📜苄基-β-L-吡喃阿拉伯糖苷置于palladium On Activated Charcoal Ammonium Formate体系中,用 甲醇 作为反应溶剂,化学反应 0.33H,以96%的收率获得产物l-(+)-阿拉伯糖 参考文献:Removal Ofo-Benzyl Protective Groups By Catalytic Transfer Hydrogenation 标题:Removal Ofo-Benzyl Protective Groups By Catalytic Transfer Hydrogenation 摘要: DOI:10.1055/s-1985-31113
专利号:US-2022395800-A1 优先权日:2019-11-04 标题:Device for automated synthesis of oligo- and polysaccharides 发明人:SEEBERGER PETER H; DANGLAD FLORES JOSE; LE MAI HOANG KIM; PARDO VARGAS ALONSO; SLETTEN ERIC; SALWICZEK MARIO 权利人:MAX PLANCK GESELLSCHAT ZU RFERDERUNG DER WSS E V; GlycoUniverse GmbH & Co KG&A 摘要:The present invention generally relates to automated synthesis technology, and more particularly, to a device and method for automated synthesis of oligo- and polysaccharides on a solid support. In particular the present invention relates to a device for automated synthesis of oligo- and polysaccharides on a solid support comprising a reaction vessel, a reagent storing component, a reagent delivery system, a cooling device for cooling reaction vessel, and a pre-cooling device for pre-cooling the reagents to be supplied.
专利号:EP-3835306-A1 优先权日:2019-12-13 标题:Microwave-assisted method for synthesis of oligo- and polysaccharides on solid phase 权利人:MAX PLANCK GESELLSCHAFT 摘要:The present invention relates to a method for synthesizing oligo- and polysaccharides using microwave radiation, in particular to a method and a device for automated synthesis of oligo- and polysaccharides.
专利号:US-8541569-B2 优先权日:2008-09-06 标题:Phosphoramidites for synthetic RNA in the reverse direction, efficient RNA synthesis and convenient introduction of 3'-end ligands, chromophores and modifications of synthetic RNA 发明人:SRIVASTAVA SURESH C; SRIVASTAVA NAVEEN P 权利人:SRIVASTAVA SURESH C; SRIVASTAVA NAVEEN P; CHEMGENES CORP 摘要:The present invention provides building blocks and methods for synthesizing very pure RNA in a form that can efficiently be modified at the 3′ end. Reverse RNA monomer phosphoramidites have been developed for RNA synthesis in 5′→3′ direction, leading to very clean oligo synthesis that allows for the introduction of various modifications at the 3′-end cleanly and efficiently. Higher coupling efficiency per step have been observed during automated oligo synthesis with the reverse RNA amidites disclosed herein, resulting in a greater ability to achieve higher purity and produce very long oligonucleotides. The use of the reverse RNA phosphoramidites in the synthetic process of this invention leads to oligonucleotides free of N+1 species.
专利号:US-11920171-B1 优先权日:2016-05-06 标题:Synthesis and oxidation of methane 发明人:MANSOORABADI STEVEN 权利人:UNIV AUBURN 摘要:The present disclosure describes genes and proteins of the coenzyme F430 synthetic pathway. The genes and proteins in the pathway find uses as isolated nucleic acids, transformation vectors, a transformation media, genetically modified cells, methods of modulating methanogenesis, methods of modulating methane oxidation, methods of making a tetrapyrrole compound, methods of oxidizing methane, methods of biogenic methane synthesis is provided, methods of assaying an organism for potential methanogenic or methanotrophic activity, and isolated proteins.
专利号:US-2022387957-A1 优先权日:2019-11-04 标 题 :Microwave-assisted method for synthesis of oligo- and polysaccharides on solid phase
专利号:CN-104096239-A 优先权日:2014-01-10 标 题:Application of hALR gene micro-ring eukaryotic expression vector in reducing synthesis of liver collagen