专利号:US-2024075466-A1 优先权日:2021-04-09 标 题:One-Pot Synthesis of Transition Metal-Promoted Chabazites 发明人:VAN TENDELOO LEEN; SCHUETZE FRANK-WALTER; VERHEYEN ELKE JANE JUNE 权利人:UMICORE AG & CO KG 摘要:The invention provides methods for a one-pot synthesis of molecular sieves of the CHA-type. The method uses molecular and non-molecular sieves as sources of silicon and aluminum. A first OSDA is selected from tetraethylenepentamine (TEPA) and triethy-lenepentamine (TETA). The synthesis mixture comprises a first metal selected from copper, iron and zinc. Optionally, the synthesis mixture may furthermore comprise a second OSDA and/or a second metal selected from manganese, cesium, magnesium, calcium, strontium, barium, yttrium, titanium, zirconium, niobium, iron, zinc, silver, lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium and mixtures thereof. The molecular sieves of the CHA-type obtainable by the method can be used as SCR-catalytically active substances for the removal of nitrogen oxides from exhaust gases of combustion engines.
专利号:US-12304885-B2 优先权日:2022-04-20 标 题:Synthesis and purification of CBDA 发明人:SHEARER RANDALL L 权利人:UNIV COLORADO REGENTS; UNIV COLORADO REGENTS 摘要:Methods and systems for the preparation of high purity and high quality cannabinoid acids and metal salts of cannabinoids. Cannabidiolic acid (CBDA) is a major cannabinoid of interest for and health reasons. It is the natural precursor of cannabidiol (CBD). The invention provides methods for the synthesis of CBDA from CBD with reagents that produce a high purity product without need for further purification. Insertion of a magnesium complexing agent prior to conversion of the reaction intermediate to the final acid product produces a high purity product with aesthetically pleasing white color and neutral odor. Methods are provided for the simultaneous synthesis and purification of cannabinoid acids, especially CBDA, produced from high purity CBD (or other cannabinoid) via a Kolbe-Schmitt type reaction using an organic base, such as DBU (1,8-diazabicyclo[5.4.0]undec-7-ene), incorporating complexation of acid anions to a multivalent metal, alkaline earth or transition metal, prior to product acid work-up. During the work-up to the final acid, the distinct solubility of the complex in selected solvents is used advantageously to first exclude water soluble reagents and impurities and next to exclude lipophilic hydroxyl-quinone impurities, as well as any unconverted CBD.
专利号:US-2012231327-A1 优先权日:2010-03-10 标题:Positive electrode active material for non-aqueous electrolyte secondary battery, process for production of same, and non-aqueous electrolyte secondary battery produced using same 发明人:HIRATSUKA HIDEKAZU 权利人:HIRATSUKA HIDEKAZU; PANASONIC CORP 摘要:At the time of synthesis of lithium nickelate, by adding a firing aid to material to be fired, crystal growth is promoted at a temperature that is lower than a firing temperature necessary for obtaining desired crystal growth of lithium nickelate, and substitution of elements that contribute to structural stability in crystals is promoted. Furthermore, distortion of crystal or loss of oxygen at the time of synthesis is suppressed. Thus, a lithium ion secondary battery having excellent charge and discharge characteristics and cycling characteristics can be provided.
专利号:US-2007054042-A1 优先权日:2005-09-06 标 题 :Method of SrCu2O2 spin-on precursor synthesis and low temperature p-type thin film deposition 发明人:ZHUANG WEI-WEI; ONO YOSHI; GAO WEI 权利人:SHARP LAB OF AMERICA INC 摘要:A method of SrCu 2 O 2 spin-on precursor synthesis and low temperature p-type thin film deposition, includes preparing a wafer to receive a spin-coating thereon; selecting metalorganic compounds to form a SrCu 2 O 2 precursor, mixing and refluxing the metalorganic compounds to form a precursor mixture; filtering the precursor mixture to produce a spin-coating precursor; applying the spin-coating precursor to the wafer in a two-step spin coating procedure; baking the spin-coated wafer using a hot-plate bake to evaporate substantially all of the solvents; and annealing the spin-coated wafer to form a SrCu 2 O 2 layer thereon in a two-step post-anneal process.
专利号:US-2025171322-A1 优先权日:2022-03-01 标题:Catalyst support materials for use in ammonia synthesis 发明人:O'HAYRE RYAN P; CADIGAN CHRISTOPHER A; HUANG JAKE D 权利人:OHAYRE RYAN P; CADIGAN CHRISTOPHER A; HUANG JAKE D; COLORADO SCHOOL OF MINES 摘要:Described herein are catalyst support materials for use in synthesizing ammonia (NH 3 ) from nitrogen gas (N 2 ) and hydrogen gas (H 2 ) and methods of making the same. The support material may comprise (MgO) x (BaO) y (Al 2 O 3 ) z and/or (MgO) x (SrO) y (Al 2 O 3 ) z , on which an ammonia synthesis catalyst such as ruthenium is dispersed. When the catalyst support material comprises (MgO) x (BaO) y (Al 2 O 3 ) z , x is from about 0.05 to about 0.7, y is from about 0.05 to about 0.6, and z is from about 0.3 to about 0.5. When the catalyst support material comprises (MgO) x (SrO) y (Al 2 O 3 ) z , x is from about 0.4 to about 0.7, y is from about 0.05 to about 0.5, and z is from about 0.05 to about 0.3.
专利号:US-6210752-B1 优先权日:1999-03-24 标 题:All-alkoxide synthesis of strontium-containing metal oxides 发明人:BOYLE TIMOTHY J 权利人:SANDIA CORP 摘要:A method for making strontium-containing metal-oxide ceramic thin films from a precursor liquid by mixing a strontium neo-pentoxide dissolved in an amine solvent and at least one metal alkoxide dissolved in a solvent, said at least one metal alkoxide selected from the group consisting of alkoxides of calcium, barium, bismuth, cadmium, lead, titanium, tantalum, hafnium, tungsten, niobium, zirconium, yttrium, lanthanum, antimony, chromium and thallium, depositing a thin film of the precursor liquid on a substrate, and heating the thin film in the presence of oxygen at between 550 and 700° C.
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合成参考文献
摘要:S13 | EUCOSMETICS | Combined Inventory of Ingredients Employed in Cosmetic Products (2000) and Revised Inventory (2006) | DOI:10.5281/zenodo.2624118