CAS: 83647-42-1; (3-Amino-2-Methylphenyl)Methanol

该化合物是一种有机化合物,其特点是存在氨基氨基化合物(-NH2)和附于苯环的氢氧基化合物,该化合物也具有甲基混合物.该化合物一般是无色的,可粉黄的液体或固体,视其纯度和形态而定.该化合物在水和各种有机溶剂中溶解,可适用于不同用途.该氨基化合物组有助于其在各种化学反应中的基本性和潜在再活动,如核细胞替代或混合反应.该氢氧基化合物组增强了其参与氢联结,影响其物理特性和再活动的能力.该化合物可用于合成药品,农用化学品或有机合成的中间体.应审查安全数据,如任何化学品一样,以了解其处理,储存和潜在危害.

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CAS号23876-13-3 2-甲基-3-硝基苯甲醇 | CAS号18583-89-6 3-氨基-2-甲基苯甲酸甲酯 | CAS号59382-59-1 2-甲基-3-硝基苯甲酸甲酯 | CAS号59383-08-3 2-methyl-3-nitr... | CAS号1975-50-4 2-甲基-3-硝基苯甲酸 | CAS号39053-41-3 2-甲基-3-硝基苯甲酰氯 | CAS号71516-35-3 2-甲基-3-硝基苯甲腈 | CAS号34529-06-1 3-氨基邻苯二甲酸二甲酯 | CAS号60-29-7 乙醚 | CAS号23876-13-3 2-甲基-3-硝基苯甲醇 | CAS号83647-43-2 3-溴-2-甲基苯甲醇

合成工艺路线路线简述

  • 23876-13-3 = 83647-42-1 [标题:Reaction Conditions
    标题:Preparation Of (Dihalovinyl)Benzyl Esters As Pesticides
    参考文献:Germany]

    34034-36-1 = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 Reagents: Potassium Carbonate Catalysts: Tetrabutylammonium Bromide Solvents: Acetonitrile; 17 H,65 °C2.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C2.2 Reagents: Sodium Chloride Solvents: Water; 2 Min3.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt3.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt4.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]

    33302-94-2 = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 Reagents: Sodium Periodate Solvents: Water; 10 Min,Rt2.1 Reagents: Potassium Carbonate Catalysts: Tetrabutylammonium Bromide Solvents: Acetonitrile; 17 H,65 °C3.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C3.2 Reagents: Sodium Chloride Solvents: Water; 2 Min4.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt4.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt5.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]

    = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]

    65-85-0 = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt1.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt2.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]

    = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C1.2 Reagents: Sodium Chloride Solvents: Water; 2 Min2.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt2.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt3.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]

    = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 300 - 900 °C2.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt2.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt3.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]

    116-53-0 = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt1.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt2.1 300 - 900 °C3.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt3.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt4.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406]

    66-84-2 + 105-45-3 = 83647-42-1 + 116-53-0 + 20282-39-7 + 18358-63-9 + 81863-45-8 + 4518-10-9 + 51-67-2 + 868-57-5 + 934-60-1 + 23950-04-1 + 13231-81-7 + 79491-14-8
    反应条件:1.1 Reagents: Sodium Bicarbonate Solvents: Water; 24 H,Rt2.1 Reagents: Sodium Periodate Solvents: Water; 10 Min,Rt3.1 Reagents: Potassium Carbonate Catalysts: Tetrabutylammonium Bromide Solvents: Acetonitrile; 17 H,65 °C4.1 Reagents: Sodium Borohydride Solvents: Methanol; 20 Min,0 °C4.2 Reagents: Sodium Chloride Solvents: Water; 2 Min5.1 Reagents: 1-Ethyl-3-(3′-Dimethylaminopropyl)Carbodiimide Solvents: Dichloromethane; 1 H,Rt5.2 Catalysts: 4-(Dimethylamino)Pyridine; 24 H,Rt6.1 300 - 900 °C
    标题:Synthesis And Pyrolysis Of Two Novel Pyrrole Ester Flavor Precursors
    作者:Fan,Wenpeng; Et Al
    参考文献:Journal Of Heterocyclic Chemistry 日期:2022 卷标:59(8) 页码:1397-1406
📜2-甲基-3-硝基苯甲醇置于钯体系中,用 乙醇 作为反应溶剂,化学反应 2.0H,以to Give 3-Amino-2-Methylbenzyl Alcohol (1.67 G,Quantitative),M.P. 104°-106°的收率获得产物3-氨基-2-甲基苯甲醇
参考文献:Substituted 4-Aminoquinoline Derivatives As Gastric Acid Secretion
标题:Substituted 4-Aminoquinoline Derivatives As Gastric Acid Secretion
摘要:以下是翻译结果: 公式为:##str1##其中r.Sup.1为氢,C.Sub.1-6烷基,C.Sub.1-6烷氧基c.Sub.1-6烷基; C.Sub.3-6环烷基,C.Sub.3-6环烷基-C.Sub.1-6烷基,苯基c.Sub.1-6烷基,苯基可以选择性地被取代; R.Sup.2为羟基c.Sub.1-6烷基,C.Sub.1-6烷氧基c.Sub.1-6烷基或者相邻的两个r.Sup.2基团形成c.Sub.1-4烷二氧基基团; R.Sup.3为氢,C.Sub.1-6烷基,C.Sub.1-6烷氧基,氨基,C.Sub.1-6烷硫基,卤素,氰基,羟基,C1-6烷酰基或三氟甲基; R.Sup.4为氢,C.Sub.1-6烷基,苯基,C.Sub.1-6烷氧基,C.Sub.1-6烷硫基,C.Sub.1-6烷酰基,氨基,C.Sub.1-6烷基氨基,二c.Sub.1-6烷基氨基,卤素或三氟甲基; N为1或2; Q为0到4; M为1,2或3; P为1,2,3或4,但是m+p不大于5; 或其盐可用作胃酸分泌抑制剂.

海关参考信息

专利信息


专利号:EP-0844261-A1
优先权日:1996-11-21
标题:Dispersions containing polyurethanes with carbonyl groups in ketone function
发明人：KOKEL NICOLAS DR; GULBINS ERICH DR; RAU MARIA GYOPAR DR; FISCHER GERHARD
权利人:BASF AG
摘要:R 1 , R 2 , R 3 jeweils Wasserstoff, C 1 - bis C 24 -Alkyl oder C 6 - bisnC 24 -Alkenyl R 4 Wasserstoff R 5 , R 6 a) gemeinsam C 4 - bis C 10 -Alkandiyl, b) jeweils C 2 - bis C 10 -Alkyl, C 5 - bis C 8 -Cycloalkylnoder C 7 - bis C 20 -Aralkyl, c) jeweils ein hydroxylterminiertes Poly-(C 2 - bisnC 4 -alkylenoxid), oder d) ein Rest R 5 oder R 6 die unter (a) bis (c) angegebenenBedeutung und der andere Rest Wasserstoffnoder ein Rest der Formel IIn nin der X C 2 - bis C 6 -Alkandiyl bedeutet und R 7 gleichbedeutend ist mit R 5 oder R 6 mit der Ausnahme,ndaß R 7 nicht ein Rest der Formel II bedeutet, nwobei n die Reste R 5 und R 6 in jedem der Fälle (a) bis (d) insgesamtneine (1) an ein aliphatisches C-Atom gebundene Hydroxylgruppenntragen, gegebenenfalls der Rest R 5 und/oder R 6 1 oder 2 aromatischngebundene Hydroxylgruppen oder 1 Nitril-, tertiäre Amino-,nCarbonsäure- oder Sulfonsäuregruppe, die gegebenenfalls innForm ihrer Salze vorliegen, trägt, und die mittlere Funktionalität (F) aller Aufbaukomponenten desnPolyurethans (A), bezogen auf die Funktionalitäten, die beimnAufbau des Polyurethans (A) in einer Additionsreaktion miteinandernreagieren, 1,5 bis 2,2 beträgt. Aqueous dispersions containing a polyurethane (A) with structural units which differ from compounds of the formula (I) in which the substituents have the following meaning: R 1 , R 2 , R 3 in each case hydrogen, C 1 - to C 24 -alkyl or C 6 - to C 24 -alkenyl R 4 hydrogen R 5 , R 6 a) together C 4 - to C 10 -alkanediyl, b) in each case C 2 to C 10 alkyl, C 5 to C 8 cycloalkyl or C 7 to C 20 aralkyl, c) in each case a hydroxyl-terminated poly (C 2 - to C 4 -alkylene oxide), or d) a radical R 5 or R 6 has the meaning given under (a) to (c) and the other radical is hydrogen or a radical of the formula II in the X C 2 - to C 6 -alkanediyl means and R 7 is equivalent to R 5 or R 6 with the exception that R 7 does not represent a radical of the formula II, in which the radicals R 5 and R 6 in each of cases (a) to (d) carry a total of one (1) hydroxyl groups bonded to an aliphatic carbon atom, optionally the radical R 5 and / or R 6 carries 1 or 2 aromatically bound hydroxyl groups or 1 nitrile, tertiary amino, carboxylic acid or sulfonic acid group, which are optionally present in the form of their salts, and the average functionality (F) of all structural components of the polyurethane (A), based on the functionalities which react with one another during the synthesis of the polyurethane (A) in an addition reaction, is 1.5 to 2.2.

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合成参考文献


摘要:Aitken, K. M.; Aitken, R. A., Science of Synthesis, (2007) 31, 1286.
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