专利号:US-8815351-B2 优先权日:2005-09-15 标 题:Method for attachment of silicon-containing compounds to a surface and for synthesis of hypervalent silicon-compounds 发明人:OWENS JEFFREY R 权利人:OWENS JEFFREY R; US AIR FORCE 摘要:A method for attaching silicon-containing compounds to a surface and for synthesis of hypervalent silicon-compounds is described. Attaching silicon-containing compounds to a surface comprises providing a silicon-containing compound having two or more leaving groups, and a first functional compound comprising at least one nucleophilic group, contacting the silicon-containing compound and the functional compound with a surface of a substrate having nucleophilic sites and exposing the silicon-containing compound, the functional compound and the surface of the substrate to microwave radiation.
专利号:US-4764581-A 优先权日:1986-07-05 标题:Liquid-crystalline diglycidyl compounds, the preparation of these, and the use of these in curable epoxide mixtures 发明人:MUELLER HANNS P; GIPP ROLAND; HEINE HEINRICH 权利人:BAYER AG 摘要:The invention relates to new, liquid-crystalline diglycidyle compounds of optionally ring-substituted 4-hydroxyphenyl 4-hydroxybenzoates, a synthesis of p-epoxypropoxy-phenyl p-epoxy-propoxybenzoate, furthermore epoxy resin mixtures containing the new diglycidyle compounds, and the use of the new diglycidyl compounds and the epoxy resin mixtures thereof in curable mixtures.
专利号:US-4367343-A 优先权日:1981-12-31 标 题:Synthesis of tetraalkylsilanes 发明人:TAMBORSKI CHRIST; SNYDER JR CARL E 权利人:US AIR FORCE 摘要:A mixture of tetraalkylsilanes is prepared by reacting a mixture of at least two organometallic compounds with a silicon tetrahalide or an alkyl silicon trihalide. The mixture of silanes is useful as a hydraulic fluid.
专利号:US-6989409-B2 优先权日:2002-06-21 标 题 :Method for synthesis of spray-dried poly(METH)acrylate polymers, use of same as polymer components for plastisols, and plastisols produced therewith 发明人:LOEHDEN GERD; ROOS SEBASTIAN; BELZNER WINFRIED; GEYER HANS-JUERGEN; JUNG HERBERT; RAUSCH URSULA 权利人:ROEHM GMBH 摘要:A plastisol formulation which can be used for coatings of metal sheets, the coatings having high abrasion resistance, contains a) a plasticizer or mixture of plasticizers; and b) a mixture of polymer particles containing at least two components A and B; c) at least one member selected from the group consisting of fillers, coupling agents, stabilizers, desiccants, rheological additives, hollow bodies and mixtures thereof; wherein the polymer particles containing at least two components A and B have one of the following structures ba) a 2-stage structure, a 3-stage structure or multi-stage structure, or bb) a gradient polymer structure.
专利号:US-9487471-B1 优先权日:2014-04-14 标题 :Synthesis of pyrethroids and pyrethroid-containing compositions 发明人:COELHO PEDRO; MEINHOLD PETER; CHEN MIKE M Y 权利人:PROVIVI INC 摘要:The present invention provides methods for synthesizing pyrethroid compounds. The methods include forming a first reaction comprising an olefin and an allethrolone-type unsaturated alcohol under conditions sufficient to form a metathesis product and converting the metathesis product to the pyrethroid. Methods of the invention can be used to prepare compounds including pyrethrin I, cinerin I, jasmolin I, pyrethrin II, cinerin II, and jasmolin II as well as other synthetic pyrethroid compounds. Insecticidal compositions and methods for controlling insects are also described.
专利号:US-2023339839-A1 优先权日:2022-04-24 标题:Synthesis method of alpha-hydroxycarboxylic acid ester 发明人:MENG ZHONGLEI; QIN RONGXIU; GAO SHOUNA; HU GUOJIAO; WEN RUSI; Liao Zhongqiu; LIANG ZHONGYUN; HU LIHONG; ZHOU YONGHONG 权利人:GUANGXI FORESTRY RES INSTITUTE 摘要:A synthesis method of alpha-hydroxycarboxylic acid ester is provided. In the method, an alpha-hydroxycarboxylic acid and an alcohol are taken as raw materials, one or more of boric acid, metaboric acid, pyroboric acid, and boric anhydride is taken as a catalyst, and one of cyclohexane, toluene, benzene, and alcohols is taken as a water-carrying agent. A reaction temperature is kept in range of 100-160° C., produced water is separated by an oil-water separator, and the alpha-hydroxycarboxylic acid ester is synthesized directly. After an esterification reaction, the water-carrying agent and unreacted alcohol are distilled by vacuum fractionation to obtain a crude product, and refined alpha-hydroxycarboxylic acid ester is obtained by performing neutralization, water washing, and vacuum rectification on the crude product. The alpha-hydroxycarboxylic acid ester prepared by the method has high purity and light color, and can be used as green solvent, surfactant, chiral resolution agent and plasticizer.
参考标题:Synthesis Of Esters By Functionalisation Of Co2 摘要:The Invention Relates To A Method For (I) Producing A Carboxylic Ester Of Formula (I). Said Method Comprises The Steps Of: A) Bringing An Organosilane/borane Of Formula Si Or B Into Contact With Co 2 , In The Presence Of A Catalyst And An Electrophilic Compound Of Formula (III), The Groups R 1 , R 2 , R 3 , R 4 , R 5 , Y, And M′ Being As Defined In Claim 1; And Optionally B) Recovering The Compound Of Formula (I) Produced.
合成参考文献
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