CAS: 605-48-1; 9,10-Dichloroanthracene

该化合物是炭疽家族的有机化合物,其特点是在炭疽结构的9和10个位置上存在两个氯原子,它看起来是固体的,典型地表现出一种晶状形式,有明显的黄色至橙色,水中溶点相对较高,溶解性较低,但在氯仿和苯等有机溶剂中是可溶解的. 9,10-二氯苯甲丙烯主要用于研究和工业应用,特别是在有机电子和光化学领域,在其中它充当各种化学合成的前体.其光物理特性使它成为与荧光和光导力有关的研究的主体.然而,必须谨慎地处理这一化合物,因为它可能对环境和健康造成危害,包括潜在的毒性和致癌性.在实验室环境中与该物质打交道时,应当注意适当的安全措施.

结构式图片

相似化合物

66259-12-9 716-53-0 17135-78-3

欧盟法规

ECHA物质C&L通报REACH预注册

上下游产品

9-chloroanthracene anthracene anthracen-9(10H)-one 9-benzylanthracene 9,10-phenanthrenequinone 9-chloroanthracene anthracene 2,7-diaminoanthraquinone

合成工艺路线路线简述

  • 合成目标产物 9,10-Dichloroanthracene 主要起始原料 Anthracene
  • (文献来源)合成步骤主要原料 Anthracene
📜9-氯蒽置于硫酸,四丁基高氯酸铵,Sodium Chloride体系中,用 二氯甲烷,水 作为反应溶剂,以50 %的收率获得产物9,10-二氯蒽
参考文献:芳烃电化学氯化和硝化的相转移催化
标题:芳烃电化学氯化和硝化的相转移催化
摘要:一种独特的双相电化学反应,其中四丁基铵 (Tba +) 盐起到电解质和相转移催化剂的双重作用,被开发用于使用廉价的无机盐进行芳香族化合物的氯化和硝化,产率高达 98%,反应时间更短,更高的法拉第效率.
DOI:10.1002/anie.202319206

海关参考信息

专利信息


专利号:US-3919155-A
优先权日:1970-12-18
标题:Synthesis of aromatic amines by reaction of aromatic compounds with ammonia
发明人:SQUIRE EDWARD NOONAN
权利人:DU PONT
摘要:An improved process for producing an aromatic amine is provided in which an aromatic compound is reacted with ammonia in the presence of a conditioned nickel/nickel oxide cataloreactant at a temperature of from about 150*C. to about 500*C. and at a pressure of from about 10 to about 1000 atmospheres and in the presence of from 1 mole percent to 250 mole percent of water based on the molar amount of the aromatic compound.

专利号:US-4031106-A
优先权日:1973-12-19
标题:Synthesis of aromatic amines by reaction of aromatic compounds with ammonia
发明人:DELPESCO THOMAS WAYNE
权利人:DU PONT
摘要:An improved process is provided for producing an aromatic amine from ammonia and an aromatic compound which comprises reacting the aromatic compound with ammonia at a temperature of from about 150 DEG C. to about 500 DEG C. and at a pressure of from about 10 to about 1000 atmospheres in the presence of a conditioned nickel/nickel oxide/zirconium oxide cataloreactant containing an oxide of lanthanum, samarium, holmium, europium, erbium, yttrium, praseodymium, neodymium, terbium, ytterbium, dysprosium or a mixture of any of them.

专利号:US-3929889-A
优先权日:1971-02-16
标 题 :Synthesis of aromatic amines by reaction of aromatic compounds with ammonia
发明人:SQUIRE EDWARD NOONAN
权利人:DU PONT
摘要:An improved process for producing an aromatic amine is provided in which an aromatic compound is reacted with ammonia in the presence of a conditioned nickel/nickel oxide cataloreactant at a temperature of from about 150*C. to about 500*C. and at a pressure of from about 10 to about 1000 atmospheres.

专利号:US-4001260-A
优先权日:1973-12-19
标 题:Synthesis of aromatic amines by reaction of aromatic compounds with ammonia
发明人:DEL PESCO THOMAS W
权利人:DU PONT
摘要:An improved process is provided for producing an aromatic amine from ammonia and an aromatic compound which comprises reacting the aromatic compound with ammonia at a temperature of from about 150° C. to about 500° C. and at a pressure of from about 10 to about 1000 atmospheres in the presence of a conditioned nickel/nickel oxide/zirconium oxide cataloreactant which has been treated with ammonia prior to introduction of the cataloreactant to the amination reactants.

专利号:TW-200800883-A
优先权日:2005-06-28
标 题:Novel system for synthesis of device forming monomers

专利号:CN-117486663-A
优先权日:2023-11-08
标 题 :A kind of synthesis method of 9,10-diphenylanthracene

供应商参考报价(招募中)

品牌试剂参考报价(招募中)

📌 第三方产品分析报告

✅ COA系统入驻 | 共享模式

合成参考文献


摘要:Stanforth, S. P., Science of Synthesis, (2007) 31, 85.
摘要:Collier, S. J.; Xiang, W., Science of Synthesis, (2010) 41, 655.
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