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CAS号7440-62-2 钒粉 | CAS号7782-50-5 氯气 | CAS号7632-51-1 四氯化钒 | CAS号80937-33-3 oxygen | CAS号7718-98-1 氯化钒 | CAS号1636-01-7 二氯氧化钒 | CAS号12035-98-2 氧化钒 | CAS号10213-09-9 二氯氧钒 | CAS号12035-98-2 氧化钒 | CAS号13520-87-1 oxovanadium,hyd... | CAS号10213-09-9 二氯氧钒 | CAS号1801-77-0 二氯乙氧基合氧钒 | CAS号18822-50-9 hydroxy-triphen... | CAS号7440-62-2 钒粉 | CAS号994-31-0 氯化三乙基锡 | CAS号227467-35-8 dioxovanadium(V... | CAS号10049-04-4 二氧化氯 | CAS号80937-33-3 oxygen合成工艺路线路线简述
- 合成目标产物 Vanadium(V) Trichloride Oxide 主要起始原料 Thionyl Chloride And Vanadium (Iv) Oxide
- (文献来源)合成步骤主要原料 Thionyl Chloride 和 Vanadium (Iv) Oxide
📜四氯化钒置于air体系中,用 Neat (No Solvent) 作为反应溶剂,化学反应生成 三氯一氧化钒 三氯代氧化钒(V)
参考文献:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: V: Mvol.B1,88,Page 237-239
标题:Gmelin Handbuch Der Anorganischen Chemie,Gmelin Handbook: V: Mvol.B1,88,Page 237-239
专利信息
专利号:US-2011172437-A1
优先权日:2008-04-01
标题:Perfluorophthalocyanine Molecules and Methods of Synthesis
发明人:GORUN SERGIU M; GERDES ROBERT; GERDES OLGA; LAPOK LUKASZ
权利人:NEW JERSEY TECH INST
摘要:Advantageous methods for synthesis of fluorinated phthalocyanines are provided. Typical implementation involves a reaction mixture that includes perfluoro compound that is reacted for a reaction period sufficient to yield a fluorinated phthalocyanine of formula F 64 PcM, wherein “Pcâ€? is any phthalocyanine macrocycle and “Mâ€? is hydrogen. Novel fluorinated phthalocyanine molecules/compounds are also provided herein, including specifically compounds that include fluorinated phthalocyanines wherein “Mâ€? is Cu or Vâ•?O. The fluorinated phthalocyanines have wide ranging applications, e.g., corrosion-related applications, coating-related applications, catalysis, and the production of optical and electronic materials.
专利号:US-2024199566-A1
优先权日:2022-11-16
标题:Catalytic synthesis of delta-valerolactone (dvl) from furfural-derived 2-hydroxytetrahydropyran (hthp)
发明人:HUBER GEORGE; DASTIDAR RAKA; JOHNSTONE SAM; MCCLELLAND DANIEL
权利人:WISCONSIN ALUMNI RES FOUND
摘要:A method to make delta-valerolactone (“DVLâ€?) by dehydrogenating 2-hydroxytetrahydropyran (“HTHPâ€?). The HTHP is contacted with a supported-metal catalyst for a time, at a temperature, and at a pressure wherein at least a portion of the HTHP is converted to DVL via dehydrogenation of the HTHP. The HTHP may be derived from biomass. Thus, the method yields DVL without requiring a petroleum-based feedstock.
专利号:US-10106487-B2
优先权日:2015-06-10
标 题:Oxidative dehydrogenation of lactate esters to pyruvate esters
发明人:UMBARKAR SHUBHANGI BHALCHANDRA; DONGARE MOHAN KERABA; PANDHARE SWATI LAXMIKANTRAO; KHOMANE SONALI BALASAHEB; DOKE DHANANJAY SHAHAURAJ
权利人:COUNCIL SCIENT IND RES
摘要:The present invention relates to a simple one step oxidative dehydrogenation process for the synthesis of alkyl pyruvate with 100% selectivity towards alkyl pyruvate comprising reacting an alkyl lactate in the presence of catalyst at the temperature ranging from 25-100° C. for the time period ranging from 5 to 40 hours in an organic solvent and hydrogen peroxide to afford alkyl pyruvate.
专利号:US-8889094-B2
优先权日:2011-02-23
标题 :Purification of TiCl4 through the production of new co-products
发明人:HELBERG LISA EDITH
权利人:HELBERG LISA EDITH; DU PONT
摘要:The present disclosure relates to reacting tin metal with crude TiCl 4 containing arsenic to produce pure TiCl 4 , SnCl 4 , and an arsenic solid co-product. In some embodiments, the contaminant vanadium is removed as well. In another embodiment, the vanadium is removed separately through a commercial process and the resulting arsenic containing commercial grade of purified TiCl 4 is reacted with elemental tin, sulfur and ferric chloride to substantially reduce the arsenic. The reaction is preferably done in a continuous fashion in two stages for maximum through-put and utility at an elevated temperature. Distillation can be used to purify the TiCl 4 produced and simultaneously yield a purified SnCl 4 product. The synthesis of SnCl 4 in this method utilizes waste chloride to save virgin chlorine which would otherwise be used.
专利号:US-4165438-A
优先权日:1973-05-03
标 题 :Synthesis of acrylic acids and esters
发明人:SCHNEIDER RONALD A
权利人:CHEVRON RES
摘要:Acrylic acids and esters are produced by reacting a lower alkanoic acid or lower alkyl ester thereof with formaldehyde in the presence of a vanadium orthophosphate catalyst having an intrinsic surface area of from about 10 m2/g to about 50 m2/g.
专利号:US-4012492-A
优先权日:1975-06-10
标 题 :Synthesis of anhydrous metal perchlorates
发明人:SCHACK CARL J; PILIPOVICH DONALD
权利人:US NAVY
摘要:Preparation of titanium tetraperchlorate, vanadium perchlorate, and chromylerchlorate by the reactions of chlorine perchlorate with the respective anhydrous metal chlorides at a temperature from about -45° C to about 20° C. These perchlorates are useful in compounding gas generating compositions.