CAS: 509-77-3; 3,3-Bis(4-Aminophenyl)Isobenzofuran-1-(3H)-One
- 英文名称3,3-Bis(4-Aminophenyl)Isobenzofuran-1-(3H)-One
- 中文名称3,3-二(4-氨基苯基)苯酞
- 其它别名Phthalide,3,3-bis(p-aminophenyl)- (7CI,8CI); 3,3-Bis(4-aminophenyl)phthalide; 3,3-Bis(p-aminophenyl)phthalide; 4,4'-Phthalidylidenedianiline; Anilinephthalein; Bis(4'-aminophenyl)phthalide
- CAS编号509-77-3
- EINECS号:208-105-5
- FDA UNII编号:CYN5889K4F
- 分子式:C20H16N2O2分子量:316.35
- 产品CID: 1498312
- 产品分类有机原料 → 有机杂环化合物 → 苯并呋喃
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上下游产品
3,3-Bis(4-(Trifluoromethylsulfonyloxy)Phenyl)-1(3H)-Isobenzofuranone 1140964-66-4合成工艺路线路线简述
📜3,3-Bis(4-(Trifluoromethylsulfonyloxy)Phenyl)-1(3H)-Isobenzofuranone置于二氯双(三邻甲苯膦)合钯(II),烟酰胺,Caesium Carbonate,R-(+)-1,1'-联萘-2,2'-双二苯膦体系中,化学反应 16.0H,以44%的收率获得产物3,3-二(4-氨基苯基)苯酞
参考文献:Direct Synthesis Of Primary Arylamines Via C-n Cross-Coupling Of Aryl Bromides And Triflates With Amides
标题:Direct Synthesis Of Primary Arylamines Via C-n Cross-Coupling Of Aryl Bromides And Triflates With Amides
摘要:Aryl Halides And Triflates Are Coupled With Primary Amides To Give The Corresponding Arylamines In The Presence Of A Palladium Catalyst,A Suitable Ligand,And A Base. The Catalyst System Performs Well For A Large Number Of Different Substrates At 100-150 Degrees C Without Solvent,And With Low Catalyst Levels (0.12 Mol% Pd). Nicotinamide Might Be Useful As A Nitrogen Source In The Pd-Catalyzed Amination Reaction. (C) 2009 Elsevier Ltd. All Rights Reserved.
DOI:10.1016/j.Tet.2009.01.033
海关参考信息
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2912110000-甲醛
2912210000-苯甲醛
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合成参考文献
参考文献:10.1016/j.bbrc.2023.08.050
摘要:Ikeda Y, Davis MI, Sumita K, Zheng Y, Kofuji S, Sasaki M, Hirota Y, Pragani R, Shen M, Boxer MB, Takeuchi K, Senda T, Simeonov A, Sasaki AT. Multimodal action of KRP203 on phosphoinositide kinases in vitro and in cells. Biochemical and Biophysical Research Communications. 2023 Oct;679():116–21. doi: 10.1016/j.bbrc.2023.08.050.
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