CAS: 3376-24-7; N-Benzylidene-2-Methylpropan-2-Amine Oxide

该化合物是一种属于硝基苯类的有机化合物,其特征是存在一个硝基功能组,由氮原子双柱组成,该组由氧原子双柱组成,与氧原子和碳原子单柱组成.该组具有一个叔丁基组,该组有助于其成份的成份,以及一个苯组,该组增强了其稳定性和再活性.N-tert-丁基-苯基-苯球在自由激进研究中扮演了旋转陷阱的作用,允许对反应性物种进行检测和定性.该组一般在室温下具有固态,在有机溶剂中具有溶解性.该组具有有趣的化学特性,包括能够形成稳定的吸附剂,使其在各种应用中具有价值,包括有机合成和材料科学.在处理这一化合物时,应当采取安全防范措施,因为许多有机化学品都具有潜在的健康危害.

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合成工艺路线路线简述

    📜N-Benzyl-N-(Tert-Butyl)Hydroxylamine置于gold,氧气体系中,用 甲醇 作为反应溶剂,化学反应 2.0H,以91%的收率获得产物n-叔丁基-α-苯基硝酮
    参考文献:纳米孔金催化剂好氧氧化羟胺作为硝酮的有效合成方法
    标题:纳米孔金催化剂好氧氧化羟胺作为硝酮的有效合成方法
    摘要:通过在温和条件下用分子氧作为氧化剂对n,N-二取代羟胺进行好氧氧化,使用无载体的纳米多孔金(aunpore)作为非均相催化剂,可以轻松实现硝酮的制备.多种胺以高化学产率被氧化成相应的硝酮.催化剂足够坚固,可以重复使用而不会浸出.
    DOI:10.1016/j.Tet.2015.05.094

    海关参考信息

    专利信息


    专利号:US-10487099-B2
    优先权日:2017-06-30
    标 题:Synthesis of hypervalent iodine reagents with dioxygen
    发明人：POWERS DAVID CHARLES; MAITY ASIM; HYUN SUNG-MIN
    权利人:TEXAS A & M UNIV SYS
    摘要:Methods of synthesis of hypervalent iodine reagents and methods for oxidation of organic compounds are disclosed.

    专利号:US-2012267111-A1
    优先权日:2009-12-30
    标题 :Synthesis of Degradable Polymers Downhole for Oilfield Applications
    发明人：KHLESTKIN VADIM KAMIL EVICH
    权利人:KHLESTKIN VADIM KAMIL EVICH
    摘要:A method is given for polymerizing monomers downhole to create well treatment polymers. The monomers each contain two polymerizable groups and a degradable group or groups which allow the polymer to degrade under downhole conditions, for example by hydrolysis. Polymerization downhole allows easier, more precise, placement of polymer. Polymer obtained from monomers pumped downhole may be used, for example, for fluid diversion plugs, isolation plugs, formation consolidation, flowback control, and fluid loss control. Synthesized polymer may form gels, films, solids or other structure in treated wellbores, fractures, and/or formations. After the desired effect is achieved, the deposited polymer degrades and the polymer degradation products dissolve, leaving the wellbore, fracture and/or formation clean, with no damage that might have decreased fluid flow.

    专利号:WO-2011081547-A1
    优先权日:2009-12-30
    标题 :Synthesis of degradable polymers downhole for oilfield applications

    专利号:KR-20220169970-A
    优先权日:2021-06-21
    标题 :Method for synthesis of aminobenzyne and multisubstituted organic nitrogen compounds using aza-brook rearrangement and multisubstituted organic nitrogen compounds prepared using the same

    专利号:US-6512143-B1
    优先权日:1998-07-10
    标 题:Salts of N-tert-butylhydroxylamine
    发明人：BLIXT JOERGEN
    权利人:ASTRAZENECA AB
    摘要:Novel salts of N-tert-butylhydroxylamine with lower carboxylic acids are disclosed, together with processes for their preparation. The salts possess advantageous properties that render them useful in synthesis.

    专利号:BR-102016007903-A2
    优先权日:2016-04-08
    标题:? PROCESS OF SYNTHESIS OF CATALYSTS BASED ON G-C3N4 DOPED WITH TRANSITIONAL METALS?

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    合成参考文献


    摘要:Li, Y.; Xie, W.; Jiang, X., Science of Synthesis Knowledge Updates, (2016) 2, 48.
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