the synthesis of biologically active piperazines
发明人：CHAN ANITA WAI-YIN; FEIGELSON GREGG BRIAN; ZELDIS JOSEPH; JIRKOVSKY IVO
权利人:WYETH CORP
摘要:A process for making an N1-(2′-pyridyl)-1,2-alkanediamine sulfamic acid of formula II by reacting a compound of formula I with NH 2 R′ n wherein R and R′ are as defined in the specification. The invention also includes the compound of formula II, and optical isomers thereof. The compound of formula II is an intermediate useful for making chiral piperazine derivatives which are active at the 5-HT 1A receptor.

专利号:JP-2005526088-A
优先权日:2002-03-12
标 题 :Synthesis of N1- (2'-pyridyl) -1,2-alkanediaminesulfamic acid and its use in the synthesis of biologically active piperazine

专利号:JP-4397693-B2
优先权日:2002-03-12
标题 :Synthesis of N1- (2'-pyridyl) -1,2-alkanediaminesulfamic acid and its use in the synthesis of biologically active piperazine

专利号:US-2003204087-A1
优先权日:2002-03-12
标 题:Preparation of N1-(2'-pyridyl)-1,2-propanediamine sulfamic acid and its use in the synthesis of biologically active piperazines