CAS: 16829-91-7; Tetraoctylammonium Iodide

该化合物是一种四硝基铵盐,广泛用作有机合成的逐步转移催化剂,其长的烷基链会提高非极溶剂的溶性,便利非极溶剂之间的反应.碘化抗冲具有核生殖特性,使其在授糖,迁移和聚合反应中具有价值.这种复合物具有高度的热稳定性,在两阶段系统中特别有效,提高了反应效率和选择性.它还被用于电化学应用和某些配方的稳定剂.它与各种反应条件的一贯性能和兼容性使它成为工业和实验室规模工艺的可靠选择.

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CAS号1116-76-3 三辛胺 | CAS号629-27-6 1-碘辛烷 | CAS号629-27-6 1-碘辛烷 | CAS号70098-05-4 tetra°Ctylammon...

合成工艺路线路线简述

    📜三辛胺,1-碘辛烷 反应生成四正辛基碘化铵
    参考文献:イオン液体の製造方法及びイオン液体製造のための中間体の製造方法
    标题:イオン液体の製造方法及びイオン液体製造のための中間体の製造方法
    摘要:提供制造所需高纯度离子液体的离子液体制造方法以及制造这种离子液体所需中间体的制造方法.本发明的离子液体制造方法是一种制造所需离子液体q+z-的方法,该离子液体由阳离子q+和阴离子z-组成,包括通过再结晶精制具有可再结晶融点的高融点中间体q+y-的步骤,以及从经过精制的高融点中间体q+y-直接或间接获得离子液体q+z-的步骤.本发明的强碱性中间体和超亲水性中间体的制造方法包括从精制后的高融点中间体q+y-通过复分解沉淀法获得强碱性中间体或超亲水性中间体的步骤,或者从经过精制的高融点中间体q+y-通过复分解沉淀法获得强碱性中间体的步骤,并包括从该强碱性中间体通过中和法获得超亲水性中间体的步骤.[选择图]图1

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    专利信息


    专利号:US-2023286918-A1
    优先权日:2020-07-02
    标 题:Manufacturing process for 3,5-dichloropicolinonitrile for synthesis of vadadustat
    发明人:JURKAUSKAS VALDAS; JUNG YOUNG CHUN; KWON TAESOO; KANNAN ARUNACHALAM; GONDI VIJAYA BHASKER
    权利人:AKEBIA THERAPEUTICS INC
    摘要:Disclosed herein are methods and processes of preparing vadadustat or a pharmaceutically acceptable salts thereof, and intermediates (e.g., a compound of Formula (I), (I-F), (II), or (IV), or a pharmaceutically acceptable salts thereof) useful for the synthesis of vadadustat.

    专利号:US-9586984-B2
    优先权日:2007-04-09
    标题:One-pot synthesis of alpha/beta-O-glycolipids
    发明人:GERVAY-HAGUE JACQUELYN; DU WENJUN; KULKARNI SUVARN S; SCHOMBS MATTHEW
    权利人:UNIV CALIFORNIA
    摘要:The present invention provides a one-pot method of preparing an unprotected α-O-glycolipid. The first step involves contacting a protected α-iodo sugar with a catalyst and a lipid comprising a hydroxy group, under conditions sufficient to prepare a protected α-O-glycolipid. The second step involves deprotecting the protected α-O-glycolipid under conditions sufficient to prepare the unprotected α-O-glycolipid, wherein the contacting and deprotecting steps are performed in a single vessel. The present invention also provides a one-pot method of preparing an unprotected β-O-glycolipid following the steps for the preparation of the unprotected α-O-glycolipid.

    专利号:WO-2024013736-A1
    优先权日:2022-07-12
    标题 :Process for preparing substituted benzamides
    发明人:HAMIRANI BHAVINKUMAR; MAHESH GANDHAM; SREEDEVI MANNAM; PILLAI BIJUKUMAR GOPINATHAN
    权利人:ADAMA MAKHTESHIM LTD
    摘要:The present invention relates to new intermediates for the preparation of pyridylmethylbenzamides via substituted hydroxyiminopyridines or acetamidopyridines, and their innovative preparation processes. The invention discloses, in particular, the total synthesis of fluopicolide fungicide. The preparation of the main substances of the fluopicolide synthesis, specifically, substituted pyridine-2-ylmethanamine or its salt, is disclosed via two different synthesis routes, comprises two novel substances.

    专利号:US-2008214386-A1
    优先权日:2004-03-01
    标题:Catalyst for Cyclic Carbonate Synthesis
    发明人:TAKAHASHI TOSHIKAZU; WATAHIKI TSUTOMU; YASUDA HIROYUKI; SAKAKURA TOSHIYASU
    权利人:TAKAHASHI TOSHIKAZU; WATAHIKI TSUTOMU; YASUDA HIROYUKI; SAKAKURA TOSHIYASU
    摘要:Provided are a solid catalyst which gives a cyclic carbonate at a high yield and a high selectivity, which is stable and which may be readily separated after reaction; and a method of industrially advantageous, inexpensive and safe production of a cyclic carbonate by the use of the catalyst. The catalyst contains an inorganic solid substance having a surface modified with an ionic substance containing a Group 15 element; or contains an ionic substance containing a Group 15 element, and an inorganic solid substance. The modifying group for surface modification of an inorganic solid substance is an ionic substance containing a Group 15 element. The ionic substance containing a Group 15 element is at least one substance selected from organic phosphonium salts, organic ammonium salts, organic arsonium salts and organic antimonium salts.

    专利号:WO-2008124729-A1
    优先权日:2007-04-09
    标题 :One-pot synthesis of alpha/beta-o-glycolipids

    专利号:CA-2464107-A1
    优先权日:2001-11-26
    标 题:Process for the synthesis of amine ethers from secondary amino oxides and uses

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    📌 第三方产品分析报告

    ✅ COA系统入驻 | 共享模式

    合成参考文献


    参考文献:10.1007/bf00616959
    摘要:Apraskin SP, Granskii PV, Denisov GS. Studies on the influence of the electric field on the band of charge transfer of tetraoctylammonium iodide by modulation spectroscopy. Journal of Applied Spectroscopy. 1974 Dec;21(6):1658–60. doi: 10.1007/bf00616959.
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