专利号:EP-4008687-A1 优先权日:2020-12-02 标 题:A method for the large scale synthesis of metal oxide nanosheets, and their uses 发明人:VINCENT MEWIN; ETACHERI VINODKUMAR 权利人:FUNDACION IMDEA MAT 摘要:The present invention relates to a rapid, scalable and inexpensive method for the synthesis of metal oxide nanosheets; the uses of the metal oxide nanosheets as electrode active materials and as catalyst; an electrode comprising the metal oxide nanosheets, a process for producing the electrode, a cell comprising the electrode and an energy storage and/or delivery system.
专利号:US-4393241-A 优先权日:1982-02-01 标 题 :Synthesis of alkoxy and phenoxy substituted aryl sulfides 发明人:HANSON HARRY T; SAPP JR JOHN B 权利人:CELANESE CORP 摘要:Provided is a novel process for the synthesis of aryl sulfides substituted with an alkoxy or phenoxy substituent. The process comprises reacting an alkoxy or phenoxy substituted aromatic compound with a sulfur dihalide, preferably sulfur dichloride, in the presence of an alkali metal tetrafluoroborate catalyst, with the amount of said aromatic reactant compound preferably being sufficient to solvate the sulfur dichloride and catalyst sufficiently to allow the reaction to occur.
专利号:US-2024150177-A1 优先权日:2022-11-07 标题 :Synthesis of cathode material for lithium battery 发明人:SHAKOOR ABDUL; NISAR UMAIR; QURESHI ZAWAR; ABRAHAM JEFFIN; ABDUL QUDDUS KHADIJA MUHAMMAD; ALQARADAWI SIHAM; KAHRAMAN RAMAZAN 权利人:QATAR FOUND EDUCATION SCIENCE & COMMUNITY DEV; UNIV QATAR 摘要:A synthesis method of cathode material for lithium battery is provided. The method includes dissolving lithium, nickel and cobalt acetate in a solution, adding ammonium dihydrogen phosphate to the solution, adding acid to the solution, heating the solution to a first temperature for a first period of time to form a solid mixer material, and sintering the solid mixer material at a second temperature for a second period of time.
专利号:US-3978140-A 优先权日:1974-09-23 标题 :Process for the preparation of carbinols 发明人:LANE CLINTON FISHER; MYATT HAL LESLIE 权利人:ALDRICH BORANES INC 摘要:Organic compounds containing a carboxylic acid or carboxylic acid anhydride group are reduced when contacted with an alkali metal borohydride and a boron trihalide in a liquid medium in which diborane is soluble in the form of a labile borane adduct. Hydrolysis of the reaction mixture then provides a useful synthesis of the corresponding carbinols. n The alkali metal borohydride-boron trihalide reagent may either be preformed and reacted subsequently with an organic compound containing a carboxylic acid or anhydride group, or the alkali metal borohydride-boron trihalide reagent may be produced in the presence of an organic compound containing a carboxylic acid or anhydride group. This development makes it possible to synthesize a wide variety of carbinols which are valuable and useful intermediates in organic synthesis.
专利号:US-2004137327-A1 优先权日:2003-01-13 标题:Synthesis of carbon/silicon composites 发明人:GROSS KARL J; WANG JAMES C F; ROBERTS GREGORY A 摘要:The present embodiment relates to a method for preparing a composite graphite-silicon negative electrode material whereby an essentially dry mixture of graphite carbon powder and an element or elements selected from the new IUPAC Group Number 12-15 of the Periodic Table of Elements that can form alloys or compounds with lithium is prepared to provide an electrochemically active mixture. A mechanical agitation process serves to mix the constituent materials and to produce a fine dispersion with intimate contact between graphite and the Group 12-15 materials. A lithium ion battery negative electrode of this composition takes synergistic advantage of the high lithium capacity of some IUPAC Group materials and the long cycle-life of graphite negative electrode materials.
专利号:US-12077559-B2 优先权日:2018-10-22 标题 :Process for the preparation of 3α-hydroxy-5α-pregnan-20-one (brexanolone) 发明人:DELFRATE CLAUDIO; RIGAMONTI DAVIDE; BORELLI TEA; LENNA ROBERTO 权利人:IND CHIMICA SRL 摘要:The present invention relates to a new process for the synthesis of 3α-hydroxy-5α-pregnan-20-one, commonly known as brexanolone, wherein the corresponding cyclic 20-ketal or cyclic 20-thioketal compound of formula (IV) is deprotected with the use or iodine in an organic solvent: (I).
[参考文献]: Takahiro Ichikawa, Et Al. 3D Interconnected Ionic Nano-Channels Formed In Polymer Films: Self-Organization And Polymerization Of Thermotropic Bicontinuous Cubic Liquid Crystals. J Am Chem Soc. 2011 Feb 23;133(7):2163-9.
合成参考文献
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