均三甲苯置于聚合甲醛,乌洛托品,溴体系中,用 水 作为反应溶剂,化学反应生成 3,5-二甲基苯甲醛 参考文献:含甲基或氟取代基的溴代五芳基环戊二烯的简便合成 标题:含甲基或氟取代基的溴代五芳基环戊二烯的简便合成 摘要:摘要 酮类 C 5 (3,5-C 6 H 3 Me 2) 4 (O) (5B) 和 C 5-2,5(3,5-C 6 H 3 Me 2) 2 (C 6 H 5) 2 (O) (5C) 被制备和表征.五芳基环戊二烯醇 C 5 (C 6 H 5) 4 (Ar')(Oh) (Ar'=3,5-C 6 H 3 Me 2,6A3 ;Ar'=2,4,6-C 6 H 2 Me 3,6A5 ; Ar'=3-C 6 H 4 F,6A6 ; Ar'=3,5-C 6 H 3 F 2,6A7),C 5 (3,5-C 6 H 3 Me 2) 4 (Ar ')(Oh) (Ar'=3-C 5 H 4 Me,6B2 ; 3,5-C 5 H 3 Me 2,6B3 ; 3,6-C 5 H 3 Me 2,6B4 ; 2,4,6-C 5 H 2 Me 3,6B5 ; Ar'=3-C 6 DOI:10.1016/s0022-328X(01)00725-2
专利号:US-2018208775-A1 优先权日:2014-06-23 标 题:New aromatic macrocyclic metal complex dyes and the synthesis thereof with active nano metal powders 发明人:OLGUN UGURSOY; YILDIZ SALIH ZEKI 权利人:OLGUN UGURSOY; YILDIZ SALIH ZEKI 摘要:The present invention relates to a new type of inorganic coordination compound dyes having advanced technology optical, electronic and medical characteristics and relates to production of these dyes by means of new synthesis methods. The present invention relates to dyes which are metal (M: Li, Na, K, Mg, Ca, Sr, Ba, Ti, Zr, V, Cr, Mo, Mn, Re, Fe, Ru, Co, Rh, Ir, Ni, Pd, Pt, Cu, Ag, Au, Zn, Cd, B, Al, Ga, In, Si, Ge, Sn, Pb, Sb, Bi, Se, Te) complexes of aromatic macrocyclic compounds of the type Phtalocyanine (Pc), Naphtalocyanine (Nc), Porphyrazine (Pz), Porphyrin (Pr), sub-Phtalocyanine (subPc), sub-Naphtalocyanine (subNc), sub-Porphyrazine (subPz), sub-Porphyrine (subPr), and relates to the synthesis of these complexes and derivatives. The subject matter dyes can be used in solar cell photovoltaic (PV) panels, in OLEDS which are organic structured light emitting diodes, in polymers, in textile and in photodynamic therapy PDT applications. Moreover, industrial applications are possible which depend on strong fluorescence characteristics.
专利号:US-4033949-A 优先权日:1976-04-14 标 题:Analogs of thromboxane B2 and processes for their synthesis 发明人:KELLY ROBERT C; NELSON NORMAN A 权利人:UPJOHN CO 摘要:The present specification provides novel intermediates and novel processes for the synthesis of various side chain and skeletal analogs of Thromboxane B 2 (11β-homo-11a-oxa-PGF 2 .sub.α). These analogs are particularly and especially useful as reproductive cycle control agents.
专利号:US-7517828-B2 优先权日:2003-04-25 标 题 :Chiral broensted acid catalyst for asymmetric synthesis and method of asymmetric synthesis with the catalyst 发明人:AKIYAMA TAKAHIKO 权利人:TOAGOSEI CO LTD 摘要:A compound usable as an asymmetric synthesis catalyst which can be easily synthesized without using any metal such as a lanthanoid group element; a method of asymmetric synthesis with the compound; and a chiral compound obtained by the asymmetric synthesis method. A Broensted acid is used as a catalyst in asymmetric synthesis, the chiral Broensted acid being represented by formula (1) below or formula (3) below. The asymmetric synthesis method employs the catalyst. Asymmetric synthesis with the catalyst gives a chiral compound.
专利号:US-2012115907-A1 优先权日:2009-04-24 标题 :Novel compounds as inhibitors of renin 发明人:THOMBARE PRAVAIN; DESAI JIGAR; JAIN MUKUL R 权利人:THOMBARE PRAVAIN; DESAI JIGAR; JAIN MUKUL R; CADILA HEALTHCARE LTD 摘要:The present invention relates to novel renin inhibitors of general formula (1), novel intermediates involved in their synthesis, their pharmaceutically acceptable salts and pharmaceutical compositions containing them. The present invention also relates to a process of preparing compounds of general formula (1), their tautomeric forms, their pharmaceutically acceptable salts, pharmaceutical compositions containing them, and novel intermediates involved in their synthesis.
专利号:EP-2883866-A1 优先权日:2012-08-13 标题 :INTERMEDIATE FOR SYNTHESIS OF 1-(2-DEOXY-2-FLUORO-4-THIO-beta-D-ARABINOFURANOSYL) CYTOSINE, INTERMEDIATE FOR SYNTHESIS OF THIONUCLEOSIDE, AND METHODS FOR PRODUCING THESE INTERMEDIATES
专利号:CN-120126588-A 优先权日:2025-01-20 标 题:A method for optimizing the synthesis of aryl porphyrin compounds
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合成参考文献
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