CAS: 73513-43-6; 6-Methylheptyl Nitrate

相似化合物

100502-66-7 27247-96-7 543-29-3

C7-9-烷基醇置于硫酸,硝酸体系中,用99.3%的收率获得产物硝酸异辛酯
参考文献:一种硝酸异辛酯的合成方法
标题:一种硝酸异辛酯的合成方法
摘要:本发明提供了一种硝酸异辛酯的合成方法,以固体酸为催化剂,用计量泵将异辛醇,硝酸送入微管式反应器,反应液经中和,分液,膜过滤得到硝酸异辛酯产品的合成工艺.本发明工艺安全性高,操作稳定,能耗低,三废少.

专利信息

专利号:US-10017457-B2
优先权日:2014-03-07
标题:Continuous synthesis of isooctyl nitrate in a flow reactor
发明人：MA BING; SHEN WEI; WANG YANHUA; ZHANG MO
权利人:CORNING INC
摘要:A process for synthesizing isooctyl nitrate in a continuous flow reactor comprises flowing a H2SO4-HNO3 mixture within a flow reactor, flowing isooctyl alcohol into said flow reactor so as to mix the isooctyl alcohol with the H2SO4-HNO3 mixture and produce a reaction mixture stream flowing in said reactor, maintaining the reaction mixture stream flowing in said flow reactor at a reaction temperature within in the range −10° to 35° C. inclusive, and wherein the residence time of the reaction mixture stream in the flow reactor is greater than or equal to 5 seconds and less than or equal to 40 seconds, and wherein the H2SO4 of the H2SO4-HNO3 mixture is H2SO4 having a concentration of in the range of 85 to 95% inclusive, more desirably 88 to 92% inclusive, most desirably of 90%.

专利号:EP-3114108-B1
优先权日:2014-03-07
标题:Continuous synthesis of isooctyl nitrate in a flow reactor

专利号:US-2017066710-A1
优先权日:2014-03-07
标 题:Continuous synthesis of isooctyl nitrate in a flow reactor

专利号:EP-3114108-A1
优先权日:2014-03-07
标题:Continuous synthesis of isooctyl nitrate in a flow reactor

专利号:CN-113105333-A
优先权日:2014-03-07
标 题 :Continuous Synthesis of Isooctyl Nitrate in a Flow Reactor

专利号:WO-2015134703-A1
优先权日:2014-03-07
标题 :Continuous synthesis of isooctyl nitrate in a flow reactor