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CAS号618-87-1 3,5-二硝基苯胺 | CAS号99-35-4 1,3,5-三硝基苯 | CAS号57-13-6 尿素 | CAS号33786-89-9 5-氯-m-苯二胺 | CAS号626-39-1 1,3,5-三溴苯 | CAS号626-40-4 3,5-二溴苯胺 | CAS号621-22-7 1,3,5-苯三酚三 | CAS号99-34-3 3,5-二硝基苯甲酸 | CAS号88-88-0 2,4,6-三硝基氯苯 | CAS号101670-67-1 1,3,5-triisothi... | CAS号108-73-6 间苯三酚 | CAS号7373-27-5 1,3,5-triis°Cya...合成工艺路线路线简述
- 合成目标产物 1,3,5-Triaminobenzene 主要起始原料 Urea
- (文献来源)合成步骤主要原料 Urea
📜1,3,5-三硝基苯置于三氯化铁,甲烷,一水合肼体系中,用 甲醇 用作溶剂,化学反应 13.0H,反应生成1,3,5-三氨基苯
参考文献:用水合肼选择性还原 1,3,5-三硝基苯中的一个,两个或三个硝基
标题:用水合肼选择性还原 1,3,5-三硝基苯中的一个,两个或三个硝基
摘要:开发了一种在氯化铁和木炭存在下使用水合肼连续选择性还原 1,3,5-三硝基苯中的一个,两个或三个硝基的方法.该方法提供了一种从 1,3,5-三硝基苯一锅合成 3,5-二硝基苯胺,1,3-二氨基-5-硝基苯或 1,3,5-三氨基苯的方法.
Doi:10.1007/s11172-006-0356-2
专利信息
专利号:US-9157156-B2
优先权日:2009-07-07
标题 :Process for the preparation of a iodinating agent
发明人:ANELLI PIER LUCIO; VISCARDI CARLO FELICE; DELOGU PIETRO; GOFFREDI FABRIZIO; NARDELLI ALFONSO; GIOVENZANA GIOVANNI BATTISTA
权利人:ANELLI PIER LUCIO; VISCARDI CARLO FELICE; DELOGU PIETRO; GOFFREDI FABRIZIO; NARDELLI ALFONSO; GIOVENZANA GIOVANNI BATTISTA; BRACCO IMAGING SPA
摘要:The present invention describes a process for the synthesis of a iodinating agent, being said iodinating agent iodine chloride (ICI.) In particular, the present invention relates to a process for the electrochemical preparation of ICI, as a useful iodinating agent in the preparation of iodinated organic compounds for use as contrast agents or their precursors in the synthesis of the same.
专利号:US-11472779-B1
优先权日:2022-05-13
标 题 :One-pot synthesis of hydrogen-bonded organic frameworks
发明人:KHAN MOHD YUSUF; KHAN ABUZAR; HELAL AASIF; YAMANI ZAIN H
权利人:UNIV KING FAHD PET & MINERALS
摘要:A hydrogen-bonded organic framework (HOF) and a method of making the HOF. The HOF has at least one amine substituted organic linker and at least one carboxylic acid-based organic linker. The HOF is prepared by dissolving the linkers separately in water and mixing the aqueous solutions, without using any organic solvents, additional catalysts, or any other reagents.
专利号:US-9943809-B2
优先权日:2014-02-27
标题 :Solvent resistant thin film composite membrane and its preparation
发明人:DOM ELKE; HERMANS SANNE; KOECKELBERGHS GUY; VANKELECOM IVO
权利人:KATHOLIEKE UNIV LEUVEN KU LEUVEN RESEARCH & DEVELOPMENT; UNIV LEUVEN KATH
摘要:The present invention relates to improved methods for synthesis of thin film composite membranes by interfacial polymerization. More in particular, the method of the present invention comprises the impregnation of an ultrafiltration porous support membrane with an aqueous solution containing a polyfunctional nucleophilic monomer, and contacting the impregnated support membrane with a second largely water-immiscible solvent containing a polyfunctional epoxide monomer.
专利号:WO-2011050245-A1
优先权日:2009-10-23
标 题:Bicyclic heteroaryls as kinase inhibitors
发明人:FENG YANGBO; CHEN YEN TING; SESSIONS HAMPTON; MISHRA JITENDRA K; CHOWDHURY SARWAT; YIN YAN; LOGRASSO PHILIP; LUO JUN-LI; BANNISTER THOMAS; SCHROETER THOMAS
权利人:FENG YANGBO; CHEN YEN TING; SESSIONS HAMPTON; MISHRA JITENDRA K; CHOWDHURY SARWAT; YIN YAN; LOGRASSO PHILIP; LUO JUN-LI; BANNISTER THOMAS; SCHROETER THOMAS
摘要:The invention is directed to heteroaryl compounds useful as inhibitors of various kinase enzymes. In various embodiments, the invention provides a heteroaryl compound having inhibitory bioactivity with respect to a Rho kinase, an AKT kinase, a p70S6K kinase, a LIM kinase, an IKK kinase, a Flt kinase, an Aurora kinase, or a Src kinase, or any combination thereof. Compounds of the invention include bicyclic heteroaryl compounds of formula (I), which can contain a bridging nitrogen atom at a ring junction. The invention further provides methods of synthesis of compounds of the invention, pharmaceutical compositions, pharmaceutical combinations, and methods of treatment of malconditions using compounds of the invention.
专利号:US-5371173-A
优先权日:1992-11-25
标题:Poled polymeric nonlinear optical materials
发明人:MARKS TOBIN J; HUBBARD MICHAEL A; LIN JIANN T
权利人:UNIV NORTHWESTERN
摘要:The synthesis of a nonlinear chromophoric co-monomer 3,5-diamino-4'-nitrodiphenylamine and use as a reactive component in combination with a bismaleimide monomer in a NLO-active polyimide matrix is disclosed. After concurrent corona or contact poling and thermal polymerization, thin films of these chromophoric polyimides exhibit high second harmonic generation efficiencies and high DSC-determined glass transition temperatures. These poled polyimides also exhibit excellent SHG temporal stability, retaining 85-90% of the initial second harmonic efficiency after more than one month in air at 85° C.
专利号:US-9241917-B2
优先权日:2003-03-17
标 题 :Facially amphiphilic polymers and oligomers and uses thereof
发明人:DEGRADO WILLIAM F; TEW GREGORY N; KLEIN MICHAEL L; LIU DAHUI; YUAN JING; CHOI SUNGWOOK
权利人:DEGRADO WILLIAM F; TEW GREGORY N; KLEIN MICHAEL L; LIU DAHUI; YUAN JING; CHOI SUNGWOOK; UNIV PENNSYLVANIA
摘要:The present invention discloses methods of use of facially amphiphilic polymers and oligomers, including pharmaceutical uses of the polymers and oligomers as antimicrobial agents and antidotes for hemorrhagic complications associated with heparin therapy. The present invention also discloses novel facially amphiphilic polymers and oligomers and their compositions, including pharmaceutical compositions. The present invention further discloses the design and synthesis of facially amphiphilic polymers and oligomers.