专利号:US-7501599-B2 优先权日:2001-04-24 标题 :Apparatus for plasma synthesis of metal oxide nanopowder 发明人:BOULOS MAHER I; JUREWICZ JERZY W; NESSIM CHRISTINE A ABDEL MESSIH 权利人:TEKNA PLASMA SYSTEMS INC 摘要:A process and apparatus for the synthesis of metal oxide nanopowder from a metal compound vapour is presented. In particular a process and apparatus for the synthesis of TiO 2 nanopowder from TiCl 4 is disclosed. The metal compound vapour is reacted with an oxidizing gas in electrically induced RF frequency plasma thus forming a metal oxide vapour. The metal oxide vapour is rapidly cooled using a highly turbulent gas quench zone which quickly halts the particle growth process, yielding a substantial reduction in the size of metal oxide particles formed compared with known processes. The metal compound vapour can also react with a doping agent to create a doped metal oxide nanopowder. Additionally, a process and apparatus for the inline synthesis of a coated metal oxide is disclosed wherein the metal oxide particles are coated with a surface agent after being cooled in a highly turbulent gas quench zone.
专利号:US-2002184969-A1 优先权日:2001-03-29 标 题 :Combinatorial synthesis of particulate materials 发明人:KODAS TOIVO T; HAMPDEN-SMITH MARK J 摘要:Methods for fabricating and analyzing particulates having a varying material property such that particulates having a selected desirable material property can be identified. The particulates can be analyzed to determine the particulates having the best properties for a particular application. The particulates can be metals, inorganic compounds, organic compounds and composites. The method of the present invention enables the rapid and economical fabrication and screening of a large number of different compositions.
专利号:US-11746274-B1 优先权日:2022-02-25 标题 :Ionic liquid monomer for synthesis of friction reducer and methods thereof 发明人:ZHANG XUAN; RUEDA JOSE I; HAN MING; BATAWEEL MOHAMMED; QI ZIYUAN 权利人:SAUDI ARABIAN OIL CO 摘要:A composition includes an ionic liquid monomer having the following structure: n nwhere n is an integer from 1 to 5 and the ionic liquid monomer has a melting point less than 100° C. A method of making the ionic liquid includes providing a mixture comprising a sulfonic acid and a diamine in a solvent, and maintaining the mixture at a temperature ranging from 10 to 80° C. for a time ranging from 1 to 10 hours to form an ionic liquid monomer having a melting point less than 100° C. A method of making a polymer from the ionic liquid monomer is also provided.
专利号:US-11078093-B2 优先权日:2017-06-30 标 题 :Surfactant-assisted synthesis of surface-functionalized nanoparticle-polymer electrospun composites 发明人:CWIERTNY DAVID; MYUNG NOSANG; PETER KATHERINE T; PARKIN GENE FRANCIS 权利人:UNIV CALIFORNIA; UNIV IOWA RES FOUND 摘要:A method is disclosed for synthesizing nanofilters for water treatment. The method includes: dispersing an active binding agent in an organic solvent solution to create a suspension of the active binding agent and the solution of the solvent; dissolving an organic polymer resin and an anionic surfactant in the suspension of the active binding agent and the solvent solution to create a sol gel; and electrospinning the sol gel to form electrospun nanofiber composites with embedded, surface-active nanoparticles.
专利号:US-8829238-B2 优先权日:2011-09-22 标 题:Methods for the synthesis of deuterated acrylate salts 发明人:YANG JUN; BONNESEN PETER V; HONG KUNLUN 权利人:YANG JUN; BONNESEN PETER V; HONG KUNLUN; UT BATTELLE LLC 摘要:A method for synthesizing a deuterated acrylate of the Formula (1), the method comprising: (i) deuterating a propiolate compound of Formula (2) to a methyne-deuterated propiolate compound of Formula (3) in the presence of a base and D 2 O: and (ii) reductively deuterating the methyne-deuterated propiolate compound of Formula (3) in a reaction solvent in the presence of deuterium gas and a palladium-containing catalyst to afford the deuterated acrylate of the Formula (1). The resulting deuterated acrylate compounds, derivatives thereof, and polymers derived therefrom are also described.
专利号:US-2002176927-A1 优先权日:2001-03-29 标 题:Combinatorial synthesis of material systems 发明人:KODAS TOIVO T; HAMPDEN-SMITH MARK J 摘要:Methods for formulating material systems of varying chemistry and stoichiometry. The material systems include two or more components and can be analyzed to select the system having the best properties for a particular application. Specific examples of materials systems that can be fabricated and analyzed according to the present invention include layers for membrane electrode assemblies (MEA's) that are useful in the construction of fuel cells and similar devices.
[参考文献]: A Wahid, Et Al. Lead Exposure In Papier Maché Workers. Hum Exp Toxicol. 1997 May;16(5):281-3. [参考文献]: J Descotes, Et Al. Comparative Effects Of Various Lead Salts On Delayed Hypersensitivity In Mice. J Appl Toxicol. 1984 Oct;4(5):265-6. [参考文献]: J Nunes, Et Al. Toxicosis Associated With Dual Oral Exposure Of Rats To Lead And Trichloroethylene. Toxicol Pathol. 2001 Jul-Aug;29(4):451-7. [参考文献]: Lachlan C W Maclean, Et Al. Chemical Transformations Of Lead Compounds Under Humid Conditions: Implications For Bioaccessibility. Environ Geochem Health. 2013 Feb;35(1):153-9. [参考文献]: M B Rabinowitz, Et Al. Isotopic Characterization Of Six Major Brands Of White Basic Lead Carbonate Paint Pigments. Bull Environ Contam Toxicol. 2002 Nov;69(5):617-23.