专利号:US-5091066-A 优先权日:1987-11-19 标 题 :Electrochemical synthesis of 2-methyl-5-pyrazinoic acid 发明人:FOA MARCO; FORLINI FABRIZIO; GATTI NORBERTO; BORSOTTI GIAMPIERO 权利人:MINI RICERCA SCIENT TECNOLOG 摘要:There is disclosed a process for the preparation of 2-methyl-5-pyrazinoic acid consisting of electrochemically oxidizing a compound having formula: ##STR1## wherein X is --OH, Cl, Br, --O--CO--R, --O--SO 2 --R, in which R is a C 1 -C 5 alkyl radical, optionally substituted with F or Cl, or it is a C 6 -C 12 aryl radical, in an aqueous alkaline medium, at a temperature ranging from 20° C. to 90° C., using anodes coated with nickel oxide-hydroxide.
专利号:EP-0316945-B1 优先权日:1987-11-19 标 题:Electrochemical synthesis of 2-methyl-5-pyrazinoic acid
专利号:JP-2594825-B2 优先权日:1987-11-19 标题:Method for electrochemical synthesis of 2-methyl-5-pyrazinecarboxylic acid
专利号:EP-0316945-A1 优先权日:1987-11-19 标 题:Electrochemical synthesis of 2-methyl-5-pyrazinoic acid
专利号:AU-619219-B2 优先权日:1987-11-19 标题 :Electrochemical synthesis of 2-methyl-5-pyrezinoic acid
专利号:JP-H02111763-A 优先权日:1987-11-19 标题 :Electrochemical synthesis method of 2-methyl-5-pyrazinecarboxylic acid
参考文献:10.1107/s1600536809041440 摘要:Fan C, Wei X, Li L. Poly[[bis(μ2-6-methylpyrazin-2-carboxylato-κ3N1,O:N4)copper(II)] dihydrate]. Acta Crystallogr E Struct Rep Online. 2009 Oct 23;65(11):m1412. doi: 10.1107/s1600536809041440.